Search results for "scanning"

Mapping electron-beam-injected trapped charge with scattering scanning near-field optical microscopy.

2016

Scattering scanning near-field optical microscopy (s-SNOM) has been demonstrated as a valuable tool for mapping the optical and optoelectronic properties of materials with nanoscale resolution. Here we report experimental evidence that trapped electric charges injected by an electron beam at the surface of dielectric samples affect the sample-dipole interaction, which has direct impact on the s-SNOM image content. Nanoscale mapping of the surface trapped charge holds significant potential for the precise tailoring of the electrostatic properties of dielectric and semiconductive samples, such as hydroxyapatite, which has particular importance with respect to biomedical applications. The meth…

Determination of the porosity, permeability and diffusivity of rock in the excavation-disturbed zone around full-scale deposition holes using the -PM…

1998

Abstract Three experimental holes the size of deposition holes in a KBS-3 type repository (depth 7.5 m and diameter 1.5 m) were bored in hard granitic rock in the Research Tunnel at Olkiluoto to study, among other things, the properties of the rock in the excavation-disturbed zone. In the analysis described in this report, the porosities, effective diffusivities and permeabilities of disturbed and intact rock were determined by using two novel methods: the 14 C -polymethylmethacrylate method and the He-gas method. In addition, the structure of the rock in the excavation-disturbed zone was assessed using both scanning electron and optical microscopy.

Imaging of Located Buried Defects in Metal Samples by an Scanning Microwave Microscopy

2011

Abstract A non-destructive method is proposed to detect the located buried defects using scanning microwave microscopy. Based on the “skin effect”, our recent developments authorize 3D tomography with nanometric resolution. This technique associates the electromagnetic microwave measurement using a Vector Network Analyzer (VNA) with the nanometer-resolution positioning capabilities of an Atomic Force Microscope. At each used frequency, an incident electromagnetic wave is send to the sample and the reflected wave gives information on a specific depth layer in the material. With a large bandwidth of frequencies, a 3D tomography is allowed inside the material. With characteristic tools of nano…

<title>Scanning probe microscopy of nanocrystalline iridium oxide thin films</title>

2003

Structural investigations of nanocrystalline iridium oxide thin films, prepared by dc magnetron sputtering technique were performed by scanning probe microscopy (SPM). SPM studies, using both atomic force microscopy (AFM) and scanning tunnelling microscopy (STM), indicate that the thin films are composed of grains with a size of about 20-50 nm. Fine crystallinity and small RMS microroughness of the films, being well below 2 nm, make iridium oxide thin films promising candidates for nanolithographic applications. The possibility to perform nanolithograhpic processes at a scale of less than 150 nm was successfully examined in AFM and STM modes.© (2003) COPYRIGHT SPIE--The International Societ…

Watching Ions Move: Scanning Probe Microscopy on Perovskite Solar Cells

2018

Field-induced tip–sample oxygen transfer in scanning tunneling microscopy on TiO2(110) (1 1).

2008

International audience; A study on the field-induced tip–surface oxygen transfer at room temperature and its influence on the tunneling conditions for stable STM imaging of the TiO2(110) (1 1) surface is reported. A simple model of field-induced transfer is applied to tungsten and platinum–iridium tips. The oxygen transition rates from the sample to the tip or from the tip to the sample depend on the oxygen desorption barriers formed at tunneling distance. For stable imaging the applied bias voltage has to balance the oxygen transfer probabilities in both directions. In the case of Pt/Ir tips, the tunneling conditions for images with clear evidence of bridging oxygen point defects have been…

Effect of Impregnation and Activation Conditions of Al2O3/CuO Supported Monolith Catalysts in the Reduction of NO

1979

Reduction of NO in the presence of CO and Ar was examined on two series of monolithic sheets carrying an active CuO/Al 2 O 3 layer. In the impregnation procedure the ratio of Al 2 O 3 to CuO was varied in a wide range. The texture of the layer and the dispersion of CuO therein was controlled by mercury porosimetry, scanning electron microscopy and secondary ion mass spectrometry (SIMS). It could be established that the surface concentration of CuO determined by SIMS measurements is the most decisive quantity of the catalyst correlating linearly with the conversion of NO.

Characterization ofBacillus thuringiensisserovarbolivia(serotype H63), a novel serovar isolated from the Bolivian high valleys

1999

The type strain Bacillus thuringiensis var. bolivia (serotype H63), isolated from the Bolivian high valleys, has been characterized at different levels. Its parasporal crystal has an unusual shape and it is composed of a protein of 155 kDa which shows two bands of 75 and 80 kDa after activation. Analysis by PCR shows the presence of cry1 genes, and amplification with specific primers gave products for cry1 E, cry1 D, cry4 A and cry4 B with sizes different to those expected. Immunoblotting tests showed positive reaction for Cry1 E, Cry3 A, Cry4 A and Cry11 A crystal proteins. The plasmid pattern revealed two large and two small plasmids. Toxicity tests were performed against 14 insects and a…

Leaf epicuticular waxes effects egg parasitoid’s response to host adult footprint contact kairomone

2009

Chemical footprints left behind by true bugs are perceived as a contact kairomones by scelionid egg parasitoids. In the system Nezara viridula and its egg parasitoid Trissolcus basalis, previous studies have shown that the kairomone mediating such behavior is part of N. viridula’s cuticular hydrocarbons. In this study, the effect of epicuticular waxes of leaves of broad bean, Vicia faba, on wasp response to footprints of N. viridula females are investigated. Plants with intact waxes layer were used (1) without host chemical contamination, or (2) contaminated by host female footprints. Mechanically de-waxed plants were tested (3) without host chemical contamination, or (4) de-waxed a few min…

Microscopic findings and soil genetic “indicators” in support of pedoarchaeological studies

2015

Archaeologists use historical artefacts and archaeological records to reconstruct the communities that produced them and the environment in which they lived. Soil protects our buried or damaged heritage of archaeological and historic remains from depletion, damage, and any disturbance. Here are presented some preliminary results obtained in the framework of the FP7 Project "MEditerranean MOntainous LAndscapes: an historical approach to cultural Heritage based on traditional agrosystems (MEMOLA)" where ancient soils horizons are themselves archaeological records. In order to implement the MEMOLA archaeological study and to identify soil genetic "indicators", two integrated approaches were us…