Search results for "Validation Studies"

showing 5 items of 25 documents

Are analysts doing method validation in liquid chromatography?

2014

International audience; Method validation is being applied in the reported analytical methods for decades. Even before this protocol was defined, authors already somehow validated their methods without full awareness. They wished to assure the quality of their work. Validation is an applied approach to verify that a method is suitable and rugged enough to function as a quality control tool in different locations and times. The performance parameters and statistical protocols followed throughout a validation study vary with the source of guidelines. Before single laboratory validation, an analytical method should be fully developed and optimized. The purpose of the validation is to confirm p…

Quality ControlValidation studyDIODE-ARRAY DETECTIONMethod validationmedia_common.quotation_subjectLiquid chromatographyValidation Studies as TopicGuidelinesBiochemistryField (computer science)Analytical Chemistry[CHIM.ANAL]Chemical Sciences/Analytical chemistrySIMPLE HPLC METHODHumansQuality (business)HUMAN PLASMATANDEM MASS-SPECTROMETRYRAT PLASMAFunction (engineering)SurveyRP-LC METHODmedia_commonProtocol (science)AnalystsChromatographyPoint (typography)ChemistryData CollectionOrganic ChemistryGeneral MedicineEvaluated validation parametersMethod developmentFully developedSOLID-PHASE EXTRACTIONESI-MS/MS METHODPHARMACEUTICAL DOSAGE FORMChromatography LiquidTHIN-LAYER-CHROMATOGRAPHY
researchProduct

Cross-cultural adaptation and test-retest reliability of the spanish ROWAN foot pain assessment questionnaire (ROFPAQ-S)

2020

Background The ROWAN Foot Pain Assessment Questionnaire (ROFPAQ) may be considered as a self-reported health questionnaire with 45 items to measure foot health problems such as foot pain. To date, the ROFPAQ has only been validated into an English-language version. Objectives Therefore this study aim was to perform the cross-cultural adaptation and test-retest reliability of the Spanish ROFPAQ version (ROFPAQ-S). Study design A cross-sectional descriptive study. Settings Podiatry and physiotherapy clinical centers. Methods The recommended forward/backward translation protocol was applied for the procedure of translation and cross-cultural adaptation from United Kingdom to Spain. Results An …

Quality of lifeAdultCross-Cultural ComparisonMalemedicine.medical_specialtyIntraclass correlationCalidad de vidaPainChronic painEnquestesFoot DiseasesQuality of lifeCronbach's alphaPain assessmentSurveys and QuestionnairesMedicineHumansTranslationsReliability (statistics)LanguagePain MeasurementFootHealth impact assessmentbusiness.industryPiePodiatryChronic painReproducibility of ResultsMiddle AgedDolor crónicomedicine.diseasePatologiaTest (assessment)ExtremitatsEstudios de validaciónAnesthesiology and Pain MedicineCross-Sectional StudiesValidation studiesSpainPhysical therapyFemalebusiness
researchProduct

Validation of a questionnaire designed to measure nursing student satisfaction with practical training

2019

Objective: to validate an instrument designed to assess practical training and measure nursing student satisfaction with clinical practice modules. Method: cross-sectional study (academic year 2014-2015). Validation of the self-administered, anonymous, 17-item Nursing Student Satisfaction with Practical Training Questionnaire, developed by consensus by eight practical training experts in three nominal group sessions. Exploratory and confirmatory factor analyses were performed to assess internal consistency and validity. Student satisfaction was measured in relation to each module and all modules as a whole. Results: 174 responses. High item-test correlation (≥0.90); Cronbach’s alpha = 0.91;…

Satisfacción PersonalEncuestas y CuestionariosNursing Education ResearchSurveys and QuestionnairesInvestigación en Educación de EnfermeríaEducación en EnfermeríaEstudiantes de EnfermeríaStudents NursingEnfermeríaPersonal SatisfactionValidation StudiesEducation NursingEstudios de Validación
researchProduct

Dose calculation in biological samples in a mixed neutron-gamma field at the TRIGA reactor of the University of Mainz

2010

To establish Boron Neutron Capture Therapy (BNCT) for non-resectable liver metastases and for in vitro experiments at the TRIGA Mark II reactor at the University of Mainz, Germany, it is necessary to have a reliable dose monitoring system. The in vitro experiments are used to determine the relative biological effectiveness (RBE) of liver and cancer cells in our mixed neutron and gamma fi eld. We work with alanine detectors in combination with Monte Carlo simulations, where we can measure and characterize the dose. To verify our calculations we perform neutron fl ux measurements using gold foil activation and pin-diodes . Material and methods . When L- α -alanine is irradiated with ionizing …

inorganic chemicalsPhysics::Instrumentation and DetectorsQuantitative Biology::Tissues and OrgansPhysics::Medical PhysicsBoron Neutron Capture TherapyValidation Studies as TopicModels BiologicalIonizing radiationTRIGAHospitals UniversityNuclear ReactorsCell Line TumorGermanyRelative biological effectivenessMedicineDosimetryHumansRadiology Nuclear Medicine and imagingNeutronNeutronsbusiness.industryRadiotherapy Planning Computer-AssistedRadiochemistryLiver NeoplasmsRadiotherapy DosageHematologyGeneral MedicineHep G2 CellsNeutron temperatureNeutron captureOncologyGamma RaysAbsorbed dosebusinessNuclear medicineColorectal Neoplasms
researchProduct

The incidence of hip fractures in Norway –accuracy of the national Norwegian patient registry

2014

Background Hip fractures incur the greatest medical costs of any fracture. Valid epidemiological data are important to monitor for time-dependent changes. In Norway, hip fractures are registered in the Norwegian Patient Registry (NPR), but no published national validation exists. The aim of the present study was a national validation of NPR as a register for hip fractures using diagnostic codes (ICD-10 S 72.0-2) and/or procedure codes (NOMESCO version 1.14 NFBxy (x = 0-9, y = 0-2) or NFJxy (x = 0-9, y = 0-2). Method A nationwide, population-based cohort comprising a random sub-sample of 1,000 hip fracture-related entries for the years 2008–09 was drawn from the NPR. 200 entries were defined…

medicine.medical_specialtyVDP::Medical disciplines: 700::Clinical medical disciplines: 750::Orthopedic surgery: 784EpidemiologyPopulationNorwegianHip fractureDatabaseCohort StudiesRheumatologyInternational Classification of DiseasesEpidemiologyMedicineHumansOrthopedics and Sports MedicineRegistrieseducationeducation.field_of_studyHip fracturebusiness.industryHip FracturesNorwayIncidence (epidemiology)Incidencemedicine.diseaselanguage.human_languageValidation studiesPopulation SurveillanceCohortlanguagePhysical therapyDiagnosis codebusinessCohort studyBMC Musculoskeletal Disorders
researchProduct