Search results for "scanning"

New amphiphilic terphenyl liquid crystals for the preparation of highly ordered ultrathin films

1991

Four new amphiphilic liquid crystals have been synthesized, in which terphenyl was used as the mesogenic unit. In order to enable the formation of Langmuir Monolayers at the air/water-interface, the molecules were equipped with slightly polar headgroups such as esters or a carboxylic acid group. All compounds can be transferred onto solid substrates. In addition, it is possible to prepare freely suspended films of at least one compound in the temperature range of the smectic phases. The phases of the different states, bulk, monolayer, freely suspended film, and Langmuir-Blodgett multilayers have been investigated by means of monolayer isotherms, optical textures, differential scanning calor…

A novel magnetic Preyssler acid grafted chitosan nano adsorbent: synthesis, characterization and adsorption activity

2015

BACKGROUND This study concerns the application of magnetic heteropolyacids composite for the adsorption of organic compounds from aqueous solutions. A novel magnetic Preyssler/chitosan/Fe3O4 nanoparticles composite (PCNF) adsorbent was designed using a one-pot synthesis method and characterized by multiple techniques including X-ray powder diffraction (XRD), infrared spectroscopy (FT-IR), N2 adsorption–desorption isotherms and scanning electron microscopy (SEM). RESULTS The adsorption activity of PCNF was evaluated by the removal of methyl orange (as an anionic azo dye model, MO) from aqueous solution and all the factors influencing the removal efficiency, such as adsorbent dosage, initial …

Template electrosynthesis of La(OH)3 and Nd(OH)3 nanowires using porous anodic alumina membranes

2007

High quality arrays of Ln(OH)3 (Ln = La, Nd) nanowires have been successfully fabricated for the first time by an electrochemical process using anodic alumina membrane templates. A physico-chemical characterisation of electrodeposited hydroxides has been carried out by different techniques (XRD, SEM and EDX). The results show that the synthesized nanostructures are crystalline, dense, continuous, well aligned, and with high aspect ratio, suggesting further development of possible applications in the lanthanide family species. Keywords: Nanowires, Anodic alumina membranes, Hydroxide electrodeposition, Template, Lanthanide compounds

The application of neutron activation analysis, scanning electron microscope, and radiographic imaging for the characterization of electrochemically …

2008

Lanthanide and actinide targets are prepared at the University of Mainz by molecular plating, an electrochemical deposition from an organic solvent, for heavy-ion reaction studies at GSI. To acquire information about deposition yield, target thickness, and target homogeneity, the following analysis methods are applied. With neutron activation analysis (NAA) the deposition yield and the average thickness of the deposited material is determined. We report on the analytical procedure of NAA performed subsequent to the molecular plating process. Scanning electron microscope (SEM) is used to determine the morphology of the target surfaces. In combination with energy dispersive X-ray spectrometer…

Bedeutung der Ganzkörper-Skelettszintigraphie im Rahmen des Staging von Malignomen im HNO-Bereich*

1992

Concerning malignant tumours of the oral cavity, pharynx and larynx, bone metastases are in general rarely seen. For the specification to which patients the whole body bone scintigraphy as detection method should be applied, the findings of 370 patients were analysed retrospectively. In respect of primary staging, bone metastases could be found by scintigraphy in only 1.4% of the patients. On the other hand, there was a detection rate of 12% during the further course of the disease, especially in case of clinical symptoms pointing at spreading metastases or in tumour recurrences. Nevertheless, positive scan findings which were not due to metastases could be found in both groups with equal f…

Measure of a limestone weathering degree using Laser Scanner.

2013

The weathering degree of the building materials and natural stones is generally quantified as the decrement of some mechanical features that can be measured experimentally by means of compressive tests or point load tests in the laboratory or Schmidt hammer tests carried out in situ. Such destructive or damaging tests are unacceptable in case of cultural heritage since even small amounts of damage must be avoided. This work shows a correlation between Schmidt hammer rebound values and the reflectivity that is detected by means of terrestrial scanner laser; therefore it allows assessing the weathering degree of buildings or stones in situ. The results demonstrate that such an investigation c…

Testing direct neuroprotective effects of current MS therapeutic compounds with intravital two photon laser scanning microscopy

2014

Characterization of laser ablation of copper in the irradiance regime of laser-induced breakdown spectroscopy analysis

2014

Abstract The LIBS signal depends both on the ablated mass and on the plasma excitation temperature. These fundamental parameters depend in a complex manner on laser ablation and on laser–plasma coupling. As several works in the literature suggest that laser ablation processes play a predominant role compared to plasma heating phenomena in the LIBS signal variations, this paper focuses on the study of laser ablation. The objective was to determine an interaction regime enabling to maximally control the laser ablation. Nanosecond laser ablation of copper at 266 nm was characterized by scanning electron microscopy and optical profilometry analysis, in air at 1 bar and in the vacuum. The laser …

AR METHODS FOR THE VISUALIZATION OF THE LOST MARBLE “TRIBUNA” IN THE MAIN APSE OF THE CATHEDRAL OF PALERMO

2022

Abstract. In recent years research works have shown that augmented reality tools can offer effective support for the dissemination of architectural heritage, when integrated into the information data extracted with surveying and representation tools and further data from other sources, e.g., history.The development and permanent updating of software platforms dedicated to augmented reality, i.e., Apple's ARKit and Google's ARCore, as well as the introduction of new features, offer today affordable support for the development of AR solutions.Some operational difficulties are due to the rapid and constant evolution of the technologies; the available solutions can be compared to prototypes and…

Integrated surveying techniques in cultural heritage documentation

2007

This paper is focused on integration between laser scanning data, CAD modelling and photogrammetric data collected during the survey of one façade of the monument called “Quattro Canti” in the historic centre of Palermo. The investigation has been directed to the production of a 3D photorealistic model of the monument. The “Quattro Canti” monument is formed by four cylindrical façades facing the square where the older streets of Palermo intersect; each façade has a symbolic reference to one of the seasons and is divided in four levels. The façade called “Canto dell’Autunno” has been surveyed both with laser scanning and with photogrammetric techniques. Laser scanning data have been collecte…