Search results for "Metallurgy"
showing 10 items of 1419 documents
Automatic Secondary Cooling Control for the Continuous Casting Process of Steel
1991
Two simulation models for finding the optimal secondary cooling strategy in continuous casting process are presented. The first one is a two-dimensional off-line model for optimizing steady state casting operation. The second one is a one-dimensional model which can be used for simulating casting operation in real-time during varying casting conditions.
Metal/Semiconductor Barrier Properties of Non-Recessed Ti/Al/Ti and Ta/Al/Ta Ohmic Contacts on AlGaN/GaN Heterostructures
2019
This paper compares the metal/semiconductor barrier height properties of non-recessed Ti/Al/Ti and Ta/Al/Ta contacts on AlGaN/GaN heterostructures. Both contacts exhibited a rectifying behavior after deposition and after annealing at temperatures up to 550 °
Controlling melt convection—an innovation potential for concerted microstructure evolution of Nd-Fe-B alloys
2005
The solidification process and the resulting microstructure of Nd-Fe-B alloys in consideration of melt convection has been investigated experimentally with a specially designed forced crucible rotation technique. Samples were subjected to well-defined forced rotation and vibration, respectively, during induction heating and solidification. A concerted microstructure evolution is possible by enhancement or suppression of the melt convection. As a result, the microstructure pattern, mainly the volume fraction of the soft magnetic a-Fe phase, vary strongly with the strength of the internal flow motion. A distinct reduction of the a-Fe volume fraction in samples with strong melt rotation was ob…
Magnetic field controlled FZ single crystal growth of intermetallic compounds
2005
Abstract Intermetallic rare-earth-transition-metal compounds with their coexistence of magnetic ordering and superconductivity are still of great scientific interest. The crystal growth of bulk single crystals is very often unsuccessful due to an unfavorable solid–liquid interface geometry enclosing concave fringes. The aim of the work is the contactless control of heat and material transport during floating-zone single crystal growth of intermetallic compounds. This control is provided by a tailored design of the electromagnetic field and the resulting electromagnetically driven convection. Numerical simulations for the determination of the electromagnetic field configuration induced by th…
Influence on the macrosegregation of binary metallic alloys by thermoelectromagnetic convection and electromagnetic stirring combination
2014
International audience; Influence of a slowly rotating 0.5 T transverse magnetic field on the directionally solidified metallic alloy has been experimentally studied in this work. Main idea is to study an influence on the melt flow and material structure caused by the simultaneous electromagnetic stirring and thermoelectromagnetic convection with comparable magnitudes. Electromagnetic stirring and thermoelectromagnetic convection intensities have been estimated analytically to find optimal experimental parameters. It is experimentally demonstrated that with such an interaction it is possible to modify component macrosegregation of Sn-10 wt% Pb alloy. Helical macrosegregation within cylindri…
Effect of current on the sintering of pre-oxidized copper powders by SPS
2017
Abstract As mentioned in the literature, SPS (Spark Plasma Sintering) technology combines uniaxial charge and pulsed currents to achieve the rapid sintering of powders. Although the utilization of current is often reported, an understanding of its role in the sintering mechanisms is still a subject of controversy. In fact, the oxide layer around metal particles is sometimes considered to be a dielectric gap in which discharges may occur: these discharges can clean the surface of particles and enhance densification. In this paper, an oxide layer was grown on the particle surface of a copper powder, and the growth enabled the study of the role of current on such dielectric layers. The powders…
Phase and structural transformations in annealed copper coatings in relation to oxide whisker growth
2015
Abstract We describe structural and phase transformation in copper coatings made of microparticles during heating and annealing in air in the temperature range up to 400 °C. Such thermal treatment is accompanied by intensive CuO nanowhisker growth on the coating surface and the formation of the layered oxide phases (Cu 2 O and CuO) in the coating interior. X-ray diffraction and focused ion beam (FIB) are employed to characterize the multilayer structure of annealed copper coatings. Formation of volumetric defects such as voids and cracks in the coating is demonstrated.
Grafting and characterization of dodecylphosphonic acid on copper: Macro-tribological behavior and surface properties
2013
International audience; Thin film of n-dodecylphosphonic acid (DDPA) was prepared on a copper oxide substrate via a molecular self-assembly process. The composition, structure, organization, surface energy, morphology, and electrochemical behavior of the DDPA filmwere characterized bymeans of X-ray photoelectron spectroscopic analysis (XPS), polarization modulation infrared reflection absorption spectroscopy (PM-IRRAS), contact angle measurement v(CAM), microscopic observations, and electrochemistry. The friction behavior of the DDPA film adsorbed on copper oxide substrate sliding against a Si3N4 ball was examined on a linear reciprocating tribological tester. Worn surfaces of the DDPA film…
The influence of hydrogen on the electrochemical properties of selected types of stainless steel=Wpływ wodoru na właściwości elektrochemiczne wybrany…
2013
Abstract The paper presents the results of the influence of electrolytic hydrogenation on the change of electrochemical properties of selected stainless steels and their susceptibility to the formation of galvanic hydrogen. It has been shown that the electrolytic hydrogenation of steel X5CrNi18-10 and X6Cr17 in the state of delivery, not only changes their corrosion resistance, but also contributes to the formation of galvanic hydrogen cells.
On-line Mössbauer measurements at low temperatures of 83mKr implanted into Al
1978
Abstract A vacuum ion implantation chamber housing a helium flow cryostat and a Mossbauer transducer has been constructed and coupled directly to an ion separator for low temperature implantation and on-line Mossbauer measurements. 83m Kr, produced by thermal neutron activation of enriched 82 Kr gas, has been implanted into Al foils in the temperature range 15–300 K. Annealing effects and the temperature dependence of the Lamb-Mossbauer factor have been studied by Mossbauer measurements (at 15–35 K) using the implanted Al targets as sources and Kr/hydrochinone as absorber.