Search results for "standards"

showing 10 items of 394 documents

Detection of gamma-hydroxybutyrate in hair: Validation of GC–MS and LC–MS/MS methods and application to a real case

2012

A gas chromatography-mass spectrometry (GC-MS) and a liquid chromatography tandem mass spectrometry (LC-MS/MS) method were validated for quantifying endogenous and exogenous hair concentrations of gamma-hydroxybutyrate (GHB). The GC-MS method is based on overnight extraction of 25 mg hair in NaOH at 56 °C, liquid/liquid extraction in ethylacetate and trimethylsylil derivatization; analysis is by electron ionization and single ion monitoring of three ions. The LC-MS/MS method entails a rapid digestion of 25 mg hair with NaOH at 75 °C for 40 min, liquid/liquid extraction in ethylacetate and reconstitution of the extract in the LC mobile phase; negative ion electrospray ionization and multiple…

AdultMaleQuality ControlSpectrometry Mass Electrospray IonizationSubstance-Related DisordersElectrospray ionizationClinical BiochemistryLiquid-Liquid ExtractionPharmaceutical ScienceAcetatesTandem mass spectrometryMass spectrometryGas Chromatography-Mass SpectrometryAnalytical ChemistryForensic ToxicologySettore MED/43 - Medicina LegaleLiquid chromatography–mass spectrometryLimit of DetectionTandem Mass SpectrometryDrug DiscoveryHumansSodium HydroxideSpectroscopyDetection limitChromatographyChemistryIllicit DrugsSelected reaction monitoringHair Segmental analysis GC–MS LC–MS/MSTemperatureReproducibility of ResultsGamma hydroxybutyrateReference StandardsSubstance Abuse DetectionGamma-hydroxybutyrate GHBCalibrationLinear ModelsCrimeGas chromatography–mass spectrometrySodium OxybateChromatography LiquidHair
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Non-compact myocardium assessment by cardiac magnetic resonance: dependence on image analysis method

2018

To compare image analysis methods for the assessment of left ventricle non-compaction from cardiac magnetic resonance (CMR) imaging. CMR images were analyzed in 20 patients and 10 normal subjects. A reference model of the MR signal was introduced and validated based on image data. Non-compact (NC) myocardium size and distribution were assessed by tracing a single, continuous contour delimiting trabeculated region (Jacquier) or by one-by-one selection of trabeculae (Grothoff). The global non-compact/compact (NC/C) ratio, the NC mass, and the segmental NC/C ratio were assessed. Results were compared with the reference model. A significant difference between Grothoff and Jacquier approaches in…

AdultMaleRadiology Nuclear Medicine and ImagingHeart VentriclesMagnetic Resonance Imaging Cine030204 cardiovascular system & hematology030218 nuclear medicine & medical imagingYoung Adult03 medical and health sciences0302 clinical medicineNuclear magnetic resonanceMagnetic resonance imagingNuclear Medicine and ImagingImage Processing Computer-AssistedmedicineHumansComputer-assisted image analysiComputer-assisted image analysis; Isolated noncompaction of the ventricular myocardium; Magnetic resonance imaging; Radiology; Nuclear Medicine and Imaging; Cardiology and Cardiovascular MedicineCardiac imagingAnalysis methodAgedReproducibilitymedicine.diagnostic_testbusiness.industryImage (category theory)Significant differenceReproducibility of ResultsMagnetic resonance imagingMiddle AgedReference StandardsComputer-assisted image analysisCardiac Imaging Techniquesmedicine.anatomical_structureVentricleIsolated noncompaction of the ventricular myocardiumFemalebusinessCardiac magnetic resonanceRadiologyCardiology and Cardiovascular Medicine
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Comparison of CT and magnetic resonance mDIXON-Quant sequence in the diagnosis of mild hepatic steatosis

2018

Objective: To determine the diagnostic performance of CT in the assessment of mild hepatic steatosis by comparison with MR mDIXON-Quant as a reference standard, and to explore their clinical applications. Methods: In this prospective study 169 volunteers were included. Each subject underwent CT and MR mDIX-ON-Quant examinations. Hepatic steatosis evaluations were performed via liver attenuation alone (CT L), liver to spleen attenuation ratio (CT L/S), difference between liver and spleen attenuation (CT L-S), and MR mDIX-ON-Quant imaging. The effectiveness of CT L, CT L/S, and CT L-S in diagnosing hepatic steatosis severity of ≥5%, ≥10%, and ≥15% was compared, using mDIX-ON-Quant results as …

AdultMaleSensitivity and Specificitynot known030218 nuclear medicine & medical imagingYoung Adult03 medical and health sciences0302 clinical medicineNon-alcoholic Fatty Liver DiseaseMultidetector Computed TomographymedicineHumansRadiology Nuclear Medicine and imagingProspective StudiesProspective cohort studyReference standardsSequence (medicine)Full Papermedicine.diagnostic_testbusiness.industryMagnetic resonance imagingGeneral MedicineMiddle Agedmedicine.diseaseMagnetic Resonance ImagingFemale030211 gastroenterology & hepatologySteatosisNuclear medicinebusinessThe British Journal of Radiology
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Evidence for a white matter lesion size threshold to support the diagnosis of relapsing remitting multiple sclerosis

2018

Abstract Background The number of white matter lesions (WML) in brain MRI is the most established paraclinical tool to support the diagnosis of multiple sclerosis (MS) and to monitor its course. Diagnostic criteria have stipulated a minimum detectable diameter of 3 mm per WML, although this threshold is not evidence-based. We aimed to provide a rationale for a WML size threshold for three-dimensional MRI sequences at 3 T by comparing patients with relapsing-remitting MS (RRMS) to control subjects (CS). Methods We analyzed MR images from two cohorts, obtained at scanners from two different vendors, each comprising patients with RRMS and CS. Both cohorts were examined with FLAIR and T1w seque…

AdultMaleWhite matter lesionNeuroimagingFluid-attenuated inversion recoveryYoung Adult03 medical and health sciencesMultiple Sclerosis Relapsing-Remitting0302 clinical medicineHumansMedicine030212 general & internal medicineRetrospective StudiesExpanded Disability Status ScaleReceiver operating characteristicbusiness.industryMultiple sclerosisGeneral MedicineOdds ratioReference Standardsmedicine.diseaseMagnetic Resonance ImagingWhite MatterHyperintensityNeurologyRelapsing remittingFemaleNeurology (clinical)businessNuclear medicine030217 neurology & neurosurgeryMultiple Sclerosis and Related Disorders
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Solid bone tumors of the spine: Diagnostic performance of apparent diffusion coefficient measured using diffusion-weighted MRI using histology as a r…

2017

Purpose To assess the diagnostic performance of mean apparent diffusion coefficient (mADC) in differentiating benign from malignant bone spine tumors, using histology as a reference standard. Conventional magnetic resonance imaging (MRI) sequences have good reliability in evaluating spinal bone tumors, although some features of benign and malignant cancers may overlap, making the differential diagnosis challenging. Materials and Methods In all, 116 patients (62 males, 54 females; mean age 59.5 ± 14.1) with biopsy-proven spinal bone tumors were studied. Field strength/sequences: 1.5T MR system; T1-weighted turbo spin-echo (repetition time / echo time [TR/TE], 500/13 msec; number of excitatio…

AdultMalemedicine.medical_specialtyAdolescentIntraclass correlationGadoliniumchemistry.chemical_elementSensitivity and Specificity030218 nuclear medicine & medical imagingDiagnosis Differential03 medical and health sciencesYoung Adult0302 clinical medicineImage Interpretation Computer-AssistedmedicineEffective diffusion coefficientHumansRadiology Nuclear Medicine and imagingStage (cooking)AgedRetrospective StudiesAged 80 and overSpinal Neoplasmsmedicine.diagnostic_testReceiver operating characteristicbusiness.industryEcho-Planar ImagingReproducibility of ResultsMagnetic resonance imagingMiddle AgedReference StandardsConfidence intervalSpineDiffusion Magnetic Resonance Imagingchemistry030220 oncology & carcinogenesisFemaleRadiologyNuclear medicinebusinessDiffusion MRIJournal of magnetic resonance imaging : JMRI
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Meniscal ramp lesions: diagnostic performance of MRI with arthroscopy as reference standard

2021

Abstract Background The posteromedial meniscal region is gaining interest among orthopedic surgeons, as lesions of this area has been reported to be significantly associated with anterior cruciate ligament tears. The current imaging literature is unclear. Purpose To evaluate the diagnostic performance of MR in the detection of meniscal ramp lesions having arthroscopy as reference standard. Materials and methods We retrospectively included 56 patients (mean age of 25 ± 7 years; 14 females) from January to November 2017 with a arthroscopically proved ACL tear and posterior meniscocapsular separation. On preoperative MRI, two radiologists with 13 and 2 years’ experience in musculoskeletal imag…

AdultMalemedicine.medical_specialtyAdolescentMeniscus (anatomy)Lesion03 medical and health sciencesArthroscopyYoung Adult0302 clinical medicineACL injuries; Anatomy; Arthroscopy; Meniscus; MRI; Adolescent; Adult; Anterior Cruciate Ligament Injuries; Arthroscopy; Female; Humans; Male; Reference Standards; Retrospective Studies; Tibial Meniscus Injuries; Young Adult; Magnetic Resonance ImagingmedicineHumansRadiology Nuclear Medicine and imagingMeniscusNeuroradiologyRetrospective StudiesACL injuries030222 orthopedicsmedicine.diagnostic_testbusiness.industryAnterior Cruciate Ligament InjuriesArthroscopyUltrasoundInterventional radiology030229 sport sciencesGeneral MedicineReference StandardsMagnetic Resonance ImagingTibial Meniscus InjuriesBruisemedicine.anatomical_structureMusculoskeletal RadiologyOrthopedic surgeryFemalemedicine.symptomAnatomySettore MED/36 - Diagnostica Per Immagini E RadioterapiaNuclear medicinebusinessMRI
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Psychometric properties of non-specific electrodermal response frequency for a sample of male students.

1990

In the present study data on the frequency of non-specific electrodermal responses (NSRs) are presented for a large and, with regard to sex, age and educational level, homogeneous sample of male students (n = 590). These data were obtained in 9 independent experiments in which NSRs were recorded under equivalent conditions. NSRs were scored as skin conductance changes greater than 0.02 muSiemens. A recording period of 5 min prior to experimental manipulations was chosen. A systematic comparison between the 9 studies, the distribution of NSRs for the total sample, as well as descriptive data for stabile and labile subgroups are presented. For 213 subjects NSR-frequency was recorded twice, wi…

AdultMalemedicine.medical_specialtyDescriptive statisticsPsychometricsGeneral NeuroscienceRestScoring criteriaIndividualitySample (statistics)Galvanic Skin ResponseAudiologyReference StandardsDevelopmental psychologyNeuropsychology and Physiological PsychologyNon specificMicrocomputersHomogeneousResearch DesignPhysiology (medical)Electrodermal responsemedicineHumansSkin conductancePsychologyInternational journal of psychophysiology : official journal of the International Organization of Psychophysiology
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Towards an international language for incontinence-associated dermatitis (IAD): design and evaluation of psychometric properties of the Ghent Global …

2018

Background Incontinence-associated dermatitis (IAD) is a specific type of irritant contact dermatitis with different levels of severity. An internationally accepted instrument to assess the severity of IAD in adults with established diagnostic accuracy, agreement, and reliability is needed to support clinical practice and research.Objectives To design and psychometrically evaluate the Ghent Global IAD Categorisation Tool (GLOBIAD).Methods The design was based on expert consultation using a three-round Delphi procedure with 34 experts from 13 countries. The instrument was tested using IAD photographs reflecting different severity levels in a sample of 823 health professionals in 30 countries…

AdultMalemedicine.medical_specialtyInternationalityPsychometricsPsychometricsFleiss' kappaDermatologySensitivity and SpecificitySeverity of Illness Index030207 dermatology & venereal diseases03 medical and health sciences0302 clinical medicineTerminology as TopicSeverity of illnessMedicineHumans030212 general & internal medicineLanguageObserver Variationbusiness.industryIntra-rater reliabilityReference StandardsConfidence interval3. Good healthInter-rater reliabilityUrinary IncontinenceCategorization030220 oncology & carcinogenesisPhysical therapyDermatitis IrritantFemalebusinessKappa
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Overview of ambulatory blood pressure monitoring in childhood and pregnancy.

2001

Despite the fact that the study and applicability of ambulatory blood pressure in children and pregnant women share characteristics which limit the potential development of knowledge for their use, advances produced in the last few years provided the present knowledge regarding the significance and the potential use of ambulatory blood pressure in children and in the pregnant women. In children ambulatory blood pressure monitoring is useful for the diagnosis of mild hypertensives, assessment of refractory hypertension, therapeutic trials with antihypertensive drugs, and clinical investigation when BP is one of the parameters to be taken into account and/or when subtle BP abnormalities are t…

AdultMalemedicine.medical_specialtyPediatricsAmbulatory blood pressurePregnancy Complications CardiovascularAssessment and DiagnosisPre-EclampsiaPregnancyClinical investigationInternal MedicinemedicineHumansIntensive care medicineChildAdvanced and Specialized NursingPregnancybusiness.industryGeneral MedicineBlood Pressure Monitoring AmbulatoryReference Standardsmedicine.diseaseTherapeutic trialBlood pressureHypertensionFemaleCardiology and Cardiovascular MedicinebusinessBlood pressure monitoring
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Clinical evaluation of a wireless ECG sensor system for arrhythmia diagnostic purposes

2013

Accepted version of an article in the journal: Medical Engineering and Physics. Also available from the publisher at: http://dx.doi.org/10.1016/j.medengphy.2013.03.002 In a clinical study, a novel wireless electrocardiogram (ECG) recorder has been evaluated with regard to its ability to perform arrhythmia diagnostics. As the ECG recorder will detect a "non-standard" ECG signal, it has been necessary to compare those signals to "standard" ECG recording signals in order to evaluate the arrhythmia detection ability of the new system. Simultaneous recording of ECG signals from both the new wireless ECG recorder and a conventional Holter recorder was compared by two independent cardiology specia…

AdultMalemedicine.medical_specialtyambulatory electrocardiographyBiomedical EngineeringBiophysicsElectrocardiographyYoung Adultevaluation studiesmedicineHumansWirelessMedical physicscardiovascular diseasesChildReference standardsAgedAmbulatory electrocardiographySensor systemclinical trialsbusiness.industryReproducibility of ResultsArrhythmias CardiacSignal Processing Computer-AssistedVDP::Technology: 500::Information and communication technology: 550Middle AgedReference StandardsHolter monitoringClinical trialVDP::Medical disciplines: 700wireless ECG sensorFemalebusinessTelecommunicationsWireless TechnologyClinical evaluationHolter monitoring
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