Search results for "api"

Determination of muscimol and ibotenic acid in mushrooms of Amanitaceae by capillary electrophoresis

2014

In this study, the CZE method for rapid quantitative and qualitative determination of ibotenic acid and muscimol in Amanita mushrooms naturally grown in Poland was developed. The investigations included the species of A. muscaria, A. pantherina, and A. citrina, collected in southern region of Poland. The studied hallucinogenic compounds were effectively extracted with a mixture of methanol and 1 mM sodium phosphate buffer at pH 3 (1:1 v/v) using ultrasound-assisted procedure. The obtained extracts were separated and determined by CZE utilizing a 25 mM sodium phosphate running buffer adjusted to pH 3 with 5% content of acetonitrile v/v. The calibration curves for both analytes were linear in…

El capitalismo, contra el planeta / 2

2007

Palaeohistology helps reveal taxonomic variability in exceptionally large temnospondyl humeri from the Upper Triassic of Krasiejów, SW Poland

2023

For more than twenty years, palaeontological excavations have been carried out at the Upper Triassic site of Krasiejów (south-west Poland), providing thousands of skeletal elements belonging to various tetrapod groups. However, almost all bones are preserved in a disarticulated state. This generates problems in taxonomic assignment among closely related groups, e.g., stereospondyl amphibians. As far as cranial elements, the pectoral girdle bones and the intercentra are very diagnostic, while all other remaining skeletal elements are difficult to unambiguously assign between either the capitosaurid Cyclotosaurus intermedius or the trematosaurid Metoposaurus krasiejowensis, both originating f…

Beneficial impact of wave-breaking for coherent continuum formation in normally dispersive nonlinear fibers

2008

International audience; We study the evolution of a pulse propagating in a normally dispersive fiber in the presence of Kerr nonlinearity. We review the temporal and spectral impact of optical wave-breaking in the development of a continuum. The impact of linear losses or gain is also investigated.

Perineural Invasion is a Strong Prognostic Moderator in Ampulla of Vater Carcinoma

2018

Objective Ampulla of Vater carcinoma (AVC) has a broad spectrum of different prognoses. As such, new moderators of survival are urgently needed. We aimed at clarifying the prognostic role of perineural invasion in AVC. Methods Using PubMed and SCOPUS databases, we conducted the first systematic review and meta-analysis on this topic. Results Analyzing 29 articles for a total of 2379 patients, we found that the presence of perineural invasion increased the risk of all-cause mortality more than 2 times (relative risk [RR], 2.07; 95% confidence interval [CI], 1.78-2.42 [P < 0.0001]; hazard ratio [HR], 2.72; 95% CI, 1.86-3.97 [P < 0.0001]), of cancer-specific mortality more than 6 times (…

un approccio teorico-sperimentale per la ricostruzione del profilo trasversale di rotaie usurate

2012

La sovrastruttura ferroviaria durante la sua vita utile è sottoposta oltre ai carichi dinamici generati dai rotabili (azioni verticali, laterali, ecc.), anche ai carichi termici e ad azioni ambientali di varia natura. Tali sollecitazioni, interagendo sinergicamente tra loro, determinano il deterioramento della sovrastruttura ferroviaria inteso come discostamento dalla configurazione geometrica di progetto e l’usura dei singoli componenti del binario e della massicciata. Per valutare lo stato di efficienza della sovrastruttura è consuetudine far riferimento ad alcuni parametri geometrici del binario che, peraltro, permettono di formulare un giudizio oggettivo circa il livello di sicurezza of…

Applicazione del metodo Failure Mode, Effects and Criticality Analysis (FMECA) in Tomoterapia: confronto tra approccio classico e metodologia fuzzy

2021

Le analisi di incidenti nel settore radioterapico hanno evidenziato ed evidenziano la necessità di incrementare le misure di garanzia della qualità (QA) a partire dall’identificazione di guasti/errori considerati rari, ma con conseguenze molto severe. In questo ambito, l’applicazione della tecnica Failure Mode, Effects And Criticality Analysis (FMECA) per la classificazione di eventi critici ha riscontrato un grande interesse. Lo scopo del presente lavoro è la comparazione dei risultati ottenuti nell’applicazione di due diverse metodologie FMECA (classica e fuzzy) per la valutazione dei rischi su pazienti sottoposti a trattamenti eseguiti con tomoterapia elicoidale. Il confronto è stato eff…

In vitro evaluation of the ability of three apex locators to determine the working length during retreatment.

2005

The purpose of this in vitro study was to evaluate the accuracy of three apex locators in determining the working length during the retreatment process. Twenty extracted single-rooted human teeth with mature apices were used in this study. The root canal length of each tooth was measured placing a #15 file until the tip was visible at the apical foramen. The direct visual measurement was reduced by 0.5 mm and recorded. The root canals were instrumented and filled to the direct visual measurement using lateral compaction technique. After 7 days the teeth were retreated using three apex locators: ProPex, NovApex, and Root ZX, for determining the retreatment working length. Afterward, comparis…

Diffusion technique for the generation of gaseous halogen standards

2009

Abstract Halogens are known to play an important role in the tropospheric ozone-depletion chemistry and are of special interest because of their influence on the atmospheric oxidation capacity. In this paper, we investigate the application of a capillary diffusion technique for the generation of gaseous halogen standards like Br 2 , IBr, ICl and I 2 . The influence of capillary dimension (i.e. length and inner diameter), ambient pressure and headspace volume of the diffusion vessel on the test gas output has been evaluated. The experimental output rates are determined from the mass loss of the analyte vessel on a regular schedule and compared with their respective theoretical predictions. W…

In tube-solid phase microextraction-nano liquid chromatography: Application to the determination of intact and degraded polar triazines in waters and…

2017

Abstract In-tube solid-phase microextraction (IT-SPME) coupled to miniaturized liquid chromatography (LC) techniques are attractive mainly due to the column efficiency improvement, sensitivity enhancement and reduction of solvent consumption. In addition, the nanomaterials based sorbents can play a key role in the improvement of the extraction efficiency taking into account their interesting physical and chemical properties. Thus, in this work the performance of IT-SPME coupled to nano LC (NanoLC) has been compared with the performance of IT-SPME coupled to capillary LC (CapLC) with similar configurations for the determination of polar triazines including their degradation products. In both…