Search results for "IDENTIFICATION"
showing 10 items of 1600 documents
Observation of s-Channel Production of Single Top Quarks at the Tevatron
2014
We report the first observation of single-top-quark production in the s channel through the combination of the CDF and D0 measurements of the cross section in proton-antiproton collisions at a center-of-mass energy of 1.96 TeV. The data correspond to total integrated luminosities of up to 9.7fb-1 per experiment. The measured cross section is σs=1.29-0.24+0.26pb. The probability of observing a statistical fluctuation of the background to a cross section of the observed size or larger is 1.8×10-10, corresponding to a significance of 6.3 standard deviations for the presence of an s-channel contribution to the production of single-top quarks. © 2014 American Physical Society.
Investigation of biocenosis in a archaeological rock-cut settlements with relevant historic-artistic evidences. A case study in South-east of Sicily.
2011
Pharmacophore modelling as useful tool in the lead compounds identification and optimization
2012
The goal of computer-aided molecular design methods in modern medicinal chemistry is to reduce the overall cost and time associated to the discovery and development of a new drug by identifying the most promising candidates to focus the experimental efforts on. Very often, many drug discovery projects have reached already a well-advanced stage before detailed structural data on the protein target have become available. A possible consequence is that often, medicinal chemists develop novel compounds for a target using preliminary structure–activity information, together with the theoretical models of interactions. Only responses that are consistent with the working hypothesis contribute to a…
Resource or waste? A perspective of plastics degradation in soil with a focus on end-of-life options.
2018
‘Capable-of-being-shaped’ synthetic compounds are prevailing today over horn, bone, leather, wood, stone, metal, glass, or ceramic in products that were previously left to natural materials. Plastic is, in fact, economical, simple, adaptable, and waterproof. Also, it is durable and resilient to natural degradation (although microbial species capable of degrading plastics do exist). In becoming a waste, plastic accumulation adversely affects ecosystems. The majority of plastic debris pollutes waters, accumulating in oceans. And, the behaviour and the quantity of plastic, which has become waste, are rather well documented in the water, in fact. This review collects existing information on pla…
Synthesis and structural characterisation of germanium(II) halide complexes with neutral N-donor ligands.
2010
The Ge(II) complexes [GeX(2)(L-L)] (L-L = 1,10-phen (X = Cl, Br); L-L = Me(2)N(CH(2))(2)NMe(2), 2,2'-bipy (X = Cl)), [GeX(L-L)][GeX(3)] (L-L = 2,2'-bipy (X = Br); L-L = pmdta (MeN(CH(2)CH(2)NMe(2))(2)) (X = Cl, Br)) have been prepared and their crystal structures determined. The crystal structure of [GeCl(2){Me(2)N(CH(2))(2)NMe(2)}] shows a weakly associated centrosymmetric dimer based upon distorted square-pyramidal coordination at Ge(II) and containing asymmetrically chelating diamine ligands. The structure of [GeCl(2)(2,2'-bipy)] contains a chelating 2,2'-bipy ligand and forms a zig-zag chain polymer via long-range intermolecular Ge...Cl bridging interactions, leading to a very distorted…
Automated multi-dimensional liquid chromatography
2004
A comprehensive on-line sample clean-up with an integrated two-dimensional HPLC system was developed for the analysis of natural peptides. Samples comprised of endogenous peptides with molecular weights up to 20 kDa were generated from human hemofiltrate (HF) obtained from patients with chronic renal failure. The (poly-)peptides were separated using novel silica-based restricted access materials with strong cation-exchange functionalities (SCX-RAM). The size-selective sample fractionation step is followed by cation-exchange chromatography as the first dimension. The subsequent second dimension of separation is based on hydrophobic interaction using four parallel short reversed-phase (RP) co…
The Contribution of Microchemical Analyses and Diagnostic Imaging to the Conservation and Identification of the Degraded Surfaces of Hellenistic-Roma…
2020
The Archaeological Museum of Palermo (Sicily) has recently presented the results of the restoration of three wall paintings from the House of the Masks of Solunto archaeological site. These significant paintings, dating back to the first century BCE, are the most significant examples of Pompeian style discovered in Sicily to date. The cycle of frescoes unearthed is the best preserved and most complete example of wall painting dating to the Republican Roman period in Sicily. This house was a luxurious private residence built on two floors and centred around a peristyle. This fresco cycle embellished the walls of a banquet room (oecus) discovered during an archaeological excavation carried ou…
Multitechnique diagnostic analysis and 3D surveying prior to the restoration of St. Michael defeating Evil painting by Mattia Preti
2021
In this study, a multimethodological analysis involving optical and physical/chemical diagnostic techniques and 3D photogrammetric survey was successfully applied, for the first time, on the large oil on canvas St. Michael defeating Evil painting by Mattia Preti, located inside the Church of the Immaculate Conception of Sarria (Floriana) in Malta. Pigmenting agents, binder media, and raw materials were first characterized, both at elemental and molecular scales, through X-ray fluorescence spectroscopy (XRF), optical stereo microscopy (SM), scanning electron microscopy coupled with energy dispersive X-ray spectroscopy (SEM-EDX), Fourier transform infrared spectroscopy (FT-IR), and gas chroma…
A Numerical Method for an Inverse Problem Arising in Two-Phase Fluid Flow Transport Through a Homogeneous Porous Medium
2019
In this paper we study the inverse problem arising in the model describing the transport of two-phase flow in porous media. We consider some physical assumptions so that the mathematical model (direct problem) is an initial boundary value problem for a parabolic degenerate equation. In the inverse problem we want to determine the coefficients (flux and diffusion functions) of the equation from a set of experimental data for the recovery response. We formulate the inverse problem as a minimization of a suitable cost function and we derive its numerical gradient by means of the sensitivity equation method. We start with the discrete formulation and, assuming that the direct problem is discret…
A linear approach for the nonlinear distributed parameter identification problem
1991
In identifying the nonlinear distributed parameters we propose an approach, which enables us to identify the nonlinear distributed parameters by just solving linear problems. In this approach we just need to identify linear parameters and then recover the nonlinear parameters from the identified linear parameters. An error estimate for the finite element approximation is derived. Numerical tests are also presented.