Search results for "Reactivity"

showing 10 items of 880 documents

DOTAGA-anhydride: a valuable building block for the preparation of DOTA-like chelating agents.

2012

International audience; A DOTA derivative that contains an anhydride group was readily synthesized by reacting DOTAGA with acetic anhydride and its reactivity was investigated. Opening the anhydride with propylamine led to the selective formation of one of two possible regioisomers. The structure of the obtained isomer was unambiguously determined by 1D and 2D NMR experiments, including COSY, HMBC, and NOESY techniques. This bifunctional chelating agent offers a convenient and attractive approach for labeling biomolecules and, more generally, for the synthesis of a large range of DOTA derivatives. The scope of the reaction was extended to prepare DOTA-like compounds that contained various f…

Magnetic Resonance SpectroscopyPropylamine[CHIM.THER]Chemical Sciences/Medicinal Chemistry010402 general chemistry01 natural sciencesCatalysisAnhydrideschemistry.chemical_compoundHeterocyclic Compounds 1-RingHeterocyclic CompoundsStructural isomerOrganic chemistryDOTAChelationReactivity (chemistry)BifunctionalChelating AgentsMolecular Structure010405 organic chemistryOrganic Chemistry[ CHIM.THER ] Chemical Sciences/Medicinal ChemistryGeneral ChemistryNuclear magnetic resonance spectroscopy0104 chemical sciencesAcetic anhydridechemistry
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Water dynamics and its role in structural hysteresis of dissolved organic matter

2016

Knowledge of structural dynamics of dissolved organic matter (DOM) is of paramount importance for understanding DOM stability and role in the fate of solubilized organic and inorganic compounds (e.g., nutrients and pollutants), either in soils or aquatic systems. In this study, fast field cycling (FFC) (1)H NMR relaxometry was applied to elucidate structural dynamics of terrestrial DOM, represented by two structurally contrasting DOM models such as Suwanee River (SRFA) and Pahokee peat (PPFA) fulvic acids purchased by the International Humic Substance Society. Measurement of NMR relaxation rate of water protons in heating-cooling cycles revealed structural hysteresis in both fulvic acids. I…

Magnetic Resonance SpectroscopyrelaxometrySettore AGR/13 - Chimica Agraria010501 environmental sciences01 natural scienceshumic substanceSoilRiversDissolved organic carbonEnvironmental ChemistryReactivity (chemistry)Benzopyrans0105 earth and related environmental sciencesChemistryHydrogen bondwater histeresiChemical polarityTemperatureSoil chemistryWaterHydrogen Bonding04 agricultural and veterinary sciencesGeneral ChemistryNuclear magnetic resonance spectroscopyEnvironmental chemistrySoil water040103 agronomy & agricultureProton NMR0401 agriculture forestry and fisheriesHydrophobic and Hydrophilic Interactions
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The Microbiota Promotes Arterial Thrombosis in Low-Density Lipoprotein Receptor-Deficient Mice

2019

Our results demonstrate a functional role for the commensal microbiota in atherothrombosis. In a ferric chloride injury model of the carotid artery, GF C57BL/6J mice had increased occlusion times compared to colonized controls. Interestingly, in late atherosclerosis, HFD-fed GF Ldlr−/− mice had reduced plaque rupture-induced thrombus growth in the carotid artery and diminished ex vivo thrombus formation under arterial flow conditions.

Male0209 industrial biotechnologyVery low-density lipoproteinChemokine CXCL102 engineering and technology030204 cardiovascular system & hematologyarterial thrombosisApplied Microbiology and BiotechnologyACTIVATIONMicechemistry.chemical_compound020901 industrial engineering & automation0302 clinical medicinegermfree0202 electrical engineering electronic engineering information engineeringMedicinevascular inflammationPlateletChemokine CCL7lcsh:QH301-705.5platelet0303 health sciencesatherosclerosis mouse modelsfood and beveragesThrombosisPlaque AtheroscleroticQR1-502late atherosclerosis3. Good healthHolobiontlow-density lipoprotein receptorgerm-freeplateletscardiovascular systemFemalelipids (amino acids peptides and proteins)GLYCOPROTEIN-VIBlood streamResearch ArticleRECRUITMENTmedicine.medical_specialtyNutritional compositionCOAGULATION610 Medicine & healthBiologyMETABOLISMBiochemistry Genetics and Molecular Biology (miscellaneous)MicrobiologyMicrobiologyHost-Microbe BiologyProinflammatory cytokinePLATELET HYPERREACTIVITY03 medical and health sciencesINFLAMMATIONVirologyInternal medicineatherothrombosisGeneticsmicrobiotaAnimalsInterleukin 9Platelet activationcardiovascular diseasesThrombusMolecular Biology030304 developmental biologygut microbiotabusiness.industryCholesterolcarotid artery020208 electrical & electronic engineeringcholesterolnutritional and metabolic diseasesCell Biologymedicine.diseaseMicroreviewCHLAMYDIA-PNEUMONIAEMice Mutant StrainsGastrointestinal MicrobiomeEndocrinologyReceptors LDLlcsh:Biology (General)chemistryArterial thrombusLDL receptorParasitologyatherosclerosisbusinessEx vivoLipoproteinmBio
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Mean Platelet Volume and Arterial Stiffness - Clinical Relationship and Common Genetic Variability

2017

AbstractVessel wall stiffening is an important clinical parameter, but it is unknown whether platelets, key elements in the pathogenesis of arterial thrombosis, are associated with arterial stiffness. The present studies sought to determine whether mean platelet volume (MPV), a potential marker of platelet activation, is linked to vascular elasticity as assessed by the augmentation index (AIx), in 15,010 individuals from the population-based Gutenberg Health Study. Multivariable analysis showed that MPV in both males (β 0.776; 95thCI [0.250;1.16]; p = 0.0024) and females (β 0.881[0.328;1.43]; p = 0.0018) is strongly associated with AIx. Individuals with MPV and AIx above the sex-specific me…

Male0301 basic medicinemedicine.medical_specialtyPopulationKaplan-Meier Estimate030204 cardiovascular system & hematologyPolymorphism Single NucleotideArticle03 medical and health sciencesSex FactorsVascular Stiffness0302 clinical medicineGUTENBERG HEALTHDEFICIENTINFLAMMATIONRisk FactorsInternal medicinemedicineHumansPlateletPlatelet activationMean platelet volumeeducationMETAANALYSISeducation.field_of_studyMultidisciplinaryHYPERTENSIONbusiness.industryProportional hazards modelHazard ratioGenetic VariationCROSS-SECTIONAL RELATIONSmedicine.diseaseThrombosisElasticityREACTIVITY030104 developmental biologyISCHEMIC-STROKEATHEROSCLEROSISCardiovascular DiseasesArterial stiffnessCardiologyFemalebusinessMean Platelet VolumeVASCULAR FUNCTIONBiomarkers
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Hormonal changes of intimate partner violence perpetrators in response to brief social contact with women

2022

This study investigated whether men with a history of real-life aggressive, dominant behavior show increases in testosterone and cortisol levels after brief social contact with women. Furthermore, we tested the prediction that such changes in hormones would be larger than those observed previously in young male students. Sixty-seven male participants convicted of intimate partner violence (IPV) either had brief social contact with a female confederate (experimental condition) or a male confederate (control condition). We also performed meta-analyses to investigate whether IPV perpetrators' hormonal responses were larger than the typical responses of young male students in prior studies. All…

MaleANDROGEN RECEPTOR GENETESTOSTERONE LEVELSSocial contactHydrocortisonemedia_common.quotation_subjectPSYCHOSOCIAL STRESSintimate partner violenceCOMPETITIONCourtshipArts and Humanities (miscellaneous)Developmental and Educational PsychologyLENGTHHumansTestosteroneReactivity (psychology)Cortisol levelGeneral Psychologymedia_commonhormonessocial contactTestosterone (patch)MENREACTIVITYAggressionmeta-analysisHUMAN-AGGRESSIONMeta-analysisDomestic violenceREPEATScourtshipFemalePsychologyCORTISOL RESPONSESClinical psychologyHormoneAggressive Behavior
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Alcohol preference, behavioural reactivity and cognitive functioning in female rats exposed to a three-bottle choice paradigm.

2012

Alcohol abuse is a substantial and growing health problem in Western societies. In the last years in vivo and in vitro studies have suggested that males and females display a different alcohol drinking behaviour, with swingeing differences not only in the propensity for alcohol use but also in the metabolic and behavioural consequences. In this study we investigated, in adult female rats, ethanol self-administration and preference pattern using a 3-bottle paradigm with water, 10% ethanol solution, and white wine (10%, v/v), along a four-week period. The influence of alcohol free-access on explorative behaviour in the open field (OF), and on spatial learning and reference memory in the Morri…

MaleAlcohol DrinkingMorris water navigation taskAlcohol abuseAlcoholWineSettore BIO/09 - FisiologiaChoice BehaviorOpen fieldDevelopmental psychologyBehavioral Neurosciencechemistry.chemical_compoundCognitionmedicineAnimalsLearningRats WistarEthanolBehavior AnimalEthanolCognitive flexibilitymedicine.diseasePreferenceAlcohol free-choice paradigm female rats Alcohol preference behavioural reactivity spatial learning and memoryRatschemistryWhite WineSettore BIO/14 - FarmacologiaFemalePsychologyClinical psychologyBehavioural brain research
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Comparison of ammoniated and nonammoniated extracts in children with latex allergy

2003

Background:  The use of ammoniated or nonammoniated latex extracts for the diagnosis of latex allergy is still a matter of debate. The aim of our study was to compare the characteristics of the two types of extracts by immunoblotting and RAST techniques in children with ascertained latex allergy. Methods:  Ammoniated (AL) and nonammoniated latex (NAL) extracts were prepared and blotted on SDS-PAGE to resolve their components. Also a solid phase for RAST assays was prepared with the two extracts. The sera from 18 children (mean age 11.4 years, range 6–15 years), with ascertained latex allergy (clinical history, skin test, CAP-RAST and provocation) were used for the experiments. Results:  The…

MaleAllergyLatex HypersensitivityAdolescentLatexImmunologyProvocation testImmunoblottingmedicine.disease_causeImmunoglobulin ESensitivity and SpecificityIge reactivityAllergenRadioallergosorbent TestAmmoniaLatex HypersensitivitymedicineImmunology and AllergyHumansChildSensitivity and Specificity; Immunoblotting; Electrophoresis Polyacrylamide Gel; Latex Hypersensitivity; Skin Tests; Ammonia; Humans; Child; Latex; Radioallergosorbent Test; Allergens; Immunoglobulin E; Adolescent; Female; Maleammoniated extract; diagnosis; immunoblotting; latex allergy; nonammoniated extract; RASTSkin Testsbiologymedicine.diagnostic_testSkin TestChemistryRadioallergosorbent testAllergenAllergensImmunoglobulin Emedicine.diseaseLatex allergyImmunologybiology.proteinElectrophoresis Polyacrylamide GelFemaleHuman
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Bronchial hyperresponsiveness in children with atopic rhinitis: a 7-year follow-up

2004

Background:  A high prevalence of bronchial hyperresponsiveness (BHR) was found in atopic subjects with rhinitis. Those subjects may be at higher risk for developing bronchial asthma. We evaluated, in a 7-year follow-up, BHR and atopy in a homogeneous population of nonasthmatic children with allergic rhinitis (AR), and their role in asthma development. Methods:  Twenty-eight children (6–15 years) with AR were studied. At enrollment (T0), skin tests, total serum IgE assay, peak expiratory flow (PEF) monitoring and methacholine (Mch) bronchial challenge were performed. BHR was computed as the Mch dose causing a 20% forced expiratory volume (FEV)1 fall (PD20FEV1) and as dose–response slope (DR…

MaleAllergymedicine.medical_specialtyAdolescentAtopic RhinitisImmunologyPopulationLongitudinal StudieFollow-Up StudieAtopychildrennonspecific bronchial hyperresponsivenessInternal medicinemedicineHypersensitivityHumansImmunology and AllergyLongitudinal StudiesHumans; Disease Progression; Asthma; Child; Rhinitis; Longitudinal Studies; Hypersensitivity; Pulmonary Ventilation; Bronchial Hyperreactivity; Follow-Up Studies; Adolescent; Female; MaleeducationChildRhinitiRhinitisAsthmaeducation.field_of_studyallergic rhinitis; asthma; children; methacholine test; nonspecific bronchial hyperresponsivenessallergic rhinitisbusiness.industryRespiratory diseasemethacholine testrespiratory systemasthmamedicine.diseaserespiratory tract diseasesBronchial hyperresponsivenessImmunologyDisease ProgressionMethacholineFemaleBronchial HyperreactivitybusinessPulmonary VentilationFollow-Up Studiesmedicine.drugHuman
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Inefficiency of emotion regulation as vulnerability marker for bipolar disorder: evidence from healthy individuals with hypomanic personality.

2012

Abstract Objective Emotion regulation deficits are a key characteristic of bipolar disorder (BD). In the present study, we asked if deficits in emotion regulation are also a vulnerability marker for BD. To this end, we investigated a healthy group of participants at high-risk for developing BD, defined on the basis of a hypomanic personality trait. We examined the neural correlates of two emotion regulation strategies, reappraisal and distraction. Method Twenty-two individuals with higher risk for BD and twenty-four controls were investigated in a functional magnetic resonance imaging paradigm. Participants were presented with negative, positive and neutral pictures and were either required…

MaleBipolar DisorderEmotionsAffect (psychology)AmygdalaDevelopmental psychologyYoung AdultFunctional neuroimagingRisk FactorsmedicineHumansBipolar disorderReactivity (psychology)Neural correlates of consciousnessmedicine.diagnostic_testFunctional NeuroimagingBrainmedicine.diseaseAmygdalaMagnetic Resonance ImagingPsychiatry and Mental healthClinical Psychologymedicine.anatomical_structureCase-Control StudiesFemalemedicine.symptomFunctional magnetic resonance imagingPsychologyManiapsychological phenomena and processesBiomarkersClinical psychologyJournal of affective disorders
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Pulmonary vascular resistance as a potential marker of reactive pulmonary hypertension reduction following sildenafil therapy in patients disqualifie…

2019

Purpose:We sought to determine the predictors of restoration of heart transplantation (HTx) candidacy in pa-tients with systolic heart failure (HF) and reactive fixed pulmonary hypertension (RFPH) defined as pulmonaryvascular resistance (PVR) > 2.5 Wood units (WU), transpulmonary gradient (TPG) > 12 mmHg or ≤2.5 WUwith systolic arterial pressure ≤85 mmHg during vasoreactivity test, following sildenafil therapy.Material and methods:Between2007and20181136patientswereevaluatedatourdepartmentascandidatesforHTx. Thirty-five of them, who presented with systolic HF and were not eligible for HTx due to RFPH, wereincluded in the study (31 men aged 55.1 ± 7.4 years). In all the patients sildenafil wa…

MaleCardiac Catheterizationmedicine.medical_specialtySildenafilHypertension PulmonaryVasodilator Agentsmedicine.medical_treatmentPH reductionSildenafilSildenafil CitratePulmonary hypertension03 medical and health scienceschemistry.chemical_compound0302 clinical medicineInterquartile rangeInternal medicinemedicineHumans030212 general & internal medicineRetrospective StudiesHeart transplantationbusiness.industryVasoreactivity testGeneral MedicineMiddle Agedmedicine.diseasePulmonary hypertensionmedicine.anatomical_structurechemistry030220 oncology & carcinogenesisHeart failureVascular resistanceCardiologyHeart TransplantationFemaleVascular ResistancebusinessBiomarkersAdvances in Medical Sciences
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