Search results for "Indentation"
showing 10 items of 178 documents
Linking structure and nanomechanical properties via instrumented nanoindentations on well-defined and fine-tuned morphology poly(ethylene)
2009
Several poly(ethylene) samples with a broad range of morphologies were studied in this work using nanoindentations. The samples had degrees of crystallinity ranging from 30 to 100% while their Young's modulus ranged from few tens of MPa up to several GPa. Experimental conditions for the correct evaluation of Young's modulus were at first identified, choosing a suitable loading rate in order to minimize viscoelastic effects on the unloading. The force curves, i.e., plots of applied load vs. penetration depth, were then analyzed following two common procedures available in the literature. None of these procedures leads to satisfying results when compared to other experimental techniques. Howe…
Role of thermal history on quiescent cold crystallization of PET
2002
8 pags., 9 figs.
Self-Healing Properties of Bioinspired Amorphous CaCO3/Polyphosphate-Supplemented Cement
2020
There is a strong interest in cement additives that are able to prevent or mitigate the adverse effects of cracks in concrete that cause corrosion of the reinforcement. Inorganic polyphosphate (polyP), a natural polymer that is synthesized by bacteria, even those on cement/concrete, can increase the resistance of concrete to progressive damage from micro-cracking. Here we use a novel bioinspired strategy based on polyP-stabilized amorphous calcium carbonate (ACC) to give this material self-healing properties. Portland cement was supplemented with ACC nanoparticles which were stabilized with 10% (w/w) Na&ndash
Effect of pre-heating on the mechanical properties of silorane-based and methacrylate-based composites
2016
Background The use of composites in dental restoration has been commonly criticized, due to their underwhelming mechanical properties. This problem may be solved partially by preheating. The present research aims to determine the effect of preheating on the mechanical properties of two different classes of composites. Material and methods A Silorane-based (Silorane) and a Methacrylate-based (Z250) composite were preheated to different temperatures (25, 37, and 68 °C) and afterwards were tested with the appropriate devices for each testing protocol. The material's flexural strength, elastic modulus, and Vickers microhardness were evaluated. Two-way ANOVA, and Tukey's post hoc were used to an…
Light transmittance of zirconia as a function of thickness and microhardness of resin cements under different thicknesses of zirconia
2012
Objective: The objective of this study was to compare microhardness of resin cements under different thicknesses of zirconia and the light transmittance of zirconia as a function of thickness. Study design: A total of 126 disc-shaped specimens (2 mm in height and 5 mm in diameter) were prepared from dual-cured resin cements (RelyX Unicem, Panavia F and Clearfil SA cement). Photoactivation was performed by using quartz tungsten halogen and light emitting diode light curing units under different thicknesses of zirconia. Then the specimens (n=7/per group) were stored in dry conditions in total dark at 37°C for 24 h. The Vicker's hardness test was performed on the resin cement layer with a micr…
Microhardness of different resin cement shades inside the root canal
2012
Objectives: To compare microhardness along the root canal post space of two resin cements in different shades and a dual-cure resin core material. Study Design: Root canals of 21 bovine incisors were prepared for post space. Translucent posts (X•Post, Dentsply DeTrey) were luted using one the following resin luting agent: Calibra (Dentsply DeTrey) in Translucent, Medium and Opaque shades, RelyX Unicem (3M ESPE) in Translucent, A2 and A3 shades and the dual-cure resin core material Core•X flow. All materials were applied according to manufacturers’ instructions and were all photopolymerized (Bluephase LED unit, Ivoclar Vivadent, 40s). After 24 hours, roots were transversally cut into 9 slice…
Effects of three different bleaching agents on microhardness and roughness of composite sample surfaces finished with different polishing techniques
2017
BACKGROUND The aim of this study was to evaluate effects of different polishing methods and whitening agents on surface hardness and roughness of nano-hybrid composite resin. MATERIAL AND METHODS In total, one hundred twenty disc-shaped specimens were prepared to nano-hybrid composite (Charisma Diamond). 60 samples were used for microhardness measurements and the others were used for the evaluation of surface roughness. Samples were divided randomly into two subgroups (n = 30 each). In first group a low-viscosity liquid polishing agent (Biscover LV) was applied. In the second group, nothing was applied. All the samples were stored in distilled water at 37°C for 24 h. After initial measureme…
Influence of different thermopolymerization methods on composite resin microhardness
2020
Background Additional heat polymerization in composite resins allows greater effectiveness of microhardness, flexural strength, fracture toughness, wear resistance, and increased color stability. Material and Methods 150 composite resin specimens were made using a 4 mm diameter and 2 mm thick bipartite steel matrix. Five resins composed of different compositions were tested (Brilliant Everglow/Coltene, Filtek One BulkFill/3M, Filtek P60/3M, Filtek Z350XT/3M, Filtek Z250XT/3M), and for each of them three types of polymerization were tested: light curing only (n=50); photopolymerization + autoclave thermopolymerization (n=50) and photopolymerization + microwave thermopolymerization (n=50). …
Effect of wetting agent coverage on the surface properties of resin composite submitted to brushing and staining cycles
2020
Background Wetting agents facilitate the composites handling, acting as a lubricant and decreasing their stickness to spatula. The effects of these materials on the properties of composites are not completely clear. This study aimed to evaluate Gloss, Color, Roughness and Microhardness of a composite (Filtek Z250 XT, 3M Oral Care) covered by a wetting agent (Modeling Resin, Bisco), submitted to brushing and staining cycles with red wine. Material and Methods Cylinder-shaped samples (8 mm ø x 2 mm height) were divided into 4 groups, according to application of wetting agent and brushing cycles (n = 20). The composite was placed in the orifice of a polytetrafluoroethylene mold, received wetti…
Evaluation of microhardness, sorption, solubility, and color stability of bulk fill resins : a comparative study
2020
Background Due to the increasing popularity of bulk fill resins, there is a concern that their components can be leached; this is because these are inserted in a single 4-5 mm increment. This in vitro study evaluated the microhardness, sorption, solubility, and color stability of three restorative bulk fill resins, namely: Filtek Bulk Fill (FBF), Tetric N-Ceram Bulk Fill (TNC), and Opus Bulk Fill (OBF). Material and Methods Cylindrical samples were fabricated to be 15 mm in diameter and 1 mm thick (n = 10). For the microhardness test, three random indentations were formulated on the samples using a micro-durometer with a load of 300 gf for 15 s. Sorption and solubility were then evaluated (…