Search results for "scatter"
showing 10 items of 8475 documents
Structural Characterization of Zirconia Nanoparticles Prepared by Microwave-Hydrothermal Synthesis
2009
Nanocrystalline zirconia powders have been prepared by microwave-hydrothermal synthesis starting from aqueous solution of ZrOCl2·8H2O. Results of investigations on the aqueous suspension stability of the washed zirconia nanopowders by dynamic light scattering showed that the suspension, constituted by superaggregates of nanoparticles (131 ± 10 nm), was stable up to 15 days. Nanopowders were investigated by means of transmission electron microscopy and small angle x-ray scattering measurements which proved that the zirconia nanopowder is constituted by small primary nanoparticles of ca. 8 nm that agglomerate forming bigger aggregates of 50 ± 1 nm.
Static and dynamic light scattering by aqueous polyelectrolyte solutions: effect of molecular weight, charge density and added salt
1990
Abstract Aqueous solutions of quaternized poly(2-vinylpyridine) were investigated by static (SLS) and dynamic (DLS) light scattering over a wide range of polyelectrolyte, c pe , and salt concentrations, c s (10 −3 ≤ c pe ≤ 10 2 gl −1 , 10 −5.5 ≤ c s ≤ 10 −1 moll −1 ). Using DLS the cooperative diffusion coefficient D was measured as a function of c pe and c s . D exhibits a characteristic behaviour in each of three different concentration regimes. In the ‘dilute lattice’ regime, where λ = c pe c s ⪡ 1 , one diffusion coefficient is observed. In the transition regime, where λ ≈ 1, D increases with increasing polyelectrolyte concentration and a slow diffusive mode gradually appears. For λ ⪢ 1…
29Si NMR and Small-Angle X-ray Scattering Studies of the Effect of Alkaline Ions (Li+, Na+, and K+) in Silico-Alkaline Sols
1999
Alkali−silica reactions (ASR) which occur in concrete can be simulated in laboratory by destabilization of silico-alkaline aqueous solutions by addition of calcium ions. The relevant features of the reaction depend on the nature of alkaline ions (Li+, Na+, or K+) and on the silica/alkaline ratios which fix the distribution of the molecular species in the precursor solution. 29Si NMR spectroscopy and small-angle X-ray scattering (SAXS) techniques were used to study the structure and size distribution of molecular and colloidal species in sols with different silica/alkaline molar ratio and several types of alkaline ions. Experimental SAXS curves were simulated using a simple structural model …
Consolidation and protection by nanolime: recent advances for the conservation of the graffiti, Carceri dello Steri Palermo and of the 18th century l…
2014
Abstract Nanolime dispersed in 2-propanol was extensively used for the consolidation of wall paintings. The knowledge of the advances of this methodology dealing with all the possible effects associated with the nanolime new material in conservation is fundamental to assess and improve the technique. In this paper, four different dispersions of Ca(OH) 2 nanoparticles were characterised by Small Angle X-rays Scattering technique (SAXS) and Transmission Electron Microscopy (TEM) in order to achieve information on size, shape, polydispersity, agglomeration, and crystal structure (by SAED patterns) of the particles. Once characterised, the dispersions were tested in two different case studies, …
Quasi-elastic Neutron Scattering Investigation of the Hydrogen Surface Self-Diffusion on Polymer Electrolyte Membrane Fuel Cell Catalyst Support
2008
International audience; Quasi-elastic neutron scattering (QENS) measurements have been performed to investigate the surface selfdiffusion of hydrogen molecules. A monolayer of molecular hydrogen was adsorbed on a carbon material commonly used in polymer electrolyte membrane fuel cells, called XC-72. QENS spectra were recorded at the time-of-flight spectrometer IN5 at Institut Laue-Langevin (ILL) in Grenoble at 40, 50, 60, and 70 K. By using the Chudley & Elliott model for jump diffusion, we found the diffusion coefficient at each temperature. The logarithm of the diffusion coefficient was plotted versus the inverse of the temperature to give the coefficient in the Arrhenius equation. From t…
Beta Decay Studies of Neutron Rich Nuclei Using Total Absorption Gamma-ray Spectroscopy and Delayed Neutron Measurements
2010
International audience; A complete characterisation of the β-decay of neutron-rich nuclei can be obtained from the measurement of β-delayed gamma rays and, whenever the process is energetically possible, β-delayed neutrons. The accurate determination of the β-intensity distribution and the β-delayed neutron emission probability is of great relevance in the fields of reactor technology and nuclear astrophysics. A programme for combined measurements using the total absorption gamma-ray spectroscopy technique and both neutron counters and neutron time-of-flight spectrometers is presented.
Why Have Many of the Brightest Radio-loud Blazars Not Been Detected in Gamma-Rays by Fermi?
2015
We use the complete MOJAVE 1.5 Jy sample of active galactic nuclei (AGNs) to examine the gamma-ray detection statistics of the brightest radio-loud blazars in the northern sky. We find that 23% of these AGNs were not detected above 0.1 GeV by the Fermi-LAT during the four-year 3FGL catalog period partly because of an instrumental selection effect and partly due to their lower Doppler boosting factors. Blazars with synchrotron peaks in their spectral energy distributions located below 10^(13.4) Hz also tend to have high-energy peaks that lie below the 0.1 GeV threshold of the LAT, and are thus less likely to be detected by Fermi. The non-detected AGNs in the 1.5 Jy sample also have significa…
Halo-independent methods for inelastic dark matter scattering
2013
We present halo-independent methods to analyze the results of dark matter direct detection experiments assuming inelastic scattering. We focus on the annual modulation signal reported by DAMA/LIBRA and present three different halo-independent tests. First, we compare it to the upper limit on the unmodulated rate from XENON100 using (a) the trivial requirement that the amplitude of the annual modulation has to be smaller than the bound on the unmodulated rate, and (b) a bound on the annual modulation amplitude based on an expansion in the Earth's velocity. The third test uses the special predictions of the signal shape for inelastic scattering and allows for an internal consistency check of …
VLBA observations of a rare multiple quasar imaging event caused by refraction in the interstellar medium
2013
We report on the first detection of the theoretically-predicted rare phenomenon of multiple parsec-scale imaging of an active galactic nucleus induced by refractive effects due to localized foreground electron density enhancements, e.g., in an AU-scale plasma lens(es) in the ionized component of the Galactic interstellar medium. We detected multiple imaging in the low galactic latitude (b=-2 deg) quasar 2023+335 from the 15.4 GHz MOJAVE observations when the source was undergoing an ESE. While the parsec-scale jet of the source normally extends along PA -20 deg, in the 28 May 2009 and 23 July 2009 images a highly significant multi-component pattern of secondary images is stretched out nearl…
Cosmological analogies in the search for new physics in high-energy collisions
2020
In this paper, analogies between multiparticle production in high-energy collisions and the time evolution of the early universe are discussed. A common explanation is put forward under the assumption of an unconventional early state: a rapidly expanding universe before recombination (last scattering surface), followed by the CMB, later evolving up to present days, versus the formation of hidden/dark states in hadronic collisions followed by a conventional QCD parton shower yielding final-state particles. In particular, long-range angular correlations are considered pointing out deep connections between the two physical cases potentially useful for the discovery of new physics.