Search results for "ToF"

showing 10 items of 841 documents

Assessing the MALDI-TOF MS sample preparation procedure to analyze the influence of thermo-oxidative ageing and thermo-mechanical degradation on poly…

2011

[EN] Multiple processing by means of successive injection cycles was used to simulate the thermo-mechanical degradation effects on the oligomeric distribution of PLA under mechanical recycling. Likewise, an accelerated thermal ageing over PLA glass transition was performed in order to simulate its service life. MALDI-TOF MS was used for the analysis and the sample preparation procedure was assessed by means of a statistical Design of Experiments (DoE). The quality effects in use for the analysis were signal-to-noise ratio and Resolution. Different matrixes, analyte/matrix proportions and the use of NaTFA as cationization agent were considered. A deep inspection of the statistical results pr…

Solucions polimèriquesPolymers and PlasticsGeneral Physics and AstronomyTransesterificationsThermo-mechanical degradationSample preparation procedureMatrix (chemical analysis)DegradationMechanismsMaterials ChemistryCationizationMechanical recyclingSample preparationRepeating unitPoly(lactide)Signal to noise ratioChemistryMultiple processingDesign of Experiments (DoE)AnalytesInjection cyclesPolylactidesMAQUINAS Y MOTORES TERMICOSMatrix-assisted laser desorption/ionization-time-of-flight mass spectrometryGlass transitionDesign of experimentsGlass lasersThermo mechanicalMALDI TOF MSChromatographyMatrixMass spectrometrySignal to noiseTermoplàsticsOrganic ChemistryDegradation mechanismThermo-oxidative ageingStatistical design of experimentsMatrix-assisted laser desorption/ionizationInvestigation methodsMatrix-Assisted Laser Desorption/Ionization Time-of-Flight Mass Spectrometry (MALDI-TOF MS)Polylactide (PLA)AgeingOligomersDegradation (geology)DesorptionDeep inspectionExperimentsPoly(lactide)European Polymer Journal
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Data for: Medically unexplained symptoms in children and adolescents: Illness-related self-concept and parental symptom evaluations

2020

Final data set for MUS in children and adolescents THIS DATASET IS ARCHIVED AT DANS/EASY, BUT NOT ACCESSIBLE HERE. TO VIEW A LIST OF FILES AND ACCESS THE FILES IN THIS DATASET CLICK ON THE DOI-LINK ABOVE

Somatoform DisorderOtherInterdisciplinary sciencesAnxietyChildAdolescence
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Polymer-Functionalised Nanograins of Mg-Doped Amorphous Calcium Carbonate via a Flow-Chemistry Approach

2019

Calcareous biominerals typically feature a hybrid nanogranular structure consisting of calcium carbonate nanograins coated with organic matrices. This nanogranular organisation has a beneficial effect on the functionality of these bioceramics. In this feasibility study, we successfully employed a flow-chemistry approach to precipitate Mg-doped amorphous calcium carbonate particles functionalized by negatively charged polyelectrolytes&mdash

SorbentMaterials sciencemicrofluidicschemistry.chemical_element02 engineering and technologyCalcium010402 general chemistrylcsh:Technology01 natural sciencesArticlePolystyrene sulfonatechemistry.chemical_compoundGeneral Materials Sciencelcsh:Microscopynanoceramicslcsh:QC120-168.85chemistry.chemical_classificationlcsh:QH201-278.5Dopantlcsh:TPolymer021001 nanoscience & nanotechnologyAmorphous calcium carbonate0104 chemical sciencesCalcium carbonatechemistryChemical engineeringlcsh:TA1-2040flow-chemistryamorphous calcium carbonatelcsh:Descriptive and experimental mechanicslcsh:Electrical engineering. Electronics. Nuclear engineeringddc:620lcsh:Engineering (General). Civil engineering (General)0210 nano-technologylcsh:TK1-9971CalcareousDepartment WerkstoffwissenschaftenbiomaterialsMaterials
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Modeling lightning observations from space-based platforms (CloudScat.jl 1.0)

2020

This is an open access article. This work is distributed under the Creative Commons Attribution 4.0 License.

Source codeSoftware_OPERATINGSYSTEMS010504 meteorology & atmospheric sciencesComputer sciencemedia_common.quotation_subjectMultispectral imageReal-time computingCloud computingComputingMilieux_LEGALASPECTSOFCOMPUTINGclouds01 natural sciencesComponent (UML)0103 physical sciencesInternational Space Station010303 astronomy & astrophysics0105 earth and related environmental sciencesmedia_commonHardware_MEMORYSTRUCTURESbusiness.industrylcsh:QE1-996.5scatteringAtmosphärische SpurenstoffeModular designLightninglcsh:GeologySatellitebusinesslightning
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CCDC 1985884: Experimental Crystal Structure Determination

2020

Related Article: Marta Mon, Rosaria Bruno, Sergio Sanz-Navarro, Cristina Negro, Jesús Ferrando-Soria, Lucia Bartella, Leonardo Di Donna, Mario Prejanò, Tiziana Marino, Antonio Leyva-Pérez, Donatella Armentano, Emilio Pardo|2020|Nat.Commun.|11|3080|doi:10.1038/s41467-020-16699-3

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinatescatena-[tris(mu-2-[{[(1-carboxylato-2-hydroxyethyl)carboximidato](oxidanidyl)methylidene}amino]-3-hydroxypropanoato)-bis(mu-hydroxo)-tetrakis(mu-aqua)-calcium(ii)-hexa-copper(ii) 1346-tetra-O-acetylfructofuranoside hexadecahydrate]
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CCDC 1828625: Experimental Crystal Structure Determination

2018

Related Article: Rosaria Bruno, Nadia Marino, Lucia Bartella, Leonardo Di Donna, Giovanni De Munno, Emilio Pardo, Donatella Armentano|2018|Chem.Commun.|54|6356|doi:10.1039/C8CC03544J

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterscatena-[tetrakis(mu-4-amino-1-(5-O-phosphonatopentofuranosyl)pyrimidin-2(1H)-one)-hexakis(110-phenanthroline)-tetra-aqua-hepta-copper(ii) hexakis(nitrate) D-aspartic acid solvate hydrate]Experimental 3D Coordinates
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CCDC 1828624: Experimental Crystal Structure Determination

2018

Related Article: Rosaria Bruno, Nadia Marino, Lucia Bartella, Leonardo Di Donna, Giovanni De Munno, Emilio Pardo, Donatella Armentano|2018|Chem.Commun.|54|6356|doi:10.1039/C8CC03544J

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterscatena-[tetrakis(mu-4-amino-1-(5-O-phosphonatopentofuranosyl)pyrimidin-2(1H)-one)-hexakis(110-phenanthroline)-tetra-aqua-hepta-copper(ii) hexakis(nitrate) hydrate]Experimental 3D Coordinates
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A model-based approach for assessing bronchodilator responsiveness in children: The conventional cutoff revisited

2020

An increase in FEV1 >=12% has been proposed in international guidelines as a clue to airway reversibility for diagnosing asthma in both adults and children. However, the validity of this cut-off has been questioned in the pediatric population. The aim of this study was to provide evidence that different cut-off values in BDR may be associated with better performance in discriminating among outpatient children with naïve asthma (A) and without asthma (NA). We compared three approaches: i) the conventional cutoff (12%); ii) the cut-off estimated by Youden's criteria; and iii) the cut-off based on a model-driven approach. we found that the conventional cut-off of 12% showed poor sensitivity in…

SpirometryMalePediatricsmedicine.medical_specialtycut-offAdolescentmedicine.drug_classImmunologyspirometrySensitivity and Specificitysegmented modelchildrenReference ValuesBronchodilatorForced Expiratory VolumeImmunology and AllergyMedicineCutoffHumansChildAsthmaModels Statisticalmedicine.diagnostic_testbusiness.industryasthmachildren asthma spirometry bronchodilator response cut-offmedicine.diseaseBronchodilator AgentsChild PreschoolFemalebronchodilator responsedynamic nomogrambusiness
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Kinematogrāfiskā maldināšana un naratīva metalepse Kristofera Nolana filmās „Starp zvaigznēm”, „Pirmsākums” un „Ilūzija”

2015

Bakalaura darba mērķis ir noskaidrot kā notiek kinematogrāfiskā maldināšana Kristofera Nolana filmās, kā arī noteikt kādi kino valodas elementi tiek izmantoti, lai radītu naratīva metalepsi. Darbā tika aplūkoti laika secības, maldināšanas, naratīva un semiotikas teorētiskie aspekti, kā arī tika veikta naratīva un semiotiskā analīze. Veiktā pētījuma rezultāti parādīja, ka maldināšanu veicina filmu naratīva struktūra, informācijas slēpšana, personāži-viltotāji un laika secības izmaiņas. Metalepsi rada montāža, reālistiska kameras izmantošana un varoņu vienlaicīga pastāvēšana vairākās dimensijās. Par autora stila elementiem var uzskatīt arī tumšus krāsu toņus, muzikālo noformējumu, sieviešu pe…

Starp zvaigznēmKristofers Nolansnaratīva metalepsemaldināšanaPirmsākumsKomunikācijas zinātne
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On powerful exact nonrandomized tests for the Poisson two-sample setting.

2020

In the case of two independent samples from Poisson distributions, the natural target parameter for hypothesis testing is the ratio of the two population means. The conditional tests which have been derived for this class of problems already in the 1940s are well known to be optimal in terms of power only when randomized decisions between hypotheses are admitted at the boundary of the respective rejection regions. The major objective of this contribution is to show how the approach used by Boschloo in 1970 for constructing a powerful nonrandomized version of Fisher’s exact test for hypotheses about the odds ratio between two binomial parameters can successfully be adapted for the Poisson c…

Statistics and Probabilityeducation.field_of_studyEpidemiologyPopulationBoundary (topology)Poisson distribution01 natural sciences010104 statistics & probability03 medical and health sciencessymbols.namesakeExact test0302 clinical medicineHealth Information ManagementSample size determinationSample SizesymbolsCutoffApplied mathematics030212 general & internal medicinePoisson Distribution0101 mathematicseducationEquivalence (measure theory)Statistical hypothesis testingMathematicsStatistical methods in medical research
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