Search results for "reparation"
showing 10 items of 944 documents
Effect of cavity preparation instruments (oscillating or rotating) on the composite-dentin interface in primary teeth.
2003
Abstract Objectives: To evaluate the effect of preparation of instruments on the interfacial integrity between cavity wall and composite restoration. Methods: Two class II slot preparations were done in 10 primary teeth either with SonicSys® or with a conventional bur. The cavities were filled using an adhesive system. One layer of a flowable composite and one layer of a condensable composite were applied. The specimens were analyzed by confocal laser scanning microscopy. Results: In the SonicSys® group the mean thickness of the hybrid layer was 6.12 (0.60) μm; in the control group it was 6.04 (0.63) μm. The difference was not statistically significant. Two fractures were observed in one to…
Shear bond strength of orthodontic metal brackets to aged composite using three primers
2017
Background This study aimed to assess the effect of surface preparation with sandblasting and diamond bur along with the use of three primers on shear bond strength (SBS) of metal brackets to aged composite. Material and methods In this in vitro, experimental study, 60 Filtek Z250 composite discs were fabricated (10×2mm), immersed in distilled water for 24 hours and subjected to 5000 thermal cycles. They were randomly divided into two groups (n=30) of sandblasting with aluminum oxide particles for 10 seconds and surface roughening with bur. Each group was randomly divided into three subgroups (n=10) for use of Transbond XT, Assure Plus and Composite Primer. Metal brackets were bonded and th…
Influence of cavity preparation technique (rotary vs. ultrasonic) on microleakage and marginal fit of six end-root filling materials
2010
Objectives: To evaluate in vitro the effect of cavity preparation with microburs and diamond-coated ultrasonic tips on the microleakage and marginal fit of six end-root filling materials. Study Design. The following materials were assessed: amalgam (Amalcap), zinc oxide eugenol (IRM), glass ionomer (Vitrebond), compomer (Cavalite), mineral particle aggregate (MTA) and composite (Clearfil). Cavity preparation was performed with microburs or diamond ultrasonic tips in single-root teeth. The seal was evaluated in two experiments: a microleakage assay on the passage of dye to the interface; and a scanning electron microscopy study and analysis of epoxy resin replicas, measuring the size of gaps…
Spark plasma sintering of cobalt ferrite nanopowders prepared by coprecipitation and hydrothermal synthesis.
2007
International audience; Cobalt ferrite exhibits a high coercivity at room temperature and a strong magnetic anisotropy compared to the other spinel ferrites and, consequently appears as an interesting material for permanent magnets and high-density recording. The magnetic properties depend also on the crystallite size. In order to keep the powder properties in a bulk material, dense nanostructured cobalt ferrite has to be sintered. A field activated sintering process like spark plasma sintering (SPS) may be promising for such challenge. The present paper deals with: (i) the preparation of cobalt ferrite by two methods: coprecipitation and hydrothermal synthesis in supercritical water; (ii) …
Large scale synthesis of nanostructured zirconia-based compounds from freeze-dried precursors
2013
Nanocrystalline zirconia powders have been obtained at the multigram scale by thermal decomposition of precursors resulting from the freeze-drying of aqueous acetic solutions. This technique has equally made possible to synthesize a variety of nanostructured yttria or scandia doped zirconia compositions. SEM images, as well as the analysis of the XRD patterns, show the nanoparticulated character of those solids obtained at low temperature, with typical particle size in the 10–15 nm range when prepared at 673 K. The presence of the monoclinic, the tetragonal or both phases depends on the temperature of the thermal treatment, the doping concentration and the nature of the dopant. In addition,…
Spray-Drying, Solvent-Casting and Freeze-Drying Techniques: a Comparative Study on their Suitability for the Enhancement of Drug Dissolution Rates.
2019
Purpose Solid dispersions (SDs) represent the most common formulation technique used to increase the dissolution rate of a drug. In this work, the three most common methods used to prepare SDs, namely spray-drying, solvent-casting and freezedrying, have been compared in order to investigate their effect on increasing drug dissolution rate. Methods Three formulation strategies were used to prepare a polymer mixture of polyvinyl-alcohol (PVA) and maltodextrin (MDX) as SDs loaded with the following three model drugs, all of which possess a poor solubility: Olanzapine, Dexamethasone, and Triamcinolone acetonide. The SDs obtained were analysed and compared in terms of drug particle size, drug-lo…
LbL multilayer capsules: recent progress and future outlook for their use in life sciences.
2010
In this review we provide an overview of the recent progress in designing composite polymer capsules based on the Layer-by-Layer (LbL) technology demonstrated so far in material science, focusing on their potential applications in medicine, drug delivery and catalysis. The benefits and limits of current systems are discussed and the perspectives on emerging strategies for designing novel classes of therapeutic vehicles are highlighted. © 2010 The Royal Society of Chemistry.
Exfoliation of Alpha-Germanium: A Covalent Diamond-Like Structure
2021
2D materials have opened a new field in materials science with outstanding scientific and technological impact. A largely explored route for the preparation of 2D materials is the exfoliation of layered crystals with weak forces between their layers. However, its application to covalent crystals remains elusive. Herein, a further step is taken by introducing the exfoliation of germanium, a narrow-bandgap semiconductor presenting a 3D diamond-like structure with strong covalent bonds. Pure α-germanium is exfoliated following a simple one-step procedure assisted by wet ball-milling, allowing gram-scale fabrication of high-quality layers with large lateral dimensions and nanometer thicknesses.…
Smart composite films of nanometric thickness based on copper-iodine coordination polymers. Toward sensors.
2018
One-pot reactions between CuI and methyl or methyl 2-amino-isonicotinate give rise to the formation of two coordination polymers (CPs) based on double zig-zag Cu2I2 chains. The presence of a NH2 group in the isonicotinate ligand produces different supramolecular interactions affecting the Cu-Cu distances and symmetry of the Cu2I2 chains. These structural variations significantly modulate their physical properties. Thus, both CPs are semiconductors and also show reversible thermo/mechanoluminescence. X-ray diffraction studies carried out under different temperature and pressure conditions in combination with theoretical calculations have been used to rationalize the multi-stimuli-responsive …
Monolayers and Langmuir-Blodgett Multilayers of Discotic Liquid Crystals?
2008
The field of monolayer and multilayer films of discotic LCs is at its very beginning. The scope and limitations of this preparation method have not yet been explored, and little is known about the structures obtainable. However, the potential access to extraordinary, ordered thin films is fascinating, and will stimulate research in the future.