Search results for "tandem"

showing 10 items of 560 documents

Peptides of the variable IgG domain as potential biomarker candidates in primary open-angle glaucoma (POAG)

2017

Autoantibody profiling has gained increasing interest in the research field of glaucoma promising the detection of highly specific and sensitive marker candidates for future diagnostic purposes. Recent studies demonstrated that immune responses are characterized by the expression of congruent or similar complementarity determining regions (CDR) in different individuals and could be used as molecular targets in biomarker discovery. Main objective of this study was to characterize glaucoma-specific peptides from the variable region of sera-derived immunoglobulins using liquid chromatography--mass spectrometry (LC-MS)-based quantitative proteomics. IgG was purified from sera of 13 primary open…

MaleProteomics0301 basic medicineQuantitative proteomicsEnzyme-Linked Immunosorbent AssayComplementarity determining regionProteomics03 medical and health sciencesTandem Mass SpectrometryGeneticsHumansBiomarker discoveryEye ProteinsMolecular BiologyIntraocular PressureGenetics (clinical)Mass screeningAgedAutoantibodiesAged 80 and overbiologyAutoantibodyGeneral MedicineMiddle AgedMolecular biologyFold change030104 developmental biologyImmunoglobulin Gbiology.proteinFemaleAntibodyPeptidesBiomarkersGlaucoma Open-AngleHuman Molecular Genetics
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An insight into the proteome of the saliva of the argasid tick Ornithodoros moubata reveals important differences in saliva protein composition betwe…

2013

26 páginas, 3 tablas, 6 figuras. -- The definitive version is available at http://www.elsevier.com

MaleProteomicsSalivaProteomeBiophysicsTickExosomesBiochemistryMicrobiologyTranscriptomeSex Factorsstomatognathic systemLC–MS/MSTandem Mass SpectrometryOrnithodoros moubataAnimalsSecretionOrnithodorosSalivaExpressed Sequence TagsbiologyProtein equalizationComputational Biologybiology.organism_classificationBlood mealActinsRecombinant ProteinsOrnithodoros moubataSialomePhosphopyruvate HydrataseSialomeImmunologyProteomeElectrophoresis Polyacrylamide GelFemaleChromatography Liquid
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Cell line DNA typing in forensic genetics—the necessity of reliable standards

2003

The incorporation of reference DNA is crucial to the validation of any DNA typing protocol. This paper aims to provide a panel of reference DNAs for actual forensic profiling strategies, i.e. autosomal and gonosomal STR typing as well as mtDNA sequencing. We have characterised three human lymphoid cell lines, GM9947, GM9948 and GM3657, and considered 58 autosomal and gonosomal microsatellites as well as the mitochondrial control region sequence. Well-established markers and STRs recently developed for forensic use were involved. K562 DNA samples which we purchased from two different suppliers were also analysed. They revealed conflicting results with regard to the ChrX STR marker genotype. …

MaleQuality ControlmtDNA control regionGeneticsMitochondrial DNAAutosomeGenotypeReference StandardsBiologyDNA FingerprintingDNA MitochondrialPathology and Forensic MedicineDNA profilingTandem Repeat SequencesCell Line TumorForensic profilingGenotypeHumansMicrosatelliteFemaleTypingK562 CellsLawDNA PrimersForensic Science International
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Saliva electrophoretic protein profiles in infants: changes with age and impact of teeth eruption and diet transition.

2011

International audience; Objective : The objective of this study was to describe the changes in salivary protein profiles in infants between the ages of 3 and 6 months, and to evaluate the impact of teeth eruption and introduction of solid foods on such profiles. Design : 73 infants were followed longitudinally at 3 and 6 months of age. Their whole saliva proteins were separated by SDS–PAGE electrophoresis and semi-quantified by image analysis. Amylase activity was also measured on a sub-sample of the population (n=42 infants). Bands which abundance was significantly different between the two ages according to paired comparisons were identified by mass spectrometry techniques. Results : Out …

MaleSalivaTooth eruptionPhysiologyTooth Eruption0302 clinical medicineTandem Mass Spectrometry[SDV.IDA]Life Sciences [q-bio]/Food engineeringAmylaseLongitudinal StudiesProspective Studies0303 health scienceseducation.field_of_studybiologyChemistryinfantsGeneral MedicineInfant FormulaBiochemistryAmylasesSalivary CystatinsElectrophoresis Polyacrylamide GelFemaleInfant FoodIntroduction of solid foodamylaseSpectrometry Mass Electrospray IonizationproteomePopulationslivaWeaning03 medical and health sciencesWeaningHumans[SPI.GPROC]Engineering Sciences [physics]/Chemical and Process EngineeringCystatin AProtease InhibitorsCystatin BSalivary Proteins and PeptideseducationGeneral DentistrycystatinSerum Albumin030304 developmental biologyMilk HumanBeta-2 microglobulinSalivary CystatinsAlbuminInfant030206 dentistryCell BiologyDietSecretory ComponentOtorhinolaryngologySpectrometry Mass Matrix-Assisted Laser Desorption-Ionizationbiology.proteinproteinbeta 2-Microglobulinteeth eruptionChromatography LiquidFollow-Up StudiesArchives of oral biology
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Food quality and nutraceutical value of nine cultivars of mango (Mangifera indica L.) fruits grown in Mediterranean subtropical environment

2019

Mango (Mangifera indica L.) quality is strongly influenced by genotype but individuating the most appropriate harvesting time is essential to obtain high quality fruits. In this trial we studied the influences of the ripening stage at harvest (mature-ripe or green-ripe) on quality of ready to eat mango fruits from nine cultivars (Carrie, Keitt, Glenn, Manzanillo, Maya, Rosa, Osteen, Tommy Atkins and Kensington Pride) grown in the Mediterranean subtropical climate through physicochemical, nutraceutical, and sensory analysis. Our results show a large variability among the different observed genotypes and in dependence of the ripening stage at harvest. With the exception of Rosa, mature-ripe f…

MaleSettore CHIM/10 - Chimica Degli AlimentiChemical PhenomenaAntioxidant activity; Apigenin (PubChem CID: 5280443); Benzoic acid (PubChem CID: 243); Caffeic acid (PubChem CID: 689043); Ferulic acid (PubChem CID: 445858); Gallic acid (PubChem CID: 370); Mangiferin; Mangiferin (PubChem CID: 5281647); P-coumaric acid (PubChem CID: 637542); Phytochemicals; Sensory profile; Syringic acid (PubChem CID: 10742); Vanillin (PubChem CID: 1183); Adult; Antioxidants; Ascorbic Acid; Carotenoids; Chemical Phenomena; Color; Dietary Supplements; Female; Food Analysis; Fruit; Humans; Male; Mangifera; Mediterranean Region; Phenols; Plant Extracts; Principal Component Analysis; Sicily; Tandem Mass Spectrometry; Taste; Food QualityPhytochemicalsHumid subtropical climateCaffeic acid (PubChem CID: 689043)Ascorbic Acid01 natural sciencesAntioxidantsAnalytical ChemistryTandem Mass SpectrometrySettore BIO/13 - Biologia ApplicataSettore BIO/10 - BiochimicaMangiferaCultivarSicilyGallic acid (PubChem CID: 370)Principal Component AnalysisMediterranean RegionSensory profileMangiferin (PubChem CID: 5281647)RipeningP-coumaric acid (PubChem CID: 637542)04 agricultural and veterinary sciencesGeneral Medicine040401 food scienceSettore AGR/03 - Arboricoltura Generale E Coltivazioni ArboreeHorticultureTasteFemaleAdultApigenin (PubChem CID: 5280443)Settore AGR/13 - Chimica AgrariaColorSubtropicsPhytochemicalBiologyVanillin (PubChem CID: 1183)0404 agricultural biotechnologyNutraceuticalAntioxidant activityBenzoic acid (PubChem CID: 243)PhenolsFood QualityHumansSyringic acid (PubChem CID: 10742)MangiferaPlant Extracts010401 analytical chemistryAscorbic acidCarotenoids0104 chemical sciencesFruitDietary SupplementsMangiferinFood qualityFerulic acid (PubChem CID: 445858)Food AnalysisFood ScienceFood Chemistry
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Targeting metabolomics analysis of the sunscreen agent 2-ethylhexyl 4-(N,N-dimethylamino)benzoate in human urine by automated on-line solid-phase ext…

2011

The in vivo metabolism of the xenobiotic agent 2-ethylhexyl 4-(N,N-dimethylamino)benzoate (EDP), a UV filter commonly used in sunscreen cosmetic products, was studied by targeting metabolomics analysis in human urine. The metabolomic study involved the use of urine from male and female volunteers before and after application of an EDP-containing sunscreen cosmetic. The metabolism of EDP in urine was studied by using the triple quadrupole detector in a combination of Precursor Ion Scanning and Neutral Loss Scanning modes, with and without enzymatic hydrolysis. Detected metabolites were subsequently confirmed as glucuronide conjugates of 4-(N,N-dimethylamino)benzoic acid and 4-(N-methylamino)…

MaleSkin AbsorptionTandem mass spectrometryMass spectrometryBiochemistryHigh-performance liquid chromatographyAnalytical ChemistrySonicationDrug StabilityTandem Mass SpectrometryLiquid chromatography–mass spectrometrypara-AminobenzoatesHumansMetabolomicsSolid phase extractionGlucuronidaseChromatographyChemistryHydrolysisSolid Phase ExtractionOrganic ChemistryGeneral MedicineTriple quadrupole mass spectrometerStandard additionMetabolomeFemaleSulfatasesTime-of-flight mass spectrometry4-Aminobenzoic AcidSunscreening AgentsChromatography LiquidJournal of Chromatography A
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DNA Commission of the International Society of Forensic Genetics: recommendations on forensic analysis using Y-chromosome STRs

2001

During the past few years, the DNA Commission of the International Society of Forensic Genetics has published a series of documents providing guidelines and recommendations concerning the application of DNA polymorphisms to the problems of human identification. This latest report addresses a relatively new area - namely, Y-chromosome polymorphisms, with particular emphasis on short tandem repeats (STRs). This report addresses nomenclature, use of allelic ladders, population genetics and reporting methods.

MaleSocieties ScientificISFGDNA CommissionPopulationLibrary scienceGuidelines as TopicPaternityCommissionBiologySTRY chromosome01 natural sciencesPathology and Forensic Medicine03 medical and health sciences0302 clinical medicineTerminology as TopicY ChromosomeHumans030216 legal & forensic medicineeducationY-chromosomeAlleles030304 developmental biologyGeneticsInternet0303 health scienceseducation.field_of_studyPolymorphism Genetic010401 analytical chemistryDna polymorphismInternational AgenciesChromosome MappingDNAForensic MedicineSettore MED/43 - MEDICINA LEGALE0104 chemical sciencesForensic scienceGenetics PopulationDatabases as TopicTandem Repeat SequencesMutationMicrosatelliteIdentification (biology)LawForensic geneticsInternational Journal of Legal Medicine
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Identification and quantification of a new family of peptide endocannabinoids (Pepcans) showing negative allosteric modulation at CB1 receptors.

2012

The α-hemoglobin-derived dodecapeptide RVD-hemopressin (RVDPVNFKLLSH) has been proposed to be an endogenous agonist for the cannabinoid receptor type 1 (CB(1)). To study this peptide, we have raised mAbs against its C-terminal part. Using an immunoaffinity mass spectrometry approach, a whole family of N-terminally extended peptides in addition to RVD-Hpα were identified in rodent brain extracts and human and mouse plasma. We designated these peptides Pepcan-12 (RVDPVNFKLLSH) to Pepcan-23 (SALSDLHAHKLRVDPVNFKLLSH), referring to peptide length. The most abundant Pepcans found in the brain were tested for CB(1) receptor binding. In the classical radioligand displacement assay, Pepcan-12 was th…

MaleSus scrofaPeptideCooperativityBiochemistrychemistry.chemical_compoundAntibodies Monoclonal Murine-DerivedHemoglobinsMice0302 clinical medicineReceptor Cannabinoid CB1NeurobiologyTandem Mass SpectrometryCricetinaeRadioligandReceptorchemistry.chemical_classification0303 health sciencesMice Inbred NZBmusculoskeletal neural and ocular physiologyfood and beveragesBrainLigand (biochemistry)humanitiesProtein TransportBiochemistrylipids (amino acids peptides and proteins)FemaleEndogenous agonistProtein BindingSignal TransductionAllosteric regulationMolecular Sequence DataHL-60 CellsCHO CellsBiologyBinding Competitive03 medical and health sciencesAllosteric RegulationCannabinoid Receptor ModulatorsAnimalsHumansAmino Acid SequenceMolecular Biology030304 developmental biologyCell BiologyCyclohexanolsHemopressinPeptide FragmentsRatsMice Inbred C57BLchemistrynervous system030217 neurology & neurosurgeryEpitope MappingThe Journal of biological chemistry
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A novel LC–MS/MS analytical method for detection of articaine and mepivacaine in blood and its application to a preliminary pharmacokinetic study

2020

Local anaesthetics (LAs) are commonly used in surgery, especially in dentistry. They cause a transitory inhibition of nerve signal due to the blockade of the voltage-gated sodium channels. LAs are administrated alone or with vasoconstriction agents, such as adrenaline. Toxicity of LAs is associated to neurological and cardiovascular alterations. Tachycardia, arrhythmia, tremors, tonic-clonic seizure and respiratory depression (at high doses) are the main symptoms of intoxication by LAs. Lidocaine, articaine and mepivacaine are among the most used anaesthetics. This study aimed to fully validated a new method for the simultaneous detection of articaine and mepivacaine in whole blood. Sample …

MaleTachycardiaLidocaineLiquid-Liquid ExtractionClinical BiochemistryMepivacainePharmaceutical ScienceCarticaineArticaine01 natural sciencesAnalytical ChemistryPharmacokineticsSettore MED/43 - Medicina LegaleLC–MS/MSTandem Mass SpectrometryArticaine Mepivacaine Local anaesthetics LC–MS/MS BloodbloodDrug DiscoverymedicineHumansAnesthetics LocalSpectroscopyarticaine; blood; LC–MS/MS; local anaesthetics; mepivacaineWhole blood010405 organic chemistryChemistry010401 analytical chemistrySelected reaction monitoringReproducibility of Results0104 chemical sciencesarticaineAnesthesiaToxicityFemalelocal anaestheticsmedicine.symptomChromatography Liquidmedicine.drugmepivacaine
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Antiulcer activity of Cyperus alternifolius in relation to its UPLC-MS metabolite fingerprint: A mechanistic study

2019

Abstract Background Gastric ulcer is one of the main prevalent gastrointestinal multi-etiological disorders with many associated complications and adverse effects. Our aim was to develop safer antiulcer therapies based on methanol or ethyl acetate extracts of tubers and aerial parts from Cyperus alternifolius. Methods Gastric ulceration was experimentally generated by administration of single oral doses of indomethacin (30 mg/kg) to fasted rats. The animals received methanol or ethyl acetate extracts of C. alternifolius tuber and methanol or ethyl acetate extracts of aerial parts at two dose levels (50 or 100 mg/kg). Ranitidine (50 mg/kg) was used as standard anti-ulcer drug. After 4 h, the…

Malemedicine.drug_classAntiulcer drugMetaboliteIndomethacinPhytochemicalsAnti-Inflammatory AgentsEthyl acetatePharmaceutical ScienceAcetatesAnti-inflammatoryRanitidine03 medical and health scienceschemistry.chemical_compound0302 clinical medicineTandem Mass SpectrometryDrug DiscoverymedicineMetabolomeAnimalsMetabolomicsStomach UlcerCyperusRats WistarAcetic Acid030304 developmental biologyPharmacology0303 health sciencesTraditional medicinebiologyPlant ExtractsChemistryMethanolPlant Components AerialAnti-Ulcer Agentsbiology.organism_classificationRatsCyperus alternifoliusPlant TubersComplementary and alternative medicinePhytochemicalGastric Mucosa030220 oncology & carcinogenesisMetabolomeMolecular MedicineChromatography Liquidmedicine.drugPhytomedicine
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