Search results for "PERFORMANCE"
showing 10 items of 4457 documents
Occurrence and risk assessment of mycotoxins, acrylamide, and furan in Latvian beer.
2018
This work reports data on the occurrence of nine mycotoxins and two food processing contaminants - acrylamide and furan - in a total of 100 beers produced in Latvia. Mycotoxins were detected by high-performance liquid chromatography (HPLC) coupled with time-of-flight mass spectrometry, acrylamide by HPLC coupled with quadrupole-Orbitrap mass spectrometry, and furan by headspace gas chromatography-mass spectrometry. The most frequently occurring mycotoxins were HT-2 and deoxynivalenol (DON), which were detected in 52% and 51% of the analysed samples. The highest content was observed for DON, reaching the maximum of 248 µg kg-1. Furan was ubiquitous, and 74% of the samples contained acrylamid…
Determination of alcohols in essential oils by liquid chromatography with ultraviolet detection after chromogenic derivatization
2013
Abstract An HPLC-UV method to determine compounds having a hydroxyl functional group in plant essential oils is developed. The sample is diluted with 1,4-dioxane and the analytes are derivatized with phthalic anhydride. The derivatives (phthalates hemiesters) are separated on a C8 column using an acetonitrile (ACN)/water gradient. Separation conditions were optimized using the DryLab® method development software. For the alcohols and phenols present in mint and rose essential oils, optimization led to a ca. 40 min gradient time and a column temperature of 8 °C. The alcohol and its derivatives were identified using HPLC with mass spectrometry (MS) detection. A large sensitivity enhancement w…
Application prospects of silica core side-glowing optical fibers
2005
The side-emitting optical fibers are specially designed to stimulate leakage of the core-transmitted radiation via their side surfaces, so creating the effect of glowing tiny wires. The basic design concepts for this kind of optical fibers are discussed, as well as some of the present and potential future applications.
Techniques de construction traditionnelles et techniques romaines dans le théâtre d’Althiburos et les monuments de spectacle de l’Afrique Proconsulai…
2023
The contribution aims to study the relationship between the traditional construction techniques of the territories of Proconsular Africa and those imported by the Romans and used in the construction of entertainment buildings, in particular theaters and amphitheatres, also taking into account the importation of typological models, starting from the “case study” of the theater of Althiburos. During the 1st and 2nd centuries AD there is a gradual introduction of Roman construction techniques, such as the opus caemaenticium, especially in the construction of substructures and vaults, sometimes with the importation of urban models, of techniques but also of Italic workers (just think of the opu…
A Quantitative Estimate of Ascorbic and Isoascorbic Acid by High Performance Liquid Chromatography: Application to Citric Juices
1993
Abstract The present report deals with the optimization and verification of a simple HPLC isocratic method useful for determining ascorbic and isoascorbic acids in standard solutions and fruit juices. Sample preparation is minimal and docs not require derivatization. The method uses an octadecyl reversed phase, a mobile phase which contains cetyltrimethyl ammonium bromide 0.05M as the ionic pair and potassium dihydrogen phosphate as a buffer, at pH=4.5, and 4-hydro-xyacetanilide as internal standard. The proposed method makes it possible to quantify ascorbic and isoascorbic acid in less than 13 minutes, with precision (C. V. 3.5%) and accuracy (recover' of 98%).
A qualitative examination of performance and energy yield of photovoltaic modules in southern Norway
2010
Three different, commercially available photovoltaic modules have been monitored outdoors in the town of Grimstad, Norway. The present paper describes the experimental setup that was implemented, in particular details of the low-cost electronic loads. Results compare measured performance with manufacturer's data, and temperature measurements enable a comparison with performance at standard test condition temperature. Overall, the monocrystalline module performed best both regarding maximum efficiency and overall energy production, whereas the module based on triple junction amorphous silicon technology had the worst performance considering these criteria. The gross numbers of energy yield c…
N-Terminal amino acid sequence analysis indicates that isolated atrial amyloid is derived from atrial natriuretic peptide
1988
Isolated atrial amyloid, the most frequent senile cardiac amyloid type, was chemically analysed. Amyloid fibrils obtained from a patient (NIP) were extracted and the predominant low-molecular-weight polypeptide (approximately 3.5 kDa, designated ASc2 NIP) was isolated by size exclusion high performance liquid chromatography in 60% formic acid. N-Terminal amino acid sequence analysis of this polypeptide was identical to that of the atrial natriuretic peptide alpha-hANP for the first 12 residues determined.
Analysis of anaerobic power in club level young rowers
2013
Aim: To date, assessment of the anaerobic components to determine performance in rowers is not part of standard evaluation or monitoring set for training. The aim of this study was to evaluate the relation between anaerobic power output and ergometer rowing performance over 2000 meters, in a group of 14 -17 years old rowers (n = 11). Methods: Each subject performed, in three separate days, two “all-out” tests, over 20 and 60 seconds, and a 2000 meters trial, using a Concept II rowing ergometer. Mean power values over 20 sec (W20) and 60 sec (W60) were measured and compared with the time to perform the 2000 m trial (t2000). Results: Statistical analysis showed high and significant correlatio…
Alla ricerca dei fattori rilevanti nell’adozione dei sistemi di gestione della performance nelle amministrazioni pubbliche territoriali. L’analisi di…
2013
La ricerca scientifica ha dimostrato che la gestione della performance nelle amministrazioni pubbliche sta oggi spostando il proprio focus dalla mera attività di raccolta e rendicontazione di dati alla generazione di informazioni atte a supportare la formulazione di decisioni. L’analisi comparativa dei casi di studio analizzati in questo articolo mira ad identificare i fattori critici sottostanti alla progettazione e all’utilizzo dei sistemi di gestione della performance nelle amministrazioni regionali. Da questa analisi emerge che alcune variabili risultano essenziali ai fini di un’efficace adozione dei sistemi di performance management. Tra queste variabili sono annoverabili: il ruolo del…
Analogical reasoning and aging: the processing speed and inhibition hypothesis.
2014
This study was designed to investigate the effect of aging on analogical reasoning by manipulating the strength of semantic association (LowAssoc or HighAssoc) and the number of distracters' semantic analogies of the A:B::C:D type and to determine which factors might be responsible for the age-related differences on analogical reasoning by testing two different theoretical frameworks: the inhibition hypothesis and the speed mediation hypothesis. We compared young adults and two groups of aging people (old and old-old) with word analogies of the A:B::C:D format. Results indicate an age-related effect on analogical reasoning, this effect being greatest with LowAssoc analogies. It was not asso…