Search results for "Electron microscope"
showing 10 items of 784 documents
Automated electron diffraction tomography – development and applications
2019
Electron diffraction tomography, a potential method for structure analysis of nanocrystals, and, in more detail, the strategies to use automated diffraction tomography (ADT) technique are described. Examples of ADT application are discussed according to the material class.
Effects of an innovative dipping treatment on the cold storage of minimally processed Annurca apples
2007
The effect of trehalose as an edible coating on minimally processed Annurca apple slices was studied during cold storage. The edible coating was prepared by dipping the fruit in a solution containing trehalose at 0.8%, sucrose at 1.0% and sodium chloride at 0.1%. During storage at 6 degrees C the following parameters were monitored: weight loss, colour (hue angle (h degrees) and whitening index (WI)), firmness, malic and ascorbic acids, polyphenol content.. microstructure by scanning electron microscopy (SEM) and microbial count. The results showed that such a coating reduced the browning phenomena; in fact the WI and h degrees values were significantly lower in coated samples than untreate…
Preparation and characterization of (Hg0.7Mo0.3)Sr2(Ca0.7Y0.3)Cu2Ox and (Hg0.9Re0.1)Ba2CaCu2Oy superconducting films by laser ablation
2000
Abstract Oriented (Hg 0.7 Mo 0.3 )Sr 2 (Ca 0.7 Y 0.3 )Cu 2 O x and (Hg 0.9 Re 0.1 )Ba 2 CaCu 2 O y superconducting films were prepared on SrTiO 3 substrates using laser ablation and post-Hg-vapor annealing. Due to the stability of Mo 0.3 Sr 2 (Ca 0.7 Y 0.3 )Cu 2 O x and Re 0.1 Ba 2 CaCu 2 O y in air, no special handling was needed during the grinding, mixing and pressing of the precursor targets. The superconductivity of the films was characterized with the temperature dependence of the ac susceptibility ( χ - T ) and the resistance ( R - T ) while the crystallography was probed with x-ray diffraction (XRD) and scanning electron microscopy (SEM).
Effect of film thickness on the transport properties of MgB2 synthesized by spray pyrolysis
2011
Abstract Polycrystalline MgB2 films of different thickness have been prepared by employing spray pyrolysis technique on MgO (1 0 0) substrate. The MgB2 and other phases have been confirmed using X-ray diffraction technique and no trace of impurities phases have been found. The resistivity behavior shows that the superconducting transition temperature lies in the range of 37–39 K with narrow transition width. The transport critical current density vary with films thickness and achieved highest value ∼1.2 × 106 A/cm2 at 20 K for 2.0 μm thick film and its values increase as thickness increases.
Microscopic studies of surface morphology of high temperature superconductor thick layers
2004
Abstract The surface morphology and structure of the YBa2Cu3O7−δ superconductor ayers prepared on passive ceramic and single crystal substrates is studied by electron microscopy. The layers reveal features of structure formation.
Quantum phase slips in superconducting Nb nanowire networks deposited on self-assembled Si templates
2012
Robust porous silicon substrates were employed for generating interconnected networks of superconducting ultrathin Nb nanowires. Scanning electron microscopy analysis was performed to investigate the morphology of the samples, which constitute of polycrystalline single wires with grain size of about 10 nm. The samples exhibit nonzero resistance over a broad temperature range below the critical temperature, fingerprint of phase slippage processes. The transport data are satisfactory reproduced by models describing both thermal and quantum fluctuations of the superconducting order parameter in thin homogeneous superconducting wires.
Comparison among superconducting models for β″-ET4[(H3O)Fe(C2O4)3]·C6H5Br single crystals by scanning tunnelling spectroscopy
2008
Single crystals of the novel superconductor beta ''-(BEDT-TTF)(4)[(H3O)Fe(C2O4)(3)]center dot C6H5Br charge-transfer salt were studied using a scanning tunnelling microscope. The measured samples have an onset critical temperature of about 4.0 K. Features often reported on similar compounds were observed in the tunnelling spectra at 1.4 K. STS spectra are compared with several models for the superconducting density of states. Our analysis evidences inhomogeneous superconductivity and indicates that the presence of a magnetic layer into the sample plays a role in determining the superconducting spectroscopic features. (C) 2008 Elsevier Masson SAS. All rights reserved.
Growth characteristics of sputter-deposited thin films
1996
Thin films of the heavy-fermion superconductor were deposited on various substrate materials in various orientations by means of a quasi-multilayer sputter process. Strongly (0001)-textured growth of the hexagonal compound was found for a uranium content in the range of 23% to 28% on sapphire and with perfect in-plane order on the latter substrate material. Atomic force microscopy and scanning electron microscopy revealed a Vollmer - Weber-like growth mode resulting in the development of large compressive strain in films on . As a result the electronic transport properties - in particular the temperature dependence of the resistivity - were strongly renormalized. Strong deviations from the …
Single-shot ultrafast laser processing of high-aspect-ratio nanochannels using elliptical Bessel beams
2017
Ultrafast lasers have revolutionized material processing, opening a wealth of new applications in many areas of science. A recent technology that allows the cleaving of transparent materials via non-ablative processes is based on focusing and translating a high-intensity laser beam within a material to induce a well-defined internal stress plane. This then enables material separation without debris generation. Here, we use a non-diffracting beam engineered to have a transverse elliptical spatial profile to generate high aspect ratio elliptical channels in glass of dimension 350 nm x 710 nm, and subsequent cleaved surface uniformity at the sub-micron level.
Measurement of magnetic fields and domain structures using a photoemission electron microscope
2000
Publisher Summary This chapter describes the theory and experiments on study of the domain structure of ferromagnets using various operation modes of a photoemission electron microscope (PEEM). The technique of PEEM allows observation of the domain boundaries on ferromagnetic surfaces arising from magnetic stray fields at definite conditions. In most cases, a very weak contrast due to the Lorentz force is formed. It can be measured by the use of digital methods of signal registration and data processing. From the form of the observed signal, conclusions about the shape of the stray field of the domain boundary can be drawn if there is additional information. The calculation of the image con…