Search results for "cyclobutane"

showing 10 items of 35 documents

Experimental and Theoretical Study on the Cycloreversion of a Nucleobase-Derived Azetidine by Photoinduced Electron Transfer.

2018

[EN] Azetidines are interesting compounds in medicine and chemistry as bioactive scaffolds and synthetic intermediates. However, photochemical processes involved in the generation and fate of azetidine-derived radical ions have scarcely been reported. In this context, the photoreduction of this four-membered heterocycle might be relevant in connection with the DNA (6-4) photoproduct obtained from photolyase. Herein, a stable azabipyrimidinic azetidine (AZT(m)), obtained from cycloaddition between thymine and 6-azauracil units, is considered to be an interesting model of the proposed azetidine-like intermediate. Hence, its photoreduction and photo-oxidation are thoroughly investigated throug…

Models MolecularPhotochemistryRadicalAzetidinePyrimidine dimer010402 general chemistryPhotochemistry01 natural sciencesCatalysisPhotoinduced electron transferNucleobaseCyclobutaneElectron transferElectron Transportchemistry.chemical_compoundElectron transferQUIMICA ORGANICAUracilCycloadditionAza CompoundsCycloaddition Reaction010405 organic chemistryOrganic ChemistryGeneral ChemistryRadicalsPhotochemical Processes0104 chemical sciencesThymineDensity functional calculationsPyrimidineschemistryPyrimidine DimersAzetidinesOxidation-ReductionThymineChemistry (Weinheim an der Bergstrasse, Germany)
researchProduct

Theoretical insight into the intrinsic ultrafast formation of cyclobutane pyrimidine dimers in UV-irradiated DNA: thymine versus cytosine.

2008

The higher formation yields measured in the ultrafast photoinduced formation of cyclobutane thymine dimers (T T) with respect to those of cytosine (C C) are explained, on the basis of ab initio CASPT2 results, by the existence in thymine of more reactive orientations and a less efficient photoreversibility, whereas in cytosine the funnel toward the photolesion becomes competitive with that mediating the internal conversion of the excited-cytosine monomer.

Models MolecularTime FactorsUltraviolet RaysAb initioPyrimidine dimerDNAInternal conversion (chemistry)PhotochemistrySurfaces Coatings and FilmsThymineCyclobutanechemistry.chemical_compoundCytosineMonomerchemistryPyrimidine DimersMaterials ChemistryNucleic Acid ConformationPhysical and Theoretical ChemistryCytosineDNAThymineDNA DamageThe journal of physical chemistry. B
researchProduct

On the Intrinsically Low Quantum Yields of Pyrimidine DNA Photodamages: Evaluating the Reactivity of the Corresponding Minimum Energy Crossing Points

2020

The low quantum yield of photoformation of cyclobutane pyrimidine dimers and pyrimidine-pyrimidone (6-4) adducts in DNA bases is usually associated with the presence of more favorable nonreactive decay paths and with the unlikeliness of exciting the system in a favorable conformation. Here, we prove that the ability of the reactive conical intersection to bring the system either back to the absorbing conformation or to the photoproduct must be considered as a fundamental factor in the low quantum yields of the mentioned photodamage. In support of the proposed model, the one order of magnitude difference in the quantum yield of formation of the cyclobutane thymine dimer with respect to the t…

PyrimidineUltraviolet RaysQuantum yieldPyrimidine dimer010402 general chemistryPhotochemistry01 natural sciencesNucleobaseAdductCyclobutanechemistry.chemical_compound0103 physical sciencesComputer SimulationGeneral Materials SciencePhysical and Theoretical Chemistry010304 chemical physicsChemistryDNAConical intersectionPhotochemical Processes0104 chemical sciences3. Good healthThymineEstructura químicaPyrimidine DimersFisicoquímica
researchProduct

Molecular Basis of DNA Photodimerization: Intrinsic Production of Cyclobutane Cytosine Dimers

2008

Based on CASPT2 results, the present contribution establishes for the first time that cytosine photodimer formation (CC) is mediated along the triplet and singlet manifold by a singlet-triplet crossing, (T1/S0)X, and by a conical intersection, (S1/S0)CI, respectively. The former can be accessed in a barrierless way from a great variety of photochemical avenues and exhibits a covalent single bond between the ethene C6-C6' carbon atoms of each monomer. The efficiency of the stepwise triplet mechanism, however, would be modulated by the effectiveness of the intersystem crossing mechanism. The results provide the grounds for the understanding of the potential photogenotoxicity of endogenous and…

Quantitative Biology::BiomoleculesPhotochemistryUltraviolet RaysChemistryDNAGeneral ChemistryConical intersectionPhotochemistryBiochemistryCatalysisCyclobutaneCytosinechemistry.chemical_compoundColloid and Surface ChemistryIntersystem crossingPyrimidine DimersCovalent bondExcited stateNucleic Acid ConformationSingle bondSinglet stateDimerizationCytosineDNA DamageJournal of the American Chemical Society
researchProduct

Squaraine Dyes for Photodynamic Therapy: Study of Their Cytotoxicity and Genotoxicity in Bacteria and Mammalian Cells¶‡

2007

Halogenated squaraine dyes are characterized by long wavelength absorption (>600 nm) and high triplet yields and therefore represent new types of photosensitizers that could be useful for photodynamic therapy. We have analyzed the cytotoxicity and genotoxicity of the bromo derivative 1, the iodo derivative 2 and the corresponding nonhalogenated dye 3 in the absence and presence of visible light. At concentrations of 1-2 microM, 1 and 2 reduced the cloning efficiency of AS52 Chinese hamster ovary cells to less than 1% under conditions that were well tolerated in the dark. Similarly, the proliferation of L5178Y mouse lymphoma cells was inhibited by photoexcited 1 and 2 with high selectivity. …

Salmonella typhimuriumLightmedicine.medical_treatmentPhotodynamic therapyCHO CellsPhotochemistrymedicine.disease_causeBiochemistryMicePhenolsCricetinaemedicineTumor Cells CulturedAnimalsPhysical and Theoretical ChemistryCytotoxicityMicronucleus TestsPhotosensitizing AgentsbiologyDose-Response Relationship DrugMolecular StructureChemistryCytotoxinsMutagenicity TestsChinese hamster ovary cellGeneral Medicinebiology.organism_classificationIn vitroPhotochemotherapyMicronucleus testMutationBiophysicsBacteriaGenotoxicityCyclobutanesVisible spectrumMutagensPhotochemistry and Photobiology
researchProduct

CCDC 2058519: Experimental Crystal Structure Determination

2021

Related Article: Esa Kukkonen, Elmeri Lahtinen, Pasi Myllyperkiö, Matti Haukka, Jari Konu|2021|New J.Chem.|45|6640|doi:10.1039/D1NJ00456E

Space GroupCrystallography11'-[24-bis(2-chloro-34-dimethoxyphenyl)cyclobutane-13-diyl]bis(4-nitrobenzene)Crystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 2058518: Experimental Crystal Structure Determination

2021

Related Article: Esa Kukkonen, Elmeri Lahtinen, Pasi Myllyperkiö, Matti Haukka, Jari Konu|2021|New J.Chem.|45|6640|doi:10.1039/D1NJ00456E

Space GroupCrystallography11'-[24-bis(2-chloro-34-dimethoxyphenyl)cyclobutane-13-diyl]bis(4-nitrobenzene)Crystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 893839: Experimental Crystal Structure Determination

2013

Related Article: Emilio Escrivá, Lucía Soto, Juan Server-Carrió, Carlos J. Gómez-García, Guillermo Mínguez Espallargas, Nailette Ruiz, Amparo Sancho, Julia García-Lozano, Carmen Ramírez de Arellano|2013|Polyhedron|56|90|doi:10.1016/j.poly.2013.03.016

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinatescatena-[tris(mu~2~-Cyclobutane-1234-tetrone)-bis(di-1H-imidazol-2-yl-N-methylmethanaminium)-diaqua-di-copper dihydrate]
researchProduct

CCDC 712097: Experimental Crystal Structure Determination

2011

Related Article: J.Carranza, J.Sletten, F.Lloret, M.Julve|2011|Inorg.Chim.Acta|371|13|doi:10.1016/j.ica.2011.02.087

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parametersbis((mu~2~-Hydroxo)-(mu~2~-cyclobutane-1234-tetrone))-tetra-aqua-di-iron dihydrateExperimental 3D Coordinates
researchProduct

CCDC 712096: Experimental Crystal Structure Determination

2011

Related Article: J.Carranza, J.Sletten, F.Lloret, M.Julve|2011|Inorg.Chim.Acta|371|13|doi:10.1016/j.ica.2011.02.087

Space GroupCrystallographyCrystal SystemCrystal Structurecatena-((mu~2~-Cyclobutane-1234-tetrone)-tetra-aqua-cobalt)Cell ParametersExperimental 3D Coordinates
researchProduct