Search results for "DEPS"

showing 10 items of 94 documents

Antifungal effects of the bioactive compounds enniatins A, A1, B, B1

2010

To produce enniatin (ENs), Fusarium tricinctum CECT 20150 was grown in a liquid medium of potato (PDB), being mycotoxin purified by high performance liquid chromatography (HPLC) with a reverse phase semipreparative column using a mobile phase of acetonitrile/water using gradient condition. The purity of the ENs fractions was verified by analytical HPLC and LC/MS-MS. The pure fractions of ENs were utilized to study the biological activity on several mycotoxigenic moulds as Fusarium verticilloides, Fusarium sporotrichioides, Fusarium tricinctum, Fusarium poae, Fusarium oxysporum, Fusarium proliferatum, Beauveria bassiana, Trichoderma harzianum, Aspergillus flavus, Aspergillus parasiticus, Asp…

FusariumAntifungal AgentsChromatographybiologyantifungal activityTrichoderma harzianumFusarium proliferatumhplcMicrobial Sensitivity TestsToxicologybiology.organism_classificationFusarium sporotrichioidesAspergillus parasiticusMicrobiologyTandem Mass SpectrometryDepsipeptidesFusarium oxysporumenniatinEnniatinAspergillus ochraceusChromatography High Pressure LiquidToxicon
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Study of the potential toxicity of commercial crispy breads by evaluation of bioaccessibility and bioavailability of minor Fusarium mycotoxins

2011

Abstract Enniatins (ENs) are bioactive compounds produced by the secondary metabolism of several Fusarium strains and known to have several biological activities, such as acting as enzyme inhibitors, antifungal and antibacterial agents, and immunomodulatory substances. This study has investigated the ENs bioaccessibility, spiked in commercial wheat crispy bread at 1.5 and 3.0 μmol/g concentrations, their transepithelial transport and bioavailability using Caco-2 cells as a model of the human intestinal epithelium. The content (%) of the four ENs contained in the gastric fluid has resulted variable from 69% to 91%, considering the two concentrations assayed. The mean bioaccessibility data fo…

FusariumBiological AvailabilityFood ContaminationAbsorption (skin)Toxicologychemistry.chemical_compoundFusariumDepsipeptidesHumansFood scienceSecondary metabolismMycotoxinTriticumchemistry.chemical_classificationbiologyGastric fluidBiological TransportBreadGeneral MedicineMycotoxinsbiology.organism_classificationBioavailabilityEnzymechemistryEnvironmental chemistryCaco-2 CellsFood SciencePotential toxicityFood and Chemical Toxicology
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A chemical approach for the reduction of beauvericin in a solution model and in food systems.

2014

Abstract Beauvericin (BEA) is a bioactive compound produced by the secondary metabolism of several Fusarium strains with a strong antibacterial, antifungal, and insecticidal activities. This study evaluated the reduction of BEA added at 25 mg/kg in phosphate buffer saline (PBS) solutions at pH of 4, 7 and 10, or to different cereal products (kernels and flours) by the bioactive compounds phenyl isothiocyanate (PITC) and benzyl isothiocyanate (BITC). The concentration of the mycotoxin was evaluated using liquid chromatography coupled to the diode array detector (LC-DAD). In solution, BEA reduction ranged from 9% to 94% on a time-dependent fashion and lower pH levels resulted in higher BEA re…

FusariumChromatographybiologyBenzyl isothiocyanatePhenyl isothiocyanatefood and beveragesFood ContaminationGeneral MedicineModels TheoreticalToxicologybiology.organism_classificationBeauvericinBioactive compoundchemistry.chemical_compoundchemistryChromatography detectorDepsipeptidesSecondary metabolismMycotoxinOxidation-ReductionFood ScienceChromatography LiquidFood and chemical toxicology : an international journal published for the British Industrial Biological Research Association
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Study of the potential toxicity of enniatins A, A(1), B, B(1) by evaluation of duodenal and colonic bioavailability applying an in vitro method by Ca…

2010

Abstract The bioavailability of the minor Fusarium mycotoxins enniatins (ENs) utilizing an in vitro method which allows the simulation of the small and large intestine tracts has been studied. This method, based on the application of the Caco-2 cells grown alone or in symbiosis with several strains characteristics of the gastrointestinal tract, has permitted to simulate the duodenal and colonic intestinal compartments, respectively. The duodenal bioavailability expressed as absorption value after 4 h of exposure, ranged from 57.7 to 76.8% for EN A, from 68.8 to 70.2% for EN A1, from 65.0 to 67.0% for EN B, and from 62.2 to 65.1% for EN B1. Colonic bioavailability after 48 h of incubation ra…

FusariumColonDuodenumBiological AvailabilityAbsorption (skin)PharmacologyToxicologyRisk AssessmentFusariumDepsipeptidesToxicity TestsmedicineHumansLarge intestineIncubationGastrointestinal tractbiologyChemistryMycotoxinsbiology.organism_classificationIn vitroBioavailabilitymedicine.anatomical_structureIntestinal AbsorptionCaco-2Caco-2 CellsToxicon : official journal of the International Society on Toxinology
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Presence of Enniatins and Beauvericin in Romanian Wheat Samples: From Raw Material to Products for Direct Human Consumption

2017

In this study, a total of 244 wheat and wheat-based products collected from Romania were analyzed by liquid chromatography tandem mass spectrometry (LC-MS/MS) in order to evaluate the presence of four enniatins (ENs; i.e., ENA, ENA1, ENB, and ENB1) and beauvericin (BEA). For the wheat samples, the influence of agricultural practices was assessed, whereas the results for the wheat-based products were used to calculate the estimated daily intake of emerging mycotoxins through wheat consumption for the Romanian population. ENB presented the highest incidence (41% in wheat and 32% in wheat-based products), with its maximum levels of 815 μg kg−1 and 170 μg kg−1 in wheat and wheat-based products,…

FusariumDaily intakeHealth Toxicology and MutagenesisorganicFlourPopulationemerging mycotoxinslcsh:MedicineFood ContaminationRaw materialToxicologyRisk Assessment01 natural sciencesArticlechemistry.chemical_compound0404 agricultural biotechnologyFusariumLiquid chromatography–mass spectrometryDepsipeptidesHumansFood scienceLC-MS/MSeducationMycotoxinTriticumestimated daily intakeconventionalcerealseducation.field_of_studywheat productsbiologyRomania010401 analytical chemistrylcsh:Rfood and beveragesBread04 agricultural and veterinary sciencesMycotoxinsbiology.organism_classification040401 food scienceBeauvericin0104 chemical sciencesemerging mycotoxins; LC-MS/MS; cereals; organic; conventional; wheat products; estimated daily intakechemistryAgronomyEnvironmental MonitoringFood contaminantToxins
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Interaction effects of Fusarium enniatins (A, A1, B and B1) combinations on in vitro cytotoxicity of Caco-2 cells

2014

Abstract Foodstuff is usually contaminated by more than one mycotoxin, however toxicological data are lacking as regards the effects in combinations compared to their individual effect. This study investigated the in vitro effects of enniatins (ENs) A, A1, B and B1, alone and in combinations, on Caco-2 cells viability by MTT assay after 24 h of exposure. Cells were treated with concentrations ranging from 0.9 to 15.0 μM, individually and in combination of two, three and four mycotoxins. Dose–response curves were generated for each mycotoxin and the isobologram method was used to determine the interactive effects of tested mixtures. Tested ENs produced significant cytotoxic effects both indi…

FusariumDose-Response Relationship DrugbiologyCell SurvivalChemistryDrug SynergismGeneral MedicineMycotoxinsToxicologybiology.organism_classificationInteractionIn vitroToxicologyInhibitory Concentration 50chemistry.chemical_compoundFusariumCaco-2DepsipeptidesHumansCytotoxic T cellMTT assayFood scienceCaco-2 CellsMycotoxinCytotoxicityToxicology in Vitro
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Emerging Fusarium mycotoxins in organic and conventional pasta collected in Spain

2012

Abstract One of the main sources of emerging Fusarium mycotoxins in human nutrition is the cereals and cereal products. In this study, an analytical method to determine enniatins A, A1, B and B1 (ENs), beauvericin (BEA) and fusaproliferin (FUS) based on Ultra-Turrax extraction followed by liquid chromatography coupled to triple quadrupole mass spectrometer detector (MS/MS QqQ), was applied for the analysis of pasta. For this purpose, 114 commercial samples of pasta were acquired from supermarkets located in Valencia. The results showed higher frequencies of contamination in organic pasta than in conventional pasta, while the concentration levels were variable for both types of pasta. In pos…

FusariumFood ContaminationToxicologychemistry.chemical_compoundFusariumTandem Mass SpectrometryLiquid chromatography–mass spectrometryDepsipeptidesHumansFood scienceMycotoxinOrganic AgriculturebiologyTerpenesDietary exposureReproducibility of ResultsGeneral MedicineMycotoxinsContaminationbiology.organism_classificationBeauvericinTriple quadrupole mass spectrometerHuman nutritionchemistrySpainPublic HealthEdible GrainChromatography LiquidFood ScienceFood and Chemical Toxicology
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Biosynthesis of beauvericin and enniatins in vitro by wheat Fusarium species and natural grain contamination in an area of central Italy

2015

Contamination of wheat grain by beauvericin (BEA) and enniatins (ENs) is a global emerging mycotoxicological food problem. In this study, strains of Fusarium avenaceum (FA), Fusarium poae (FP), Fusarium equiseti and Fusarium sporotrichioides, all potential BEA and EN producers, isolated from 162 grain samples of durum and soft wheat harvested in 2009 and 2010 collected in an area of central Italy, were preliminarily screened for the presence of the esyn1 gene, encoding the multifunctional enzyme enniatin-synthetase for the detection of potential hexadepsipeptide-producing isolates. All positive isolates were tested for their ability to biosynthesize BEA and ENs in vitro. In addition, all wh…

FusariumFusarium avenaceumFood ContaminationMicrobiologyFungal Proteinschemistry.chemical_compoundFusariumBiosynthesisDepsipeptidesBotanyFusarium poaeFusarium poaeLC-DADFood scienceLC-MS/MSMycotoxinTriticumEnniatinbiologyMedicine (all)food and beveragesMycotoxinsContaminationbiology.organism_classificationBeauvericinFusarium sporotrichioidesBeauvericinIn vitroItalychemistryFood Science
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Individual and Combined Effect of Zearalenone Derivates and Beauvericin Mycotoxins on SH-SY5Y Cells

2020

Beauvericin (BEA) and zearalenone derivatives, &alpha

FusariumMTTElectrosprayTime FactorsHealth Toxicology and MutagenesisNeurotoxinslcsh:MedicineToxicologyMass spectrometryArticleSH-SY5Y cells03 medical and health scienceschemistry.chemical_compoundInhibitory Concentration 500404 agricultural biotechnologyCell Line TumorDepsipeptidesHumansMTT assayMycotoxinZearalenone030304 developmental biologyNeurons0303 health scienceszearalenone derivatesChromatographybiologyCell DeathDose-Response Relationship Druglcsh:RbeauvericinDrug Synergism04 agricultural and veterinary sciencesbiology.organism_classification040401 food scienceBeauvericinqTOF–MS/MSchemistryZeranolAntagonismToxins
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Production of enniatins A, A1, B, B1, B4, J1 by Fusarium tricinctum in solid corn culture: structural analysis and effects on mitochondrial respirati…

2013

Enniatins (ENs) are secondary fungal metabolites with hexadepsipeptidic chemical structure and they possess a number of potent biological activities that can contaminate several kind of food and foodstuffs increasing the exposure risk for consumers. ENs are produced by several Fusariun strains including Fusarium subglutinans, Fusarium proliferatum and Fusarium tricinctum. Production of a mixture of ENs was performed by culturing F. tricinctum ITEM 9496 on white corn as substrate. The solid culture components were dried and subsequently extracted with water/methanol (50/50 v/v, 0.5% NaCl), homogenised, filtered, extracted by ethyl acetate and analysed by liquid chromatography with diode arra…

FusariumMagnetic Resonance SpectroscopyChemical structureEthyl acetateFusarium proliferatumZea maysAnalytical Chemistry03 medical and health scienceschemistry.chemical_compoundFusariumLiquid chromatography–mass spectrometryDepsipeptidesChromatography High Pressure Liquid030304 developmental biology0303 health sciencesChromatographybiologyMolecular StructureChemistry030302 biochemistry & molecular biologySubstrate (chemistry)General MedicineNuclear magnetic resonance spectroscopyMycotoxinsbiology.organism_classificationCulture MediaMitochondriaFusarium subglutinansFood Science
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