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showing 10 items of 3080 documents

Association of basal forebrain volumes and cognition in normal aging.

2013

The basal forebrain cholinergic system (BFCS) is known to undergo moderate neurodegenerative alterations during normal aging and severe atrophy in Alzheimer's disease (AD). It has been suggested that functional and structural alterations of the BFCS mediate cognitive performance in normal aging and AD. But, it is still unclear to what extend age-associated cognitive decline can be related to BFCS in normal aging. We analyzed the relationship between BFCS volume and cognition using MRI and a comprehensive neuropsychological test battery in a cohort of 43 healthy elderly subjects spanning the age range from 60 to 85 years. Most notably, we found significant associations between general intell…

TelencephalonMaleAgingCognitive NeuroscienceIntelligenceExperimental and Cognitive PsychologyNeuropsychological TestsNucleus basalisWhite matterCohort StudiesBehavioral NeuroscienceExecutive FunctionAtrophyCognitionMemorymedicineHumansAttentionEffects of sleep deprivation on cognitive performanceddc:610Cognitive declineAgedAged 80 and overIntelligence TestsBasal forebrainmedicine.diagnostic_testCognitionNeuropsychological testOrgan SizeMiddle Agedmedicine.diseaseMagnetic Resonance Imagingmedicine.anatomical_structureLinear ModelsEducational StatusFemaleanatomy & histology [Telencephalon]PsychologyNeuroscience
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Accuracy and Completeness of Drug Information in Wikipedia: A Comparison with Standard Textbooks of Pharmacology

2014

The online resource Wikipedia is increasingly used by students for knowledge acquisition and learning. However, the lack of a formal editorial review and the heterogeneous expertise of contributors often results in skepticism by educators whether Wikipedia should be recommended to students as an information source. In this study we systematically analyzed the accuracy and completeness of drug information in the German and English language versions of Wikipedia in comparison to standard textbooks of pharmacology. In addition, references, revision history and readability were evaluated. Analysis of readability was performed using the Amstad readability index and the Erste Wiener Sachtextforme…

Textbooks as TopicInformation DisseminationMEDLINESocial Scienceslcsh:Medicine-PharmacologyEducationGermanSociologyMedizinische FakultätGermanyHumansMedicineTextbooks as TopicMass Mediaddc:610lcsh:ScienceLanguageInternetTextbooksMultidisciplinaryConsumer Health InformationInformation Disseminationbusiness.industrylcsh:RReproducibility of ResultsOnline EncyclopediasKnowledge acquisitionCommunicationsReadabilitylanguage.human_languageTeaching MethodsIndex (publishing)Drug Information ServicesPharmacology ClinicallanguageInformation sourceEncyclopediaslcsh:QbusinessResearch ArticlePLoS ONE
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Elucidating Gating Effects for Hydrogen Sorption in MFU-4-Type Triazolate-Based Metal-Organic Frameworks Featuring Different Pore Sizes

2011

A highly porous member of isoreticular MFU-4-type frameworks, [Zn(5)Cl(4)(BTDD)(3)] (MFU-4l(arge)) (H(2)-BTDD=bis(1H-1,2,3-triazolo[4,5-b],[4',5'-i])dibenzo[1,4]dioxin), has been synthesized using ZnCl(2) and H(2)-BTDD in N,N-dimethylformamide as a solvent. MFU-4l represents the first example of MFU-4-type frameworks featuring large pore apertures of 9.1 Å. Here, MFU-4l serves as a reference compound to evaluate the origin of unique and specific gas-sorption properties of MFU-4, reported previously. The latter framework features narrow-sized pores of 2.5 Å that allow passage of sufficiently small molecules only (such as hydrogen or water), whereas molecules with larger kinetic diameters (e.…

Thermogravimetric analysisHydrogenChemistryThermal desorption spectroscopythermal desorption spectroscopyOrganic ChemistryInorganic chemistrytriazolateschemistry.chemical_elementGeneral ChemistryCrystal structureCatalysisadsorption; hydrogen; metal-organic frameworks; thermal desorption spectroscopy; triazolatesAdsorptionadsorptionhydrogenDesorptionPhysical chemistryddc:530Metal-organic frameworkmetal-organic frameworksPowder diffractionChemistry - A European Journal
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Comparison of Permeation Measurements and Hybrid Density Functional Calculations on Oxygen Vacancy Transport in Complex Perovskite Oxides

2014

The oxygen vacancy (VO••) formation enthalpy (ΔHF) was determined from the effective activation energies obtained in the permeation measurements on a series of solid solutions La0.98–xSrxCo0.2Fe0.8O3−δ (x = 0.125–0.8) and compared with the results of ab initio calculations at finite temperatures based on the hybrid (PBE0) and GGA+U calculations, as well as previous thermogravimetric experiments. The Mulliken atomic charges, magnetic moments, and the Fe-VO•• and Sr-VO•• distances are analyzed. The strong dependence of formation enthalpy of VO•• on the Fe oxidation state due to variation in Sr and VO•• concentrations is discussed.

Thermogravimetric analysisMagnetic momentChemistryEnthalpy02 engineering and technologyPermeation010402 general chemistry021001 nanoscience & nanotechnology01 natural sciences7. Clean energy0104 chemical sciencesSurfaces Coatings and FilmsElectronic Optical and Magnetic MaterialsGeneral EnergyOxidation stateAb initio quantum chemistry methodsddc:540Physical chemistryPhysical and Theoretical Chemistry0210 nano-technologyPerovskite (structure)Solid solution
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Charge transfer interactions in self-assembled single walled carbon nanotubes/Dawson–Wells polyoxometalate hybrids

2014

We demonstrate the success in self-assembling pyrene-modified Dawson–Wells-type polyoxometalates (POMs) with single walled carbon nanotubes (SWCNTs) by means of π–π interactions. In this context, the immobilization of POMs onto SWCNTs is corroborated by aberration-corrected high-resolution electron microscopy, thermogravimetric analysis, and Raman spectroscopy. From steady-state and time-resolved photophysical techniques we derived evidence for mutual interactions between SWCNTs and POMs in the excited states. The latter are the inception to a charge transfer from the SWCNTs to the POMs. Our results corroborate the suitability of POM–SWCNTs assemblies for photoactive molecular devices.

Thermogravimetric analysisMaterials scienceContext (language use)Nanotechnology-02 engineering and technologyCarbon nanotube010402 general chemistry01 natural scienceslaw.inventionSelf assembledsymbols.namesakelaw[CHIM]Chemical SciencesComputingMilieux_MISCELLANEOUSCharge (physics)General ChemistryNaturwissenschaftliche Fakultät021001 nanoscience & nanotechnology0104 chemical sciencesChemical engineeringExcited stateddc:540Polyoxometalatesymbols0210 nano-technologyRaman spectroscopy
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Alkoxide-intercalated NiFe-layered double hydroxides magnetic nanosheets as efficient water oxidation electrocatalysts

2016

Alkoxide-intercalated NiFe-layered double hydroxides were synthesized via the nonaqueous methanolic route. These nanoplatelets exhibit high crystalline quality as demonstrated by atomic resolution scanning transmission electron microscopy combined with electron energy-loss spectroscopy. Moreover, the presence of the alkoxide moieties has been unambiguously demonstrated by means of thermogravimetric analysis coupled to a mass spectrometer. These NiFe-LDHs can be exfoliated in water or organic solvents and processed into homogeneous ultra-thin films (< 3nm thick) with the assistance of O2-plasma. The study of their behaviour as water oxidation electrocatalysts has shown an outstanding perf…

Thermogravimetric analysisMaterials scienceFOS: Physical sciences-02 engineering and technologyOverpotentialengineering.material010402 general chemistryMass spectrometry01 natural sciencesInorganic Chemistrychemistry.chemical_compoundPhysics - Chemical PhysicsScanning transmission electron microscopySpectroscopyChemical Physics (physics.chem-ph)Condensed Matter - Materials ScienceTafel equationLayered double hydroxidesMaterials Science (cond-mat.mtrl-sci)Naturwissenschaftliche Fakultät021001 nanoscience & nanotechnology0104 chemical sciencesChemical engineeringchemistryddc:540Alkoxideengineering0210 nano-technologyInorganic Chemistry Frontiers
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Straightforward preparation of highly loaded MWCNT-polyamine hybrids and their application in catalysis

2020

Multiwalled carbon nanotubes (MWCNTs) were easily and efficiently functionalised with highly cross-linked polyamines. The radical polymerisation of two bis-vinylimidazolium salts in the presence of pristine MWCNTs and azobisisobutyronitrile (AIBN) as a radical initiator led to the formation of materials with a high functionalisation degree. The subsequent treatment with sodium borohydride gave rise to the reduction of imidazolium moieties with the concomitant formation of secondary and tertiary amino groups. The obtained materials were characterised by thermogravimetric analysis (TGA), elemental analysis, solid state 13C-NMR, Fourier-transform infrared spectroscopy (FT-IR), transmission ele…

Thermogravimetric analysisNitroaldol reactionPotentiometric titrationHeterogeneous Catalysis Carbon nanotubes Ionic Liquids Green Chemistry AminesBioengineering02 engineering and technology010402 general chemistry01 natural sciencesCatalysischemistry.chemical_compoundSodium borohydridePolymer chemistryGeneral Materials ScienceGeneral EngineeringAzobisisobutyronitrileGeneral ChemistrySettore CHIM/06 - Chimica OrganicaMWCNT-polyamine hybrids021001 nanoscience & nanotechnologyAtomic and Molecular Physics and Optics0104 chemical scienceschemistryddc:540Radical initiatorKnoevenagel condensation0210 nano-technologyddc:546
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Interface Amorphization of Two‐Dimensional Black Phosphorus upon Treatment with Diazonium Salts

2021

Abstract Two‐dimensional (2D) black phosphorus (BP) represents one of the most appealing 2D materials due to its electronic, optical, and chemical properties. Many strategies have been pursued to face its environmental instability, covalent functionalization being one of the most promising. However, the extremely low functionalization degrees and the limitations in proving the nature of the covalent functionalization still represent challenges in many of these sheet architectures reported to date. Here we shine light on the structural evolution of 2D‐BP upon the addition of electrophilic diazonium salts. We demonstrated the absence of covalent functionalization in both the neutral and the r…

Thermogravimetric analysisred phosphoruschemistry.chemical_element010402 general chemistryPhotochemistryMass spectrometryblack phosphorus01 natural sciencesCatalysislaw.inventionsymbols.namesakeX-ray photoelectron spectroscopylawElectron paramagnetic resonanceMaterialsFull Paper010405 organic chemistryChemistryPhosphorusOrganic ChemistryBalz–Schiemann productGeneral ChemistryQuímicaFull Paperssacrificial catalysts6. Clean waterMaterials Science | Hot Paperamorphization0104 chemical sciencesElectrophilesymbolsSurface modificationRaman spectroscopyddc:547Chemistry – A European Journal
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Childhood cancer survival in Europe 1999-2007: results of EUROCARE-5-a population-based study.

2014

To access publisher's full text version of this article. Please click on the hyperlink in Additional Links field. Survival and cure rates for childhood cancers in Europe have greatly improved over the past 40 years and are mostly good, although not in all European countries. The EUROCARE-5 survival study estimates survival of children diagnosed with cancer between 2000 and 2007, assesses whether survival differences among European countries have changed, and investigates changes from 1999 to 2007. We analysed survival data for 157,499 children (age 0-14 years) diagnosed between Jan 1, 1978 and Dec 31, 2007. They came from 74 population-based cancer registries in 29 countries. We calculated …

Time FactorsAdolescentPopulationChildhood cancerMEDLINEBörnNOmedicineChildhood cancer survivalHumansUnglingarChildeducationddc:613Krabbameinchildhood cancer; Europe; EUROCARE-5Ungbörneducation.field_of_studybusiness.industryHazard ratioConfoundingInfant NewbornInfantCancermedicine.diseaseEuropeEastern europeanInstitutional repositoryOncologyChild PreschoolNýburarsense organsNeoplasms/mortalityNeoplasms/mortality*businessDemography
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Non-cross-linked collagen type I/III materials enhance cell proliferation: in vitro and in vivo evidence

2014

Objective: To analyze Mucograft®(MG), a recently introduced collagen matrix, in vitro and in vivo, and compare it with BioGide®(BG), a well-established collagen membrane, as control. Material and Methods: A detailed analysis of the materials surface and ultra-structure was performed. Cellular growth patterns and proliferation rates of human fibroblasts on MG and BG were analyzed in vitro. In addition, the early tissue reaction of CD-1 mouse to these materials was analyzed by means of histological and histomorphometrical analysis. Results: MG showed a three-fold higher thickness both in dry and wet conditions, when compared to BG. The spongy surface of BG significantly differed from that of …

Time FactorsCell SurvivalSurface PropertiesCellBiocompatible MaterialsMatrix (biology)BiologyPeripheral blood mononuclear cellCollagen Type IIIMiceRandom AllocationCollagen type IIn vivoMaterials TestingmedicineAnimalsHumansddc:610Bone regenerationGeneral DentistryCells CulturedCell ProliferationGuided tissue regenerationCell growthReproducibility of ResultsAnatomyOriginal ArticlesFibroblastsCollagen type IIIMolecular biologyImmunohistochemistryIn vitroBone regenerationlcsh:RK1-715medicine.anatomical_structurelcsh:DentistryFemaleCollagenJournal of Applied Oral Science
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