Search results for "Characterisation"
showing 10 items of 45 documents
Ceramic productions and human interactions during the Early Bronze Age in northern Iberia
2021
The Early Bronze Age ceramic collection found into the caves of La Llana and El Toral III in Asturias (Spain) presents common decoration such as that found in the centre of Cantabrian Spain from the same period, which resembles others found in the Ebro Valley and Atlantic Europe. Therefore, the main objective of this study it is to identify the raw material origin and understand the pottery production process during the Early Bronze Age in the Cantabrian region. A methodological approach based on the chemical and mineralogical analysis of vessels and experimentally fired clay samples collected all over the centre of this region was developed. Furthermore, the post-depositional processes aff…
Technical Note on the quality of DNA sequencing for the molecular characterisation of genetically modified plants
2018
Abstract As part of the risk assessment (RA) requirements for genetically modified (GM) plants, according to Regulation (EU) No 503/2013 and the EFSA guidance on the RA of food and feed from GM plants (EFSA GMO Panel, 2011), applicants need to perform a molecular characterisation of the DNA sequences inserted in the GM plant genome. The European Commission has mandated EFSA to develop a technical note to the applicants on, and checking of, the quality of the methodology, analysis and reporting covering complete sequencing of the insert and flanking regions, insertion site analysis of the GM event, and generational stability and integrity. This Technical Note puts together requirements and r…
Microstructure and shear strength evolution of a lime-treated clay for use in road construction
2020
The results of a comprehensive experimental programme are presented for assessing the long-term microstructural modifications and evaluating the effects of microstructural rearrangement on the stress–strain behaviour of a lime-treated high-plasticity clay for road embankments. The stress–strain behaviour at different lime content and curing time was investigated by means of direct shear tests; microstructural analyses were carried out combining Scanning Electron Microscope observations and Mercury Intrusion Porosimetry tests. The results show that the stress–strain behaviour of treated clay is strongly dilatant with a high peak of strength, which increases with time and lime content. Furthe…
ATR-FTIR chemical screening for adulterants and sugar characterisation in honeys
2019
The search for improvements in honey analysis is an important topic due to the relevance that adulterations and variations of sugar composition have in this food. Attenuated Total Reflectance Fourier Transform InfraRed spectroscopy (ATR-FTIR) is a reliable and fast analytical instrumentation for analysis of liquids, semi-solids and solids, which is currently used in food chemistry for qualitative and quantitative investigations. This work is aimed to build a fast analytical method, using ATR-FTIR and Partial Least Square (PLS) chemometric tool, to quantitative determination of glucose, fructose and sucrose present in honeys. We analyzed 25 honeys from Trentino and Sicily and a significant s…
Effect of substrate improvement on optimising biogas yield from anaerobic digestion
2014
Masteroppgave i fornybar energi ENE 500 Universitetet i Agder 2014 The anaerobic digestion process involves the decomposition of the organic matter to yield biogas; gas that is mainly composed of methane and carbon dioxide with traces of some other gases. This process is used for different purposes including municipal waste treatment, wastewater treatment, fertilizer production, and farm wastes disposal as well as energy production. It is accomplished in three main stages; hydrolysis, acidogenesis and methanogenesis with each of the stages achieved by specific microorganisms that are active in limited ranges of operational and environmental conditions. These conditions are controlled to ach…
Photoactivity of Nanostructured TiO2 Catalysts in Aqueous System and their Surface Acid-Base, Bulk and Textural Properties
2007
This work reports on the characterisation and determintion of the photocatalytic activity of some TiO2 catalysts prepared using TiCl4 as precursor. The samples, consisting of suspensions, dispersions or powders of nanonstructured anatase or rutile phases, were obtained in very mild conditions, i.e., by boiling the solution obtained after hydrolysis of TiCl4 at atmospheric pressure: it is worth noting that no calcination was necessary to obtain photoactive phases. The samples were characterised by X-ray diffraction (XRD), determination of the BET specific surface area (SSA), scanning electron microscopy (SEM) observations and diffuse reflectance spectroscopy (DRS). FT-IR spectroscopy was use…
The value of open-source clinical science in pandemic response
2021
International audience
Effect of two novel bio-based rejuvenators on the performance of 50% RAP mixes - a statistical study on the complex modulus of asphalt binders and as…
2019
An experimental study was conducted to evaluate the effectiveness of two bio-additives as rejuvenators on the properties of asphalt mixtures containing 50% RAP and their binder constituents containing 37% RAP binder. Before mixing, the rejuvenators were blended with fresh bitumen and the extracted and recovered RAP bitumen, and changes in the rheological properties of the binders were assessed using performance grading (PG) criteria. The results showed that both rejuvenators could improve the low-temperature performance of the aged RAP binder and restore its low-temperature properties. Master curves for the unaged, RTFO-aged, and PAV aged blends were constructed using both the Christensen-A…
Assessment of Plant Origin By-Products as Lightweight Aggregates for Bio-Composite Bounded by Starch Binder
2022
Thermal insulation bio-composites made of plant origin by-products as bio-aggregates are one of the ways to decrease the impact of the building and construction sector on CO2 emissions. In this study, three bio-aggregates were analysed for their potential use in the production of bio-composites with potato starch binder. Technologically important properties, such as particle size, shape and compacted bulk density, as well as properties of the resulting bio-composites were identified. The main characteristics of the aggregates are relatively similar: density of 80–100 kg/m3, thermal conductivity of 0.042–0.045 W/m∙K, specific heat capacity of 1240–1330 J/g∙K, ki…
Degradation study of XVIII century graffiti on the walls of Chiaramonte Palace (Palermo, Italy)
2010
A systematic investigation of the original materials and the degradation phenomena induced by soluble salts on the wall matrix and on the graffiti of the Inquisition jails of Chiaramonte Palace in Palermo (Italy) was carried out. Built in the XIV century, Chiaramonte Palace was used as Inquisition court during the XV–XVI centuries. The ancient graffiti, recently discovered, represent a unique historical witness of the prisoners that lived during that terrible period. In order to study the nature, the amount and the distribution of the salts in the masonry, stone materials sampled at different depth from the wall matrix and saline efflorescences were analysed. Different physical techniques w…