Search results for "STANDARD"
showing 10 items of 3299 documents
Instrucción en estrategias de comprensión lectora mediante enseñanza recíproca: efectos del agrupamiento de los estudiantes
2013
The aim of this study was to compare the effects of two grouping formats on the reading comprehension. Reading comprehension Instruction used reciprocal teaching (RT) that is an instructional procedure to teach students cognitive strategies that might lead to improved reading comprehension. A sample of 43 students in the fourth year of primary education was selected: 18 children were instructed in regular classroom (GG), 8 were instructed in small group (PG), while the remaining 17 made up the comparison group (GC). Two types of comprehension measures were used: tasks of specific effects (getting the main idea, comprehension-monitoring test) and transfer effect measures (standardized test, …
Precision luminosity measurements at LHCb
2014
Measuring cross-sections at the LHC requires the luminosity to be determined accurately at each centre-of-mass energy $\sqrt{s}$. In this paper results are reported from the luminosity calibrations carried out at the LHC interaction point 8 with the LHCb detector for $\sqrt{s}$ = 2.76, 7 and 8 TeV (proton-proton collisions) and for $\sqrt{s_{NN}}$ = 5 TeV (proton-lead collisions). Both the "van der Meer scan" and "beam-gas imaging" luminosity calibration methods were employed. It is observed that the beam density profile cannot always be described by a function that is factorizable in the two transverse coordinates. The introduction of a two-dimensional description of the beams improves sig…
Conclusion: Transnational Histories of the ‘Royal Nation’
2017
The Conclusion summarily analyses the ‘Royal Nation’ as an autonomous historical category. It draws on arguments presented in different chapters of the book, and brings out commonalities between the viewpoints of the authors of these chapters, to demonstrate as to why the interdependence between monarchies and nation-state formation gathered momentous practical significance as well as conceptual plausibility in different parts of the modern world, from the nineteenth century onwards. The Conclusion emphasizes the intellectual, aesthetic and performative, juridical, social, and political underpinnings of this interdependency; it suggests that this mutual imbrication of the royal and the nati…
Application of an HPLC-MS/MS method for mycotoxin analysis in commercial baby foods
2012
Abstract This article describes the validation of an analytical method for the detection of 21 mycotoxins in baby food. The analytical method is based on the simultaneous extraction of selected mycotoxins by matrix solid-phase dispersion (MSPD) followed by liquid chromatography coupled with tandem mass spectrometry (LC–MS/MS) using a hybrid triple quadrupole-linear ion trap mass spectrometer (QTRAP®). Information Dependent Acquisition (IDA), an extra confirmation tool for samples that contain the selected mycotoxins, was used. The matrix effects were evaluated, and the corrections for the matrix effects were performed using two calibration approaches: external matrix-matched calibration and…
Substitution–dilution method to correct the matrix effect in multi-element quantitative analysis by X-ray fluorescence
2001
Abstract A mathematical model based on the dilution–addition method (DAM) for multi-elemental analysis using an X-ray fluorescence technique is proposed. The conditions for sample preparation do not require both the unknown and standard samples to be similar in composition and mineralogy, and the unknown sample is replaced quantitatively by the standard sample, hence the denomination substitution–dilution method (SDM). This method makes it possible to correct the matrix effect in multi-elemental quantitative analysis by X-ray fluorescence for each analyte. The proposed model presents hyperbolic behaviour of the experimental data when the X-ray fluorescence intensities are represented versus…
H-Point standard additions method for resolution of binary mixtures with simultaneous addition of both analytes
1995
Abstract The basis of the H-point standard additions method, HPSAM, with simultaneous addition of both analytes is proposed for the resolution of binary mixtures. It is a modification of the previously described H-point standard additions method that permits the resolution of both species from a unique calibration set by making the simultaneous addition of the two analytes. The method uses as analytical signals the absorbances at pairs of wavelengths where each species shows the same absorbance. The required data to apply the method are the absorbance values at the previously selected wavelengths for the sample alone and spiked with both species at known concentrations. Linear relations bet…
Determination of metabolite concentrations in human brain tumour biopsy samples using HR-MAS and ERETIC measurements.
2009
Accurate determination of the concentration of the metabolites contained in intact human biopsies of 10 glioblastoma multiforme samples was achieved using one-dimensional 1H high-resolution magic angle spinning (HR-MAS) NMR combined with ERETIC™ (electronic reference to in vivo concentrations) measurements. The amount of sample used ranged from 6.8 to 12.9 mg. Metabolite concentrations were measured in each sample using two methods: with DSS (2,2-dimethyl-2-silapentane-5-sulfonate sodium salt) as an internal reference and with ERETIC™ as an external electronically generated reference. The ERETIC™ signal was shown to be highly reproducible and did not affect the spectral quality. The concent…
Determination and separation of diarylheptanoids from alder growing in Latvia
2015
The composition of diarylhepatnoids fraction isolated from bark of two alder species (grey alder and black alder) was studied. The efficiency of three extraction methods used for isolation of diarylhepatnoids from alder bark was compared. Two diarylhepatnoids: 1,7-bis-(3,4-dihydroxyphenyl)-heptan- 3-one-5-O-β-D-xylopyronoside (oregonin) and 1,7-bis-(3,4-dihydroxyphenyl)-3-hydroxyheptane-5-O-β-D- xylopyranoside were isolated from the bark of grey alder. The phenolic components of the extracts were analyzed by high-performance liquid chromatography (HPLC). Quantitative determination of oregonin was performed using an internal standard method. The results obtained show that alder barks are ric…
Massive Open Online Courses for IFRS Education: A Point of view of Spanish Accounting Educators
2016
Abstract This paper is based on a survey of 103 accounting educators from different universities of Spain on the use of MOOC, especially as regards teaching IFRS. The results show significant differences in three areas of opinion: i) the importance of the use of Internet and some Web tools for academic use; ii) general knowledge and perception of MOOCs; and iii) the opinions regarding the interest of MOOCs on IFRS. The overall opinion of educators is positive because, although the majority has never taught or participated in a MOOC, over 80% consider it useful in the learning process. Flexibility is considered the main advantage of MOOCs as well as its valuable potential for autonomous lear…
Un análisis empírico del impacto de la regulación contable en el mercado de auditoría
2017
El objetivo de la presente tesis se centra en el estudio de la estructura del mercado de la auditoría así como en analizar el impacto económico que la regulación contable ejerce sobre determinados elementos del mercado de auditoría (honorarios y rentabilidad de las firmas de auditoría). A partir de la publicación del Reglamento europeo 1606/2002 se requirió a los grupos cotizados que formulasen sus estados financieros consolidados desde el 1 de enero de 2005, conforme a las Normas Internacionales de Información Financiera o NIIF. En España, la adaptación de las NIIF al resto de empresas, no se llevó a cabo hasta la aprobación del Nuevo Plan General Contable (NPGC) y del plan para pequeñas y…