Search results for "Solid"
showing 10 items of 3575 documents
Comparison of various liquid chromatographic methods for the analysis of avermectin residues in citrus fruits.
2001
Abstract Various liquid chromatographic (LC) techniques for analyzing avermectin (Abamectin) were compared after extraction of residues from citrus fruit samples by matrix solid-phase dispersion (MSPD). LC with UV and fluorescence detection were used as also was LC coupled to the mass spectrometer by an electrospray interface. The results obtained by the three methods were compared in terms of sensitivity and selectivity. The combination of MSPD extraction and LC with fluorescence detection have made it possible to quantify 0.5 μg kg −1 of Abamectin in 0.5 g of orange sample, with an overall average recovery of 94%. The procedure provides a simple and sensitive method for monitoring Abamect…
Analysis of meat samples for anabolic steroids residues by liquid chromatography/tandem mass spectrometry.
2007
A rapid, specific and highly sensitive multi-residue method for the determination of anabolic steroid residues in bovine, pork and poultry muscle tissues was developed. The sample preparation involves enzymatic digestion followed by extraction with methanol. The crude extract was cleaned up by solid-phase extraction (SPE) combining C18 and NH2 columns. The detection was carried out by a highly sensitive liquid chromatography/electrospray ionization tandem mass spectrometry (LC/ESI-MS/MS) method using both positive and negative ionization modes. Natural and synthetic steroids covering different polarities could be extracted, concentrated and purified using one single method. Mobile phase com…
Effects of acute amitriptyline administration on memory, anxiety and activity in male and female mice
2002
The effects of acute administration of amitriptyline on memory consolidation in male and female CD1 mice were investigated. Three doses of this tricyclic antidepressant (7.5, 15 and 30 mg/kg) were administered immediately after inhibitory avoidance training. Forty-five minutes after injection, subjects explored the elevated plus-maze for five minutes. Subjects were tested for avoidance twenty-four hours later. Amitriptyline impaired inhibitory avoidance consolidation at doses 7.5, 15 and 30 mg/kg in males, and at doses 7.5 and 30 mg/kg in females. In the elevated plus-maze, amitriptyline had no effect on anxiety (percentage of open arm entries) and induced a dose-dependent impairment of act…
Preconcentration and speciation of chromium in waters using solid-phase extraction and atomic absorption spectrometry
2000
Abstract A method for the preconcentration and speciation of chromium was developed. After formation of an anionic compound with ethylenediaminetetraacetic acid (CrY − ), Cr (VI) and Cr (III) are retained on a strong anionic phase (SAX) and controlled elution with 0.5 M NaCl permits their speciation. The retention and elution conditions were optimised, and interferences due to the presence of other ions such as Mg(II), Mn(II), Sn(II), Fe(III), Ba(II), Al(III), Ca(II), chloride, iodine, bromide, fluoride, sulphate, phosphate, bicarbonate and nitrate were studied. The detection limits were 0.4 μg l −1 and 1.1 μg l −1 for Cr(III) and Cr(VI), respectively, and reproducibility was 9%. The result…
Compasión y solidaridad. Hacia una propuesta de acción moral de los medios y las redes de comunicación
2019
Esta tesis tiene como objetivo indagar cómo los medios de comunicación y las TIC pueden constituirse en actores morales capaces de influir en la generación de condiciones sociales para el florecimiento de la compasión, y para su establecimiento como orientadora de la acción en las interacciones, desde las perspectivas de la ética discursiva y de la ética cordial, y cómo esto permite la construcción de solidaridad y confianza. Para rescatar esta dimensión comunicativa y visibilizar la potencialidad moral de los medios y las TIC se analiza su acción desde la ética discursiva de Jürgen Habermas y Karl Otto Apel, desde la mirada que lleva a cabo Adela Cortina con su propuesta de una “ética cord…
Premio mundial de las artes 2001
2001
Se trata de la transcripción del borrador del discurso de José Vidal-Beneyto en la entrega del Premio Mundial de las Artes a Peter Brook (Encuentro Mundial de las Artes, 2001).
Membrane-bound exosomal HSP70 as a biomarker for detection and monitoring of malignant solid tumours: a pilot study
2019
Abstract Background Cancer is the second leading cause of death globally. Early detection and disease management lead to a better survival rate. Consequently, discovery of novel methods in cancer early diagnosis is a field of active research. Minimally invasive liquid biopsies are generating growing interest. Circulating tumour cells (CTCs) have been identified in patients’ blood; nevertheless, these cells are rare and heterogeneous. Exosomes are extracellular nanovesicles released into the extracellular environment via the endosomal vesicle pathway and found in different body fluids. Exosomes deliver bioactive cargo such as proteins, mRNA and miRNA to recipient cells in the tumour environm…
Future district heating plant integrated with municipal solid waste (MSW) gasification for hydrogen production
2019
Abstract Characterizing municipal solid waste (MSW) is a critical step in planning, designing, operating, or upgrading solid waste management systems. For a theoretical investigation of hydrogen production by gasification and water-gas shift reaction, we characterized Norwegian MSW and used the data. Three different gasification setups, named as ‘A-1’, ‘A&S-2’, and ‘S-3’ were modeled using Aspen plus simulation software for direct and indirect gasification processes according to the different gasification agents. The MSW characterization result showed a reasonable agreement with existing studies in different countries. The maximum hydrogen yield achieved in setup ‘S-3’ was around 94% of the…
Energy recovery from Municipal Solid Waste in EU: proposals to assess the management performance under a circular economy perspective
2017
In 2015 the European Commission issued a package of documents on Circular Economy concerning an integrated revision of legislative proposals on waste management. The aim was to stimulate a European transition towards a circular economy concept, which is expected to foster competitiveness, sustainable economic growth and new jobs generation. Three indicators are proposed in this paper to contribute to the assessment of the energy recovery management performance from MSW in a scenario of circular economy: a) referring to MSW directly used (RMSW) or indirectly used (SRF) as input of thermochemical plants, an indicator can be the percentage of waste having LHV > 13MJ/kg; b) referring to the MSW…
Refuse Derived Fuel Gasification Possibilities in Small Scale Units
2018
Fossil fuels use reduction and waste recycling are two great challenges facing our society nowadays. A concept intended to solve both problems is Waste-to-Energy (WtE) approach (Brunner and Rechberger in Waste Manag 37: 3–12, 2015). The routes to the energy recovery can be grouped as thermo-chemical and biochemical approaches and the selection of the WtE technologies also depends on the waste composition. Waste sources can be industrial and agricultural production and urban regions but growing attention is paid to municipal solid waste in OECD countries (Hoornweg and Bhada-Tata in What a waste: a global review of solid waste management. World Bank, Washington, DC 2012) consisting dominantly…