Search results for "Hydrogen"

showing 10 items of 4254 documents

Crystal structure of bis(2-aminoanilinium) hydrogen phosphate

2016

In the title compound, the hydrogen phosphate anions are linked by O—H⋯O hydrogen bonds into chains parallel to [100]. The inorganic anionic chains and the organic cations are linked by N—H⋯O and N—H⋯N hydrogen bonds, forming a two-dimensional supra­molecular network extending parallel to (001).

crystal structure2-aminoaniliniumChemistryHydrogen bondInorganic chemistryGeneral ChemistryCrystal structure010402 general chemistry010403 inorganic & nuclear chemistryCondensed Matter PhysicsHydrogen phosphate2-amino­anilinium01 natural sciencesResearch Communications0104 chemical scienceslcsh:ChemistryCrystalCrystallographylcsh:QD1-999hydrogen bondssupra­molecular networkGeneral Materials Sciencehydrogen phosphatesupramolecular networkActa Crystallographica Section E Crystallographic Communications
researchProduct

2-[4-(Di­methyl­amino)­phen­yl]-3,3-di­fluoro-3H-naphtho­[1,2-e][1,3,2]oxaza­borinin-2-ium-3-uide

2017

In the title compound, C19H17BF2N2O, a twist about the N—C single bond is observed, making the cross conjugation not as efficient as in the case of a planar structure. The borone complex has tetrahedral geometry. In the crystal, molecules are conected by weak C—H...F hydrogen bonds.

crystal structureBODIPY dyes010405 organic chemistryChemistryHydrogen bondCrystal structure010403 inorganic & nuclear chemistry01 natural sciences0104 chemical sciencesCrystalCrystallographyflurophoreslcsh:QD901-999Single bondCross-conjugationlcsh:CrystallographyIUCrData / International Union of Crystallography
researchProduct

catena-Poly[[diaquabis[1,4-bis(pyridin-4-yl)buta-1,3-diyne-κN]iron(II)]-μ-cyanido-κ2N:C-[dicyanido-κ2C-platinum(II)]-μ-cyanido-κ2C:N]

2017

The molecular structure of the title compound, [FePt(CN)4(C14H8N2)2(H2O)2]n, consists of one-dimensional polymeric [–Fe–NC–Pt(CN)2–CN–]∞chains. Two water molecules and two monodentate 1,4-bis(pyridin-4-yl)buta-1,3-diyne (bpb) ligand molecules complete the octahedral coordination sphere of the FeIIatoms. The Fe—N(py) bond length (py is pyridine) is 2.2700 (15) Å, Fe—N(cyanide) is 2.1185 (16) Å and the Fe—O distance is 2.1275 (14) Å. The water molecules are hydrogen bonded to either bpb ligands or cyanide groups of the planar [Pt(CN)4]2−anion of adjacent polymeric chains. These O—H...N hydrogen bonds, in conjunction with offset and tilted π–π stacking interactions between bpb ligands and cyan…

crystal structureCoordination sphereDenticityLigandHydrogen bondStereochemistryCyanideCrystal structurebitopic bpb ligandhydrogen bonding010402 general chemistry010403 inorganic & nuclear chemistry01 natural sciencesMedicinal chemistry0104 chemical sciencesBond lengthchemistry.chemical_compoundchemistryπ–π stacking interactionsPyridinelcsh:QD901-999lcsh:CrystallographyIUCrData
researchProduct

Crystal structure, Hirshfeld surface analysis and DFT studies of (E)-1-(4-bromophenyl)-3-(3-fluorophenyl)prop-2-en-1-one

2018

The title halogenated organic chalcone was prepared by a Claisen–Schmidt condensation reaction. A Hirshfeld surface analysis was carried out to reveal the percentage contributions of the inter­molecular inter­actions. A theoretical study was performed using the density functional theory (DFT) at B3LYP with the 6–311 G++(d,p) basis set level to compare with the experimental results of the X-ray analysis and UV–vis absorption analysis in term of the geometrical parameters, HOMO-LUMO energy gap and charge distributions.

crystal structureCrystal structure010402 general chemistry010403 inorganic & nuclear chemistryDFT01 natural sciencesResearch Communicationslcsh:ChemistryCrystalHOMO–LUMOmolecular electrostatic potentialNucleophileGeneral Materials ScienceHOMO/LUMOBasis setmol­ecular electrostatic potentialUV–visHydrogen bondChemistryHirshfeld surfaceGeneral ChemistryCondensed Matter Physics0104 chemical sciencesCrystallographylcsh:QD1-999Electrophilehalogen chalconeDensity functional theoryActa Crystallographica Section E Crystallographic Communications
researchProduct

Crystal structure, Hirshfeld surface analysis and electrostatic potential study of naturally occurring cassane-type diterpenoid Pulcherrimin C monohy…

2019

Single crystal X-ray diffraction analysis and Hirshfeld surface analysis of the title compound were carried out to analyse qu­anti­tatively the inter­molecular inter­actions involved in the crystal packing. The electrostatic potential surface was generated over the Hirshfeld surface to visualize the potential active sites.

crystal structureCrystal structurecassane-type diterpenoids010402 general chemistry010403 inorganic & nuclear chemistryRing (chemistry)01 natural sciencesResearch Communicationslcsh:ChemistryCrystalchemistry.chemical_compoundFuranHirshfeld surface analysisGeneral Materials SciencebiologyHydrogen bondGeneral ChemistryCondensed Matter PhysicsCaesalpinia pulcherrimabiology.organism_classificationTerpenoid0104 chemical sciencesCaesalpinia pulcherrimapulcherrimin CCrystallographyelectrostatic potentiallcsh:QD1-999chemistryActa Crystallographica Section E Crystallographic Communications
researchProduct

Crystal structure of 2-{[1-(2-methyl-5-nitro-1H-imidazol-1-yl)propan-2-yloxy]carbonyl}benzoic acid

2014

In the title compound, C15H15N3O6, the dihedral angle between the planes of the benzene and imidazole rings is 34.93 (10)°. An intramolecular C—H...O hydrogen bond is observed. In the crystal, O—H...N hydrogen bonds link the molecules into chains parallel to thecaxis.

crystal structureCrystal structurepharmaceuticalsDihedral angleBioinformaticsMedicinal chemistrynitro­imidazolesCrystalchemistry.chemical_compoundImidazoleGeneral Materials SciencePhysics::Chemical PhysicsO—H⋯N hydrogen bondsBenzeneBenzoic acidQuantitative Biology::BiomoleculesnitroimidazolesCrystallographyHydrogen bondGeneral ChemistryCondensed Matter PhysicsData ReportsO—H...N hydrogen bondschemistryQD901-999NitroActa Crystallographica Section E Structure Reports Online
researchProduct

Crystal structure ofS-octyl (E)-3-(4-methoxybenzylidene)dithiocarbazate

2015

As already observed in similar molecules, the dithiocarbazate group in the title compound, C17H26N2OS2, adopts anEEconfiguration with respect to the C=N bond of the benzylidene moiety. In the crystal, molecules are connected into inversion dimers by pairs of N—H...S hydrogen bonds. The dimers are linked by weak π–π interactions, with centroid-to-centroid distances of 3.723 (11) Å, forming chains parallel to [110].

crystal structureCrystallographyChemistryHydrogen bonddithiocarbazateThio-General ChemistryCrystal structurehydrogen bondingCondensed Matter PhysicsData ReportsCrystalCrystallographyQD901-999S-containing Schiff basesdi­thio­carbazateMoietyGeneral Materials ScienceActa Crystallographica Section E Crystallographic Communications
researchProduct

Crystal structure of tricarbon­yl(N-di­phenyl­phosphanyl-N,N′-diisopropyl-P-phenyl­phospho­nous di­amide-κ2 P,P′)cobalt(I) tetra­carbonyl­cobaltate(−…

2014

The title compound {Co(CO)3[Ph2PN(i-Pr)P(Ph)N(H)i-Pr]}[Co(CO)4] is an ionic species consisting of a Co(CO)3[Ph2PN(i-Pr)P(Ph)N(H)i-Pr] cation and a [Co(CO)4] anion.

crystal structureCrystallographyChemistryHydrogen bondmetallacycleTricarbonchemistry.chemical_elementGeneral ChemistryCrystal structureMetallacycleCondensed Matter PhysicsTolueneMedicinal chemistrycobaltResearch Communicationsphosphine ligandchemistry.chemical_compoundQD901-999AmideGeneral Materials ScienceCobaltCoordination geometryActa Crystallographica Section E: Structure Reports Online
researchProduct

Crystal structure and Hirshfeld surface analysis of dimethyl (1R*, 3aS*, 3a(1)R*, 6aS*, 9R*, 9aS*)-3a(1),5,6,9a-tetrahydro-1H,4H,9H-1,3a:6a,9-diepoxy…

2019

The title diepoxyphenalene derivative, C17H18O6, comprises a fused cyclic system containing four five-membered rings (two dihydrofuran and two tetrahydrofuran) and one six-membered ring (cyclohexane). The five-membered dihydrofuran and tetrahydrofuran rings adopt envelope conformations, and the six-membered cyclohexane ring adopts a distorted chair conformation. Two methyl carboxylate groups occupy adjacent positions (2- and 3-) on a tetrahydrofuran ring. In the crystal, two pairs of C-H center dot center dot center dot O hydrogen bonds link the molecules to form inversion dimers, enclosing two R-2(2)(6) ring motifs, that stack along the a-axis direction and are arranged in layers parallel …

crystal structureCrystallographyC—H...O hydrogen bondsQD901-999fused hexacyclic systemHirshfeld surface analysisdiepoxyphenalene
researchProduct

Influences of Chemical Functionalities on Crystal Structures and Electrochemical Properties of Dihydro-benzoxazine Dimer Derivatives

2021

Dihydro-1,3,2H-benzoxazine dimer derivatives or dihydro-benzoxazine dimers are a class of compounds typically prepared by ring-opening reactions between dihydro-benzoxazines and phenols. Dihydro-benzoxazine dimers act as chelating agents for several transition and rare-earth cations. To better understand the chelating properties, it is necessary to examine their structural features and electrochemical characteristics thoroughly. However, the electrochemical properties of dihydro-benzoxazine dimers have not been tremendously examined. Herein, eight derivatives of dihydro-benzoxazine dimers possessing different substituents on the benzene ring and the tertiary-amine nitrogen were synthesized …

crystal structureCrystallographyHydrogen bondGeneral Chemical EngineeringDimerHirshfeld surfaceIntermolecular forceCrystal structureCondensed Matter PhysicsRedoxInorganic ChemistryCrystalelectrochemical propertychemistry.chemical_compoundCrystallographychemistryQD901-999General Materials SciencebenzoxazineCyclic voltammetryMethyleneCrystals
researchProduct