Search results for "Radiation"
showing 10 items of 5298 documents
NanoESCA: imaging UPS and XPS with high energy resolution
2005
Abstract A novel imaging electron spectrometer has been used for laterally resolved ultraviolet photoelectron spectroscopy (UPS) and X-ray photoelectron spectroscopy (XPS) in the soft X-ray range. The instrument is based on a high-resolution emission microscope optics using a cathode lens and an imaging dispersive analyser. The analyser is corrected for the leading aberration term ( α 2 -term) by means of two hemispherical analysers in antisymmetric configuration with an appropriate transfer lens. Small-area spectra as well as energy-filtered images have been taken in the soft X-ray range for a meteorite sample and in the range of the d-band of a Cu polycrystal. An energy resolution of 106 …
Fast elemental mapping and magnetic imaging with high lateral resolution using a novel photoemission microscope
1998
Abstract Using tunable soft X-ray synchrotron radiation and a new-generation photoemission electron microscope with integral sample stage and microarea selector, elemental images and local XANES spectra have been measured. Given the present conditions (PM3 at BESSY), the lateral resolution was in the range of 130 nm with the potential of considerable improvement with high-brilliance sources (a base resolution of 25 nm was obtained in threshold photoemission). Measurements at the oxygen K-edge demonstrate that differences in the local chemical environment of the emitter atom are clearly revealed and can thus be used as a fingerprint technique for its chemical state and geometrical surroundin…
X-ray powder diffraction of mineral pigments and medicines from the 17th century pharmacy (Spezieria) Santa Maria della Scala in Rome, Italy
2018
The pharmacy (spezieria) Santa Maria della Scala was founded in Rome by the Discalced Carmelites Order in the 17th century, and during the 18th and 19th centuries it became the official supplier of medicines for Vatican Popes. The laboratory and the cases of this spezieria still preserve glass jars with organic and inorganic materials, which were presumably used for medicine and artistic material preparation, whose composition is unknown to date. A research project was initiated with the aim to study the stored materials and the role that the pharmacy played in regional, national and international contexts. In this manuscript, the compounds were analysed through X-ray powder diffraction wit…
CAD of complex passive devices composed of arbitrarily shaped waveguides using Nyström and BI-RME methods
2004
In this paper, a novel computer-aided design (CAD) tool of complex passive microwave devices in waveguide technology is proposed. Such a tool is based on a very efficient integral-equation analysis technique that provides a full-wave characterization of discontinuities between arbitrarily shaped waveguides defined by linear, circular, and/or elliptical arcs. For solving the modal analysis of such arbitrary waveguides, a modified version of the well-known boundary integral-resonant-mode expansion (BI-RME) method using the Nyström approach, instead of the traditional Galerkin version of the method of moments, is proposed, thus providing significant savings on computational costs and implement…
FDTD characterization of evanescent modes-multimode analysis of waveguide discontinuities
2000
In this paper, a finite-difference time-domain numerical dispersion relation for evanescent waves is derived, and its impact on the modeling accuracy is studied. The numerical evanescent constant is found to differ from the analytical one. As a result, a correction must be used to compute discontinuity parameters. This influences the reference plane chosen for the analysis of propagating modes. Moreover, on calculating multimode transmission and reflection coefficients, the dispersion for evanescent higher order modes is determinant. The dispersive relation is derived, discussed, and used to correct the evanescent constants for the multimode analysis of a waveguide discontinuity.
Inorganic/organic hybrid nanoparticles synthesized in a two-step radiation-driven process
2022
In this work, we have synthesized inorganic-organic hybrid nanoparticles via radiation synthesis of inorganic nanoparticles (Ag and CeO2) in aqueous dispersions containing radiation-synthesized poly(N-vinyl pyrrolidone) (PVP) nanogels (NG). The experiments show that there are strong interactions between the inorganic precursors (Ag+ and Ce3+) and the nanogel prior to irradiation. The two hybrid systems (Ag/NG and CeO2/NG) were characterized using X-ray diffraction (XRD) and transmission electron microscopy (TEM). XRD confirms the formation of crystalline Ag and CeO2. TEM reveals that the inorganic nanoparticles are evenly distributed in/on the nanogel. Both XRD and TEM show that size of the…
The luminescence of ZnO ceramics
2010
Abstract The luminescence properties of ZnO ceramics with grains 100–5000 nm sintered by different techniques from nanopowders were studied. The luminescence decay times were compared with that obtained for ZnO single crystal. The temperature dependence of non-exponential decay of defect luminescence (2.0–2.6 eV) was measured in wide time, intensity and temperature range. The luminescence decay kinetic at T ≤ 20 K shows the decay close to I(t) ∼ t−1 dependence. At temperature region 50–250 K the decay kinetics is more complicate since the TSL was observed in this temperature region. It is shown that the luminescence properties of NP and ceramics strongly depend on defect distribution on gra…
Adaption of a PIN-diode detector as an online neutron monitor for the thermal column of the TRIGA research reactor.
2017
A BNCT online neutron monitoring system was tested in a TRIGA reactor, using a silicon PIN-diode with a conversion foil. The setup was tested with different reactor powers at the hot and cold ends of the irradiation channel, using activation foils to compare with measured fluxes. The results demonstrate good reproducibility and show a linear correlation between signal of the PIN-diode and neutron flux at all positions, demonstrating this approach to be suitable for online monitoring of the neutron flux.
TL-dating applied to building archaeology: The case of the medieval church Notre-Dame-Sous-Terre (Mont-Saint-Michel, France)
2007
Abstract The recent application of thermoluminescence (TL) dating to young building materials is being increasingly developed for use in the field of buildings archaeology [ Bailif, I.K., Holland, N., 2000. Dating bricks of the two last millennia from Newcastle upon Tyne: a preliminary study. Radiat. Meas. 32, 615–619 ; Gallo N, Fieni L, Martini M, Sibillia E, 1999. Building archaeology, 14C and thermoluminescence: two examples comparison, Actes du Colloque, “C14 et Archeologie”, III e Congres International, Lyon 6–10 avril 1998, Memoire de Societe prehistorique Francaise, tome XXVI et Supplement de la revue d’Archeometrie, pp. 425–431 ; Vieillevigne, E., Guibert, P., Bechtel, F., Leriche, …