Search results for "Monochromator"
showing 10 items of 14 documents
New fine structures resolved at the ELNES Ti-L2,3 edge spectra of anatase and rutile: comparison between experiment and calculation.
2010
Abstract Anatase and rutile Ti- L 2,3 edge spectra were measured in electron energy loss spectroscopy (EELS) using a transmission electron microscope (TEM) coupled to a CEOS Cs-probe corrector, an omega-type monochromator and an in-column omega-type energy filter fully corrected for 2nd order aberrations. Thanks to the high energy resolution, high electron probe current and high stability achieved under this instrumental configuration, new fine structures, never reported before, were resolved at the L 3 band of both rutile and anatase. The data suggest that new peaks also exist in the L 2 e g band. The experimental spectra are compared with multichannel multiple scattering (MMS) calculation…
Influence of clouds on the spectral actinic flux density in the lower troposphere (INSPECTRO): overview of the field campaigns
2008
Ultraviolet radiation is the key factor driving tropospheric photochemistry. It is strongly modulated by clouds and aerosols. A quantitative understanding of the radiation field and its effect on photochemistry is thus only possible with a detailed knowledge of the interaction between clouds and radiation. The overall objective of the project INSPECTRO was the characterization of the three-dimensional actinic radiation field under cloudy conditions. This was achieved during two measurement campaigns in Norfolk (East Anglia, UK) and Lower Bavaria (Germany) combining space-based, aircraft and ground-based measurements as well as simulations with the one-dimensional radiation transfer model UV…
Comparison of LIBS and micro-XRF measurements on bronze alloys for monitoring plasma effects
2011
The laser-induced breakdown spectroscopy (LIBS) technique is often used as atomic spectroscopic technique for elemental analysis of materials. However, it presents some drawbacks that make an accurate quantitative analysis difficult. Since the plasma properties, such as spatial inhomogeneity and plume stoichiometry strongly depend on the experimental conditions, the measurements are less reproducible. In order to evaluate the measurement fluctuations, we propose to use the more established micro X-Ray fluorescence (μ-XRF) technique for validating LIBS data. In particular, the quantitative data, obtained by varying the laser fluence, the shot numbers and the temporal acquisition parameters, …
ECRIS plasma spectroscopy with a high resolution spectrometer
2020
Electron Cyclotron Resonance Ion Source (ECRIS) plasmas contain high-energy electrons and highly charged ions implying that only noninvasive methods such as optical emission spectroscopy are reliable in their characterization. A high-resolution spectrometer (10 pm FWHM at 632 nm) enabling the detection of weak emission lines has been developed at University of Jyväskylä, Department of Physics (JYFL) for this purpose. Diagnostics results probing the densities of ions, neutral atoms, and the temperature of the cold electron population in the JYFL 14 GHz ECRIS are described. For example, it has been observed that the cold electron temperature drops from 40 eV to 20 eV when the extraction volta…
Transition radiation in the x-ray region from a low emittance 855 MeV electron beam
1997
A quasi-monochromatic hard x-ray beam with a photon energy of 33 keV has been produced from transition radiation (TR) at the Mainz Microtron MAMI. The radiator was a stack of 30 polyimide foils of 25 μm thickness and 75 μm separation and the monochromator a highly-oriented pyrolytic graphite crystal. The intrinsic bandwidth was measured with a critical absorption technique to be 100 eV. On the basis of these experiments a photon flux of 4⋅109/mm2s over an illuminated area of 5.7×125 mm2 can be expected from an optimized beryllium radiator at a beam current of 100 μA. At the K-absorption edge of titanium at 5 keV narrow band transition radiation has been observed from a stack of four foils o…
Performance and characterization of the FinEstBeAMS beamline at the MAX IV Laboratory
2021
European Regional Development Fund (grant No. TK-141 HiTechDevices 2014-2020.4.01.15-0011 to University of Tartu; grant No. MAX-TEENUS 2014-2020.4.01.20-0278 to University of Tartu; grant No. Eesti Kiirekanal SLOFY11156T/1 to University of Tartu); Estonian Research Council (grant No. PRG-629 to University of Tartu); Jane & Aatos Erkko Foundation (grant No. SOFUS); Business Finland (grant No. 1464/31/2019); Academy of Finland (grant No. 319042; grant No. 326461; grant No. 326406; grant No. 320165); University of Oulu; University of Turku; Tampere University; University of Tartu.
Advanced Hardware and Software for the Upgrade of Mirror/Prisma Monochromator SPM-2 (Carl Zeiss Jena) for the Measurements of Basic Spectroscopic Pro…
2021
Today's digital electronics and fast computers allow the efficiently processing of large volumes of spectroscopic information, which means the opportunity to reuse and upgrade monochromator with sophisticated optical and mechanical systems being designed and used in the middle of the last century. Particular interest is towards high-resolution prism monochromator. We used such an approach to computerize manual operations of universal mirror monochromator SPM-2, which has changeable quartz, glass, NaCl and KBr crystal prisms. SPM-2 was produced by VEB Carl Zeiss JENA in the early sixties of the last century (in former GDR), and its advanced features were widely used [1]. The current interest…
Study and implementation of a soft X-ray 100 eV -20 keV fixed exit monochromator system
2006
We describe a “built in house” X-ray monochromator which produces a fixed exit X-ray beam tunable in the full energy range 0.1 - 20 keV. The system is based on a double diffraction on two large size parallel crystals positioned using a remotely controlled micropositioning system in order to keep the position of the monochromatic beam for any chosen energy. Up to six different diffracting elements can be selected without breaking the vacuum. This allows to cover the full energy range of interest. The system is part of an upgrading project of the XACT facility at the Istituto Nazionale di Astrofisica - Osservatorio Astronomico di Palermo G.S. Vaiana, and will be employed for the testing and c…
Novel optical interferometry of synchrotron radiation for absolute electron beam energy measurements
2018
Abstract A novel interferometric method is presented for the measurement of the absolute energy of electron beams. In the year 2016, a pioneering experiment was performed using a 195 MeV beam of the Mainz Microtron (MAMI). The experimental setup consisted of two collinear magnetic undulators as sources of coherent optical synchrotron light and a high-resolving grating monochromator. Beam energy measurements required the variation of the relative undulator distance in the decimeter range and the analysis of the intensity oscillation length in the interference spectrum. A statistical precision of 1 keV was achieved in 1 h of data taking, while systematic uncertainties of 700 keV were present …
Ageing studies of TPB in noble gas detectors for dark matter and neutrinoless ββ decay searches
2017
Noble gases (Xe, Ar, Kr) are very attractive as detector media in Dark Matter search and neutrinoless double-beta decay experiments. However, the detection of their scintillation light (in the VUV spectral region) requires shifting the VUV light to visible light, where standard photosensors are more efficient. Tetraphenyl butadiene (TPB) is widely used as wavelength shifter, absorbing the VUV light and re-emitting in the blue region (~430nm). TPB is an organic molecule that may degrade due to exposure to environmental agents and also to ultraviolet light. In this work, we present TPB ageing studies due to exposure to VUV light, aiming at quantifying the reduction of the absolute fluorescenc…