Search results for "FLE"
showing 10 items of 3517 documents
Astronomical soft x-ray mirrors reflectivity enhancement by multilayer coatings with carbon overcoating
2004
A number of X-ray astronomical missions of near future will make use of hard X-ray optics with broad-band multilayer coatings. However multilayer mirrors can be also useful to enhance the effective area of a given X-ray telescope in the "classical" low energy X-ray band (0.1 – 10 keV), the window where X-ray spectroscopy provides very useful plasma diagnostics) with a consistent gain with respect to usual single-layer reflectors. Multilayers for soft X-rays are based on stacks with constant d-spacing (in order to minimize the loss due to the photoelectric effect). A further gain in reflectivity (however only restricted to the energy range between 0.5 and 4 keV) can be achieved by using a lo…
Broadband observations of the X-ray burster 4U1705-44 with Beppo SAX
2016
4U 1705-44 is one of the most-studied type I X-ray burster and Atoll sources. This source represents a perfect candidate to test different models proposed to self-consistently track the physical changes occurring between different spectral states because it shows clear spectral state transitions. The broadband coverage, the sensitivity and energy resolution of the BeppoSAX satellite offers the opportunity to disentangle the components that form the total X-ray spectrum and to study their changes according to the spectral state. Using two BeppoSAX observations carried out in August and October 2000, respectively, for a total effective exposure time of about 100 ks, we study the spectral evol…
Thin plastic foil X-ray optics with spiral geometry
2007
Winding a plastic foil ribbon into spiral cylinder or spiral cones we can design and build single or multiple reflection X-ray grazing incidence focusing optics with potential applications in Astronomy as well as experimental physics. The use of thin plastic foils from common industrial applications and of a mounting technique which does not require the construction of mandrels make these optics very cost effective. A spiral geometry focusing optic produces an annular image of a point source with the angular size of the annulus depending mainly on the pitch of the winding and the focal length. We use a ray-tracing code to evaluate the performances of cylindrical, and double conical spiral g…
Structural Characterization of Molecular Interface Layers Using Neutron and X-Ray Reflectivity Techniques
1992
Synthetic microstructures used in biological research today include a variety of different systems that serve very diverse purposes and require very different fabrication and characterization techniques. One class of microstructures that is at the boundary between life and materials sciences, and certainly has been associated closer to the latter in the past, is that of molecularly structured planar interface films. In fact, Langmuir-Blodgett (LB) films,1 i.e. molecularly layered films comprised of amphiphatic organic molecules on solid substrates, have been used for many years as model systems for the investigation of molecular interactions between chromophores or donor/ acceptor couples, …
Tracking the evolution of the accretion flow in MAXI J1820+070 during its hard state with the JED-SAD model
2021
X-ray binaries in outburst typically show two canonical X-ray spectral states, i.e. hard and soft states, in which the physical properties of the accretion flow and of the jet are known to change. Recently, the JED-SAD paradigm has been proposed for black hole X-ray binaries, aimed to address the accretion-ejection interplay in these systems. According to this model, the accretion flow is composed by an outer standard Shakura-Sunyaev disk (SAD) and an inner hot Jet Emitting Disk (JED). The JED produces both the hard X-ray emission, effectively playing the role of the hot corona, and the radio jets. In this paper, we use the JED-SAD model to describe the evolution of the accretion flow in th…
Mechanical characterization of TiO2 nanofibers produced by different electrospinning techniques
2015
Abstract In this work TiO2 nanofibers produced by needle and needleless electrospinning processes from the same precursor were characterized and compared using Raman spectroscopy, transmission electron microscopy (TEM), scanning electron microscopy (SEM) and in situ SEM nanomechanical testing. Phase composition, morphology, Young's modulus and bending strength values were found. Weibull statistics was used to evaluate and compare uniformity of mechanical properties of nanofibers produced by two different methods. It is shown that both methods yield nanofibers with very similar properties.
Determination at low ppm levels of dithiocarbamate residues in foodstuff by vapour phase-liquid phase microextraction-infrared spectroscopy
2010
Abstract A methodology based on the vapour phase (VP) generation of carbon disulphide from non-volatile dithiocarbamate compounds has been developed for determination of pesticide residues in foodstuff at low ppm levels. The method involves a selective reaction combined with liquid phase microextraction (LPME) and transmission infrared measurements. The use of a home made transmission cell improved the detection limits (LOD) compared to the use of attenuated total reflectance measurements by a factor of approximately 80. Using the most appropriate experimental conditions for the CS2 generation and LPME preconcentration, the precision of the methodology, expressed as the relative standard de…
Study on the initial stages of water corrosion of fluorozirconate glasses
2004
Abstract The surface corrosion process associated with the hydrolysis of fluorozirconate glass, ZBLAN (53ZrF 4 , 20BaF 2 , 20NaF, 4LaF 2 , 3AlF 3 ) was investigated using X-ray photoelectron spectroscopy (XPS), grazing-incidence small angle X-ray scattering (GISAXS), X-ray reflectivity (XRR) and scanning electron microscopy (SEM). After a short exposure period (25 min) of the glass surface to deionized water the XPS data indicate an increase of the oxygen content accompanied by a decrease of fluorine concentration. The analysis of the chemical bonding structure identified the predominant surface reaction products as zirconium hydroxyfluoride and oxyfluoride species. The second most abundant…
Self-Cleaning Bending Sensors Based on Semitransparent ZnO Nanostructured Films
2023
The design of multifunctional nanostructured materials is the key to the development of smart wearable devices. For instance, nanostructures endowed with both piezoelectric and photocatalytic activities could well be the workhorse for solar-light-driven self-cleaning wearable sensors. In this work, a simple strategy for the assembly of a flexible, semitransparent piezophotocatalytic system is demonstrated by leveraging rational wet chemistry synthesis of ZnO-based nanosheets/nanoflowers (NSs/NFs) under basic pH conditions onto flexible ITO/PET supports. A KMnO4 pretreatment before the ZnO synthesis (seeded ZnO) allows for the control of the density, size, and orientation of the NSs/NFs syst…
Discrimination of coral reflectance spectra in the Red Sea
2002
Benthic populations can potentially be mapped from remotely acquired spectral imagery, provided that they have distinctive reflectance signatures. We examined the spectral reflectance characteristics of 14 genera of Red Sea coral using a submersible spectroradiometer. Coral spectra varied quantitatively and qualitatively over the depth interval 5–20 m. Tissue pigment content had a larger effect on reflectance than colony morphology. Ten coral genera could be discriminated with a statistical probability of 52% on the basis of their absolute reflectance. Six groups of two to three coral genera could be discriminated with a probability of 60% on the basis of their rates of change in reflectanc…