Search results for "ample"
showing 10 items of 2398 documents
Selection From Bibliographic Resources of an Analytical Method for Cosmetic Products
2018
Abstract This chapter is focussed on a general strategy to select an appropriate method from the scientific literature to solve an analytical problem in cosmetic analysis using useful and flexible web tools. A short introduction on the use of ScienceDirect (Elsevier), Scopus (Elsevier), SciFinder Scholar (American Chemical Society), Web of Science (Thomson Reuters) and the freely available Google Scholar is given. The main analytical features to be considered in the selection of the method, such as limit of detection, limit of quantification, linearity, precision (repeatability, intermediate precision and reproducibility), selectivity, robustness and accuracy, are briefly described. Additio…
From the crowd to the market: The role of reward-based crowdfunding performance in attracting professional investors
2017
Abstract We focus on new technology-based entrepreneurial ventures engaging in reward-based crowdfunding and examine the effect of their performance in such funding channel on the likelihood of securing subsequent funding from professional investors. We also study how this effect is influenced by the presence of patents granted for the new product idea and the entrepreneur social capital. Results from a sample of technology projects launched on Kickstarter demonstrate that pledging a higher amount of money in crowdfunding can ignite professional investors’ interest and thus help secure subsequent funding. However, this positive evidence is effective only when complemented by the presence of…
Comparison of green sample preparation techniques in the analysis of pyrethrins and pyrethroids in baby food by liquid chromatography–tandem mass spe…
2017
A new selective and sensitive liquid chromatography triple quadrupole mass spectrometry method was developed for simultaneous analysis of natural pyrethrins and synthetic pyrethroids residues in baby food. In this study, two sample preparation methods based on ultrasound-assisted dispersive liquid–liquid microextraction (UA-DLLME) and salting-out assisted liquid–liquid extraction (SALLE) were optimized, and then, compared regarding the performance criteria. Appropriate linearity in solvent and matrix-based calibrations, and suitable recoveries (75–120%) and precision (RSD values ≤ 16%) were achieved for selected analytes by any of the sample preparation procedures. Both methods provided the…
Confirmation of Fenthion Metabolites in Oranges by IT-MS and QqTOF-MS
2007
14 pages, 4 figures, 4 tables.-- PMID: 18020315 [PubMed].-- Printed version published Dec 15, 2007.
Implant insertion torque value in immediate loading : a retrospective study
2019
Background The aim of this study is to verify if the Insertion Torque Value (ITV) of 32 Ncm for immediate loading protocol (ILP), as indicated by literature, is still, with the advance in implant research, a real significant cut-off for long-term implant survival. Material and Methods In this retrospective study, data from 224 patients that during three years of clinical practice, were submitted to the insertion of 322 implants with immediate loading protocol, have been recorded, pooled and analyzed. Data were organized based on Insertion Torque Value (ITV): > 32 Ncm (CG) and 32 Ncm are still characterized by a lower crestal bone resorption, there are no statistically significant difference…
Triggering Open Innovation Processes Through Organizational Emotional Capability and Rival's Absorptive Capacity Orientation
2022
In this article, we analyze the direct effects of the open innovation (OI) processes of acquisition and exploitation on innovation performance (IP), as well as the effects of two antecedents of OI: organizational emotional capability (EC) and rivaĺs absorptive capacity orientation (RACO). RACO implies processing external information in an analytical manner, whereas an intuitive approach is implicit in EC. The research model is tested in a sample of medium-low-technology Colombian small and medium-sized enterprises (SMEs) using structural equations by the consistent partial least squares method. Our results provide evidence on a significant effect of the OI acquisition process on IP, as well…
Ensuring content validity of psychological and educational tests – the role of experts
2020
Many test developers try to ensure the content validity of their tests by having external experts review the items in terms of relevance, difficulty, clarity, and so on. Although this approach is widely accepted, a closer look reveals there are several pitfalls that need to be avoided if experts’ advice is to be truly helpful. First, I offer a classification of tasks experts are given by test developers as reported on in the literature dealing with procedures of drawing on experts’ advice. Second, I review a sample of reports on test development (N = 72) to identify the common current procedures for selecting and consulting experts. Results indicate that often the choice of experts seems to…
Substitution–dilution method to correct the matrix effect in multi-element quantitative analysis by X-ray fluorescence
2001
Abstract A mathematical model based on the dilution–addition method (DAM) for multi-elemental analysis using an X-ray fluorescence technique is proposed. The conditions for sample preparation do not require both the unknown and standard samples to be similar in composition and mineralogy, and the unknown sample is replaced quantitatively by the standard sample, hence the denomination substitution–dilution method (SDM). This method makes it possible to correct the matrix effect in multi-elemental quantitative analysis by X-ray fluorescence for each analyte. The proposed model presents hyperbolic behaviour of the experimental data when the X-ray fluorescence intensities are represented versus…
Determination of metabolite concentrations in human brain tumour biopsy samples using HR-MAS and ERETIC measurements.
2009
Accurate determination of the concentration of the metabolites contained in intact human biopsies of 10 glioblastoma multiforme samples was achieved using one-dimensional 1H high-resolution magic angle spinning (HR-MAS) NMR combined with ERETIC™ (electronic reference to in vivo concentrations) measurements. The amount of sample used ranged from 6.8 to 12.9 mg. Metabolite concentrations were measured in each sample using two methods: with DSS (2,2-dimethyl-2-silapentane-5-sulfonate sodium salt) as an internal reference and with ERETIC™ as an external electronically generated reference. The ERETIC™ signal was shown to be highly reproducible and did not affect the spectral quality. The concent…
Principales problemas de internacionalización de las cooperativas agroalimentarias españolas
2013
Food and agricultural cooperatives, as well as other food companies must consider internationalization as essential for them for their survival; and although there are governmental and private agencies that can support them in this challenge, it is necessary to deeply study the problems that cooperatives face in international markets. Using a methodology that combines theoretical review with qualitative research, the main problems from a sample of internationalized Spanish cooperatives are identified and classified by differentiating the internal from the external ones so as in the near future the necessary measures to minimize or avoid them could be taken by managers and support agencies. …