Search results for "STANDARDS"
showing 10 items of 394 documents
Application of solid-phase microextraction for determining phenylurea herbicides and their homologous anilines from vegetables.
2004
Abstract Residues of metobromuron, monolinuron and linuron herbicides and their aniline homologous were analyzed in carrots, onions and potatoes by solid-phase microextraction (SPME) performed with a polyacrylate fiber. A juice was obtained from food samples that were further diluted, and an aliquot was extracted after sodium chloride (14%) addition and pH control. At pH 4 only the phenylureas were extracted. A new extraction at pH 11 allowed the extraction of phenylureas plus homologous aniline metabolites. Determination was carried out by gas chromatography with nitrogen–phosporus detection (NPD) the identity of the determined compounds was studied by gas chromatography–mass spectrometry.…
Application of matrix solid-phase dispersion to the determination of a new generation of fungicides in fruits and vegetables.
2002
A method based on matrix solid-phase dispersion (MSPD) and gas chromatography to determine eight fungicides in fruits and vegetables is described. Fungicide residues were identified and quantified using nitrogen-phosphorus detection and electron-capture detection connected in parallel and confirmed by mass spectrometric detection. The method required 0.5 g of sample, C18 bonded silica as dispersant sorbent, silica as clean-up sorbent and ethyl acetate as eluting solvent. Recoveries from spiked orange, apple, tomato, artichoke, carrot and courgette samples ranged from 62 to 102% and relative standard deviations were less than 15% in the concentration range 0.05-10 mg kg(-1). Detection and qu…
Determination of dithiocarbamates and metabolites in plants by liquid chromatography–mass spectrometry
2004
Abstract A quantitative matrix solid-phase dispersion and liquid chromatography–atmospheric pressure chemical ionization mass spectrometry (LC–APCI–MS) method is outlined for the simultaneous analysis of dithiocarbamates (DTCs) and their degradation products in plants. Compounds analyzed are dazomet, disulfiram, thiram and the metabolites ethylenthiourea and propylenthiourea. The performance of two different sample preparation protocols, the proposed one and other based on solid-phase extraction, as well as, of both atmospheric pressure ionization sources, APCI and electrospray, were compared. The effect of several parameters on the extraction, separation and detection was studied. Dithioca…
Determination of anti GAD65 autoantibodies with an ELISA before and after standardization with the new international reference serum
2009
The serum of a stiff-man syndrome patient was declared international GAD reference standard at the "1st GAD Antibody Workshop" held at the "12th International Immunology and Diabetes Workshop" in Orlando, Florida, USA 1993. A comparative study was performed with 123 diabetic and non-diabetic patients to evaluate whether standardization of this reference serum had changed the properties of a commercially available ELISA assay. All samples classified positive with the old test were confirmed with the new assay. Four additional samples with high "normal" values became positive with the new test. One of them was a control person having a family history of diabetes and genetic loci DR4/DR11. The…
Technology standard diffusion and negative network externalities: a lesson from the third Browser War
2009
This paper presents a new model for technology standard diffusion that highlights the importance of negative network externalities in some fields of technology product such as web browsers. Again, as often happened in this research field, motivation and suggestion for such a research has been acquired from the evolution of the web browser war. So, in the paper, the main literature concerning standard diffusion has been reviewed in conjunction with web browser evolution, and the necessity of a new development of technology standard diffusion models is highlighted and supported by empirical evidences.
The alhambra photometric system
2010
Aparicio Villegas, Teresa et al.
Standard, estandarización y aplicación del artículo 102 TFUE a los conflictos sobre licencias relativas a derechos de propietad intelectual
2014
The standardization, de jure as well as de facto, gives rise to critical issues also in the field of antitrust law. Especially in recent years, the European case law and that of some member states have in particular dealt with the violation of the so-called FRAND commitments, which are undertaken by the holders of those patents that become essential for the implementation of the selected standard (Standard Essential Patents - SEPs). The EU Commission and the Courts have then several times applied the provisions on abuse of a dominant position to the attempt of the SEPs holders to prevent access to these patents by subjects that need them to operate in the downstream markets. The essay trace…
Saturated absorption spectroscopy: elimination of crossover resonances by use of a nanocell
2007
It is demonstrated that velocity selective optical pumping/saturation resonances of reduced absorption in a Rb vapor nanocell with thickness \textit{L=} $\lambda $, 2$\lambda $, and 3$\lambda $ (resonant wavelength $\lambda $ = 780 nm) allow the complete elimination of crossover (CO) resonances. We observe well pronounced resonances corresponding to the F$_{g}=3$ $\to $ F$_{e}=2,3,4$ hyperfine transitions of the $^{85}$Rb D$_{2}$ line with linewidths close to the natural width. A small CO resonance located midway between F$_{g}=3$ $\to $ F$_{e}=3$ and F$_{g}=3$ $\to$ F$_{e}=4$ transitions appears only for \textit{L} = 4$\lambda $. The D$_{2}$ line ($\lambda $ = 852 nm) in a Cs nanocell exhi…
The spanish banks in face of the corporate social responsibility Standards: previous analysis of the financial crisis
2013
Transparency of information in the field of CSR (Corporate Social Responsibility) is common to various standards. In recent years there has been a proliferation of standards and models for the formalization of CSR strategies. The objective is to assess the degree of implementation of standards of normalization. The analysis was conducted with data from the year 2008, coinciding with the first signs of the financial crisis, serving as a reference point to analyze the effect of the crisis. The field work was conducted using a survey answered by 57 Spanish credit institutions. We found a low degree of implementation of standards. The GRI (Global Reporting Initiative) and the ISO 14001 stood ou…
Measurement of the single-top-quark production cross section at CDF.
2008
We report a measurement of the single top quark production cross section in 2.2 ~fb-1 of p-pbar collision data collected by the Collider Detector at Fermilab at sqrt{s}=1.96 TeV. Candidate events are classified as signal-like by three parallel analyses which use likelihood, matrix element, and neural network discriminants. These results are combined in order to improve the sensitivity. We observe a signal consistent with the standard model prediction, but inconsistent with the background-only model by 3.7 standard deviations with a median expected sensitivity of 4.9 standard deviations. We measure a cross section of 2.2 +0.7 -0.6(stat+sys) pb, extract the CKM matrix element value |V_{tb}|=0…