Search results for "hardness"
showing 10 items of 160 documents
Influence of Post-machining Thermal Treatment on the Corrosion Behaviour of Copper
2014
Abstract In this paper, the influence of a post-machining thermal treatment (PMTT) on the corrosion behaviour of copper was investigated in a salt fog atmosphere. The corrosion behaviour was affected by the presence of a high density of grain boundaries generated during machining or dislocations formed during PMTT under certain conditions. The obtained results showed that it is possible to find PMTT conditions to cancel changes induced by machining and that the critical factor leading to a sharp increase of the percentage of oxidized surface seems to be the density of dislocations near the machined surface.
Aluminum oxide from trimethylaluminum and water by atomic layer deposition:The temperature dependence of residual stress, elastic modulus, hardness a…
2014
Use of atomic layer deposition (ALD) in microelectromechanical systems (MEMS) has increased as ALD enables conformal growth on 3-dimensional structures at relatively low temperatures. For MEMS device design and fabrication, the understanding of stress and mechanical properties such as elastic modulus, hardness and adhesion of thin film is crucial. In this work a comprehensive characterization of the stress, elastic modulus, hardness and adhesion of ALD aluminum oxide (Al2O3) films grown at 110-300 C from trimethylaluminum and water is presented. Film stress was analyzed by wafer curvature measurements, elastic modulus by nanoindentation and surface-acoustic wave measurements, hardness by na…
ε-Regularized two-level optimization problems: Approximation and existence results
2006
The purpose of this work is to improve some results given in [12], relating to approximate solutions for two-level optimization problems. By considering an e-regularized problem, we get new properties, under convexity assumptions in the lower level problems. In particular, we prove existence results for the solutions to the e-regularized problem, whereas the initial two-level optimization problem may fail to have a solution. Finally, as an example, we consider an approximation method with interior penalty functions.
Tribological properties of commercial optical disks estimated from nanoindentation and scratch techniques
2007
Abstract The structure of optical disks is a complex superposition of several layers with different objectives. The most external layer is usually designed with a protective purpose. When the scratch of the substrate occurs, the optical properties of the device decrease inducing a deficiency in the storage or access of data. Nowadays, the latest commercial optical disks exhibit protective coatings made of polymeric materials (copolymers, and polymeric matrix composite materials). The efficiency of these layers depends on a combination of several mechanical properties like hardness and Young's modulus. In this work, a compositional and mechanical study was carried out on four commercial opti…
Remineralization effects of conventional and experimental ion-releasing materials in chemically or bacterially-induced dentin caries lesions
2019
Abstract Objectives The aim of this study was to evaluate the remineralization effects of conventional and experimental ion-releasing materials on different artificial dentin carious lesions. Methods Forty human dentin discs were submitted to different demineralization protocols for simulated caries lesion: (D1) Shallow chemically-induced caries, (D2) deep chemically-induced caries, (D3) deep bacterially-induced caries. Each disc was divided in five parts; one of those served as baseline control. The remaining parts of each disc (n = 12–16/group) were treated using the following materials: EXP, an experimental resin-based bioactive material consisting of a self-etch primer and an adhesive c…
PETTERDITE, THE Cr-DOMINANT ANALOGUE OF DUNDASITE, A NEW MINERAL SPECIES FROM DUNDAS, TASMANIA, AUSTRALIA AND CALLENBERG, SAXONY, GERMANY
2000
Petterdite is a newly discovered hydrated lead chromium hydroxyl carbonate, the Cr 3+ -dominant analogue of dundasite, with a formula PbCr 2 (CO 3 ) 2 (OH) 4 ·H 2 O. The type locality is the Red Lead mine, on the Zeehan–Dundas mining field in northwestern Tasmania, Australia. The mineral also occurs in small amounts at the Callenberg nickel deposit, Saxony, Germany. Petterdite forms thin crusts made up of tiny platy crystals up to about 15 μm across, associated with crocoite and anglesite at the type locality, and with crocoite, cerussite, bindheimite, pyromorphite, and relict galena at Callenberg. The petterdite crusts are pale greyish to pinkish violet and non-fluorescent; they have an ea…
Mechanical Properties of Pore-Spanning Lipid Bilayers Probed by Atomic Force Microscopy
2006
AbstractWe measure the elastic response of a free-standing lipid membrane to a local indentation by using an atomic force microscope. Starting point is a planar gold-coated alumina substrate with a chemisorbed 3-mercaptopropionic acid monolayer displaying circular pores of very well defined and tunable size, over which bilayers composed of N,N,-dimethyl-N,N,-dioctadecylammonium bromide or 1,2-dioleoyl-3-trimethylammonium-propane chloride were spread. Centrally indenting these “nanodrums” with an atomic force microscope tip yields force-indentation curves, which we quantitatively analyze by solving the corresponding shape equations of continuum curvature elasticity. Since the measured respon…
Reduction of Polymerization Shrinkage Stress and Marginal Microleakage Using Soft-Start Polymerization
2003
Purpose: This study evaluated the influence of a soft-start light-curing exposure on polymerization shrinkage stress and marginal integrity of adhesive restorations. Materials and Methods: Six resin-based composites (Pertac II, Tetric Ceram, Definite, Surefil, Solitaire, and Visio-Molar) were adhesively bonded to a cylindrical cavity (n = 9 per material/light) in a photoelastic material. Visible light-curing was applied using either the standard polymerization mode (800 mW/cm2 exposure duration 40 s) of the curing light (Elipar TriLight, 3M ESPE) or the exponential mode from the same device (ramp-curing: 150 mW/cm2 to 800 mW/cm2 within the first 15 s of a total curing time of 40 s). Polymer…
Effects of elevated hydrogen peroxide 'strip' bleaching on surface and subsurface enamel including subsurface histomorphology, micro-chemical composi…
2007
Abstract Objectives This study examined the effects of elevated concentration hydrogen peroxide tooth whitening treatments on tooth surface and subsurface integrity. Methods Sound human molars were ground and polished to prepare an uniform substrate for bleaching treatments. A cycling treatment included alternating ex vivo human salivary exposures with bleaching treatments under conditions of controlled temperature and durations of treatment. Bleaching was carried out with prototype bleaching strips containing hydrogen peroxide gel at 13% and 16% concentrations. A non-bleached group was used as a control. Treatments included 28 h of total bleaching exposure in vitro . Surface color was meas…
Phenomenological approach to compare the crystallization kinetics of isotactic polypropylene and polyamide-6 under pressure
2001
Reliable experimental data for semicrystalline polymers crystallized under pressure are supplied on the basis of a model experiment in which drastic solidification conditions are applied. The influence of the pressure and cooling rate on some properties, such as the density and microhardness, and on the product morphology, as investigated with wide-angle X-ray scattering (WAXS), is stressed. Results for isotactic polypropylene (iPP) samples display a lower density and a lower microhardness with increasing pressure over a wide range of cooling rates (from 0.01 to 20 °C/s). Polyamide-6 (PA6) samples exhibit the opposite behavior, with the density and microhardness increasing at higher pressur…