0000000000020139

AUTHOR

Carlos Bartual-murgui

0000-0003-1547-8018

showing 116 related works from this author

Influence of Host-Guest and Host-Host Interactions on the Spin-Crossover 3D Hofmann-type Clathrates {FeII(pina)[MI(CN)2]2·xMeOH (MI = Ag, Au)

2019

[EN] The synthesis, structural characterization and magnetic properties of two new isostructural porous 3D compounds with the general formula {FeII(pina)[MI(CN)2]2}·xMeOH (x = 0¿5; pina = N-(pyridin-4-yl)isonicotinamide; MI = AgI and x ~ 5 (1·xMeOH); MI = AuI and x ~ 5 (2·xMeOH)) are presented. The single-crystal X-ray diffraction analyses have revealed that the structure of 1·xMeOH (or 2·xMeOH) presents two equivalent doubly interpenetrated 3D frameworks stabilized by both argentophilic (or aurophilic) interactions and interligand C¿O···HC H-bonds. Despite the interpenetration of the networks, these compounds display accessible void volume capable of hosting up to five molecules of methano…

Hydrogen bondInorganic ChemistrySolventCrystallographychemistry.chemical_compoundchemistrySpin crossoverDesorptionFISICA APLICADAMoleculeIsonicotinamideMethanolPhysical and Theoretical ChemistryIsostructural
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Guest Effect on Nanopatterned Spin-Crossover Thin Films

2011

International audience; Nanopatterned thin films of the metal–organic framework {Fe(bpac)[Pt(CN)4]} (bpac=bis(4‐pyridyl)acetylene) are elaborated by the combination of a sequential assembly process and a lithographic method. Raman microspectroscopy is used to probe the temperature dependence of the spin state of the iron(II) ions in the films (40–90 nm in thickness), and reveals an incomplete but cooperative spin transition comparable to that of the bulk material. Adsorption/desorption of pyridine guest molecules is found to have a substantial influence on the spin‐crossover properties of the thin layers. This interplay between host–guest and spin‐crossover properties in thin films and nano…

Materials scienceSpin statesSpin transitionNanotechnology02 engineering and technologyMicroscopy Atomic ForceSpectrum Analysis Raman010402 general chemistry01 natural sciencesBiomaterialssymbols.namesakeSpin crossoverMetals HeavyDesorptionTransition TemperatureGeneral Materials ScienceThin film[SPI.NANO]Engineering Sciences [physics]/Micro and nanotechnologies/MicroelectronicsCyanidesThin layersTransition temperatureGeneral Chemistry021001 nanoscience & nanotechnologyNanostructures0104 chemical sciencessymbolsPhysical chemistrySpin Labels0210 nano-technologyRaman spectroscopyBiotechnology
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Chiral and Racemic Spin Crossover Polymorphs in a Family of Mononuclear Iron(II) Compounds

2017

[EN] Understanding the origin of cooperativity and the equilibrium temperature of transition (T1/2) displayed by the spin-crossover (SCO) compounds as well as controlling these parameters are of paramount importance for future applications. For this task, the occurrence of polymorphism, presented by a number of SCO complexes, may provide deep insight into the influence of the supramolecular organization on the SCO behavior. In this context, herein we present a novel family of mononuclear octahedral FeII complexes with formula cis- [Fe(bqen)(NCX)2], where bqen is the chelating tetradentate ligand N,N¿-bis(8-quinolyl)ethane-1,2-diamine and X = S, Se. Depending on the preparation method, these…

010405 organic chemistryChemistryStereochemistrySupramolecular chemistryCooperativity010402 general chemistry01 natural sciences0104 chemical sciencesInorganic ChemistryCrystallographyOctahedronPolymorphism (materials science)Spin crossoverFISICA APLICADARacemic mixtureOrthorhombic crystal systemPhysical and Theoretical ChemistryEnantiomerInorganic Chemistry
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Enhanced Interplay between Host–Guest and Spin-Crossover Properties through the Introduction of an N Heteroatom in 2D Hofmann Clathrates

2021

Controlled modulation of the spin-crossover (SCO) behavior through the sorption-desorption of invited molecules is an extensively exploited topic because of its potential applications in molecular sensing. For this purpose, understanding the mechanisms by which the spin-switching properties are altered by guest molecules is of paramount importance. Here, we show an experimental approach revealing a direct probe of how the interplay between SCO and host-guest chemistry is noticeably activated by chemically tuning the host structure. Thus, the axial ligand 4-phenylpyridine (4-PhPy) in the 2D Hofmann clathrates {Fe(4-PhPy)2[M(CN)4]} (PhPyM; M = Pt, Pd) is replaced by 2,4-bipyridine (2,4-Bipy),…

010405 organic chemistryLigandHeteroatomSubstituent010402 general chemistry01 natural sciences0104 chemical sciencesInorganic Chemistrychemistry.chemical_compoundCrystallographyAdsorptionchemistrySpin crossoverMoleculeMethanolPhysical and Theoretical ChemistryChemical compositionInorganic Chemistry
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Enhanced porosity in a new 3D Hofmann-like network exhibiting humidity sensitive cooperative spin transitions at room temperature

2011

The porous coordination polymers (PCPs) of general formula {Fe(bpac)[M(CN)4]}·guest (M = Pt, Pd) exhibit larger channels than previously synthesised 3D-Hofmann-like PCP. The channels are partially occupied by uncoordinated guest bpac ligands and labile H2O molecules. These PCPs exhibit very scarce cooperative spin crossover behaviour around room temperature with a large hysteresis loop (up to 49 K) and also display sensitivity to humidity and guest molecules. The inclusion of bpac molecules in the 3D network can be avoided by adding competitive volatile molecules during the crystallization process, affording the guest-free material. The spin crossover behavior of different guest and guest-f…

ChemistryPorous Coordination PolymersHumidityNanotechnologyGeneral Chemistrylaw.inventionCrystallographylawSpin crossoverMaterials ChemistryMoleculeCrystallizationSpin (physics)PorosityJournal of Materials Chemistry
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High quality nano-patterned thin films of the coordination compound {Fe(pyrazine)[Pt(CN)4]} deposited layer-by-layer

2011

International audience; An optimised procedure was developed for the layer-by-layer deposition of the Hofmann clathrate-like coordination compound {Fe(pyrazine)[Pt(CN)4]} either as continuous or as nano-patterned thin films. Characterization of the thickness and topography of the thin films by atomic force microscopy (AFM) and by surface plasmon resonance (SPR) spectroscopy, which also yields the layer's refractive index and losses, are reported. We found that the films are of good optical quality and the results of both AFM and SPR experiments are in good agreement with the theoretical predictions of the films thicknesses.

Pyrazine010405 organic chemistryChemistryLayer by layerAnalytical chemistryGeneral Chemistry010402 general chemistry01 natural sciencesCatalysis0104 chemical scienceschemistry.chemical_compoundNano-Materials ChemistryThin filmSurface plasmon resonance[SPI.NANO]Engineering Sciences [physics]/Micro and nanotechnologies/MicroelectronicsSpectroscopyRefractive indexLayer (electronics)
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Reversible guest-induced gate-opening with multiplex spin crossover responses in two-dimensional Hofmann clathrates.

2021

Spin crossover (SCO) compounds are very attractive types of switchable materials due to their potential applications in memory devices, actuators or chemical sensors. Rational chemical tailoring of these switchable compounds is key for achieving new functionalities in synergy with the spin state change. However, the lack of precise structural information required to understand the chemical principles that control the SCO response with external stimuli may eventually hinder further development of spin switching-based applications. In this work, the functionalization with an amine group in the two-dimensional (2D) SCO compound {Fe(5-NH2Pym)2[MII(CN)4]} (1M, 5-NH2Pym = 5-aminopyrimidine, MII =…

Materials scienceSpin states010405 organic chemistryKineticsGeneral Chemistry010402 general chemistry01 natural sciences3. Good health0104 chemical sciencesChemistryChemical physicsSpin crossoverDesorptionSurface modificationMoleculeSpin (physics)Single crystalChemical science
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Correction: Effect of nanostructuration on the spin crossover transition in crystalline ultrathin films

2019

Correction for ‘Effect of nanostructuration on the spin crossover transition in crystalline ultrathin films’ by Víctor Rubio-Giménez et al., Chem. Sci., 2019, DOI: 10.1039/c8sc04935a.

Materials scienceCondensed matter physicsSpin crossoverGeneral ChemistryChemical Science
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Bistable Hofmann-Type FeII Spin-Crossover Two-Dimensional Polymers of 4-Alkyldisulfanylpyridine for Prospective Grafting of Monolayers on Metallic Su…

2021

Aiming at investigating the suitability of Hofmann-type two-dimensional (2D) coordination polymers {FeII(Lax)2[MII(CN)4]} to be processed as single monolayers and probed as spin crossover (SCO) junctions in spintronic devices, the synthesis and characterization of the MII derivatives (MII = Pd and Pt) with sulfur-rich axial ligands (Lax = 4-methyl- and 4-ethyl-disulfanylpyridine) have been conducted. The thermal dependence of the magnetic and calorimetric properties confirmed the occurrence of strong cooperative SCO behavior in the temperature interval of 100-225 K, featuring hysteresis loops 44 and 32.5 K/21 K wide for PtII-methyl and PtII/PdII-ethyl derivatives, while the PdII-methyl deri…

chemistry.chemical_classificationSpintronics010405 organic chemistryChemistrymedia_common.quotation_subjectFrustrationPolymer010402 general chemistry01 natural sciences0104 chemical sciencesInorganic ChemistryMetalHysteresisCrystallographySpin crossovervisual_artExcited stateMonolayervisual_art.visual_art_mediumPhysical and Theoretical Chemistrymedia_commonInorganic Chemistry
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Discrimination between two memory channels by molecular alloying in a doubly bistable spin crossover material

2019

[EN] A multistable spin crossover (SCO) molecular alloy system [Fe1-xMx(nBu-im)(3)(tren)](P1-yAsyF6)(2) (M = Zn-II, Ni-II; (nBu-im)(3)(tren) = tris(n-butyl-imidazol(2-ethylamino))amine) has been synthesized and characterized. By controlling the composition of this isomorphous series, two cooperative thermally induced SCO events featuring distinct critical temperatures (T-c) and hysteresis widths (Delta T-c, memory) can be selected at will. The pristine derivative 100As (x = 0, y = 1) displays a strong cooperative two-step SCO and two reversible structural phase transitions (PTs). The low temperature PTLT and the SCO occur synchronously involving conformational changes of the ligand's n-buty…

Materials science010405 organic chemistryLigandHydrostatic pressureKineticsGeneral Chemistry010402 general chemistry01 natural sciences0104 chemical sciencesCrystallographyHysteresischemistry.chemical_compoundChemistrychemistrySpin crossoverIsomorphous substitutionFISICA APLICADASingle crystalDerivative (chemistry)Chemical Science
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Extrinsicvs.intrinsic luminescence and their interplay with spin crossover in 3D Hofmann-type coordination polymers

2020

The research of new multifunctional materials, as those undergoing spin crossover (SCO) and luminescent properties, is extremely important in the development of further optical and electronic switching devices. As a new step towards this ambitious aim, the coupling of SCO and fluorescence is presented here following two main strategies: whether the fluorescent agent is integrated as a part of the main structure of a 3D SCO coordination polymer {FeII(bpan)[MI(CN)2]2} (bpan = bis(4-pyridyl)anthracene, MI = Ag (FebpanAg), Au (FebpanAu)) or is a guest molecule inserted within the cavities of the 3D switchable framework {FeII(bpb)[MI(CN)2]2}·pyrene (bpb = bis(4-pyridyl)butadiyne, MI = Ag (FebpbA…

chemistry.chemical_classificationAnthraceneMaterials scienceCoordination polymer02 engineering and technologyGeneral ChemistryPolymer010402 general chemistry021001 nanoscience & nanotechnology01 natural sciencesFluorescence0104 chemical sciencesCrystallographychemistry.chemical_compoundchemistrySpin crossoverMaterials ChemistryMoleculeAbsorption (chemistry)0210 nano-technologyLuminescenceJournal of Materials Chemistry C
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Thermo- and photo-modulation of exciplex fluorescence in a 3D spin crossover Hofmann-type coordination polymer

2018

[EN] The search for bifunctional materials showing synergies between spin crossover (SCO) and luminescence has attracted substantial interest since they could be promising platforms for new switching electronic and optical technologies. In this context, we present the first three-dimensional Fe-II Hofmann-type coordination polymer exhibiting SCO properties and luminescence. The complex {Fe-II(bpben)[Au(CN)(2)]}@pyr (bpben = 1,4-bis(4-pyridyl)benzene) functionalized with pyrene (pyr) guests undergoes a cooperative multi-step SCO, which has been investigated by single crystal X-ray diffraction, single crystal UV-Vis absorption spectroscopy, and magnetic and calorimetric measurements. The resu…

Materials scienceAbsorption spectroscopyCoordination polymerPopulationContext (language use)02 engineering and technology010402 general chemistryPhotochemistry01 natural sciencesLIESSTEmissionchemistry.chemical_compoundComplexesSpin crossoverPressureeducationFE(ABPT)(2)(NCX)(2) XBehavioreducation.field_of_studyNanocompositeHysteresisGeneral Chemistry021001 nanoscience & nanotechnology0104 chemical sciencesChemistrychemistryFISICA APLICADATransitionNetworks0210 nano-technologyLuminescenceSingle crystalStateChemical Science
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Heteroleptic Iron(II) Spin-Crossover Complexes Based on a 2,6-Bis(pyrazol-1-yl)pyridine-type Ligand Functionalized with a Carboxylic Acid

2019

Two new heteroleptic complexes [Fe- (1bppCOOH)(3bpp-bph)](ClO4)2·solv (1·solv, solv = various solvents; 1bppCOOH = 2,6-bis(1H-pyrazol-1-yl)- isonicotinic acid; 3bpp-bph = 2,6-bis(5-([1,1′-biphenyl]-4- yl)-1H-pyrazol-3-yl)pyridine) and [Fe(1bppCOOH)- (1bppCOOEt)](ClO4)2 ·0.5Me2CO (2·0.5Me2CO, 1bppCOOEt = ethyl 2,6-bis(1H-pyrazol-1-yl)isonicotinate) were designed and prepared. The heteroleptic compound 1· solv was obtained by the combination of stoichiometric amounts of Fe(ClO4)2, 1bppCOOH, and 3bpp-bph, and it was designed to fine-tune the spin crossover (SCO) properties with respect to the previously reported homoleptic compound [Fe(1bppCOOH)2](ClO4)2. Indeed, the introduction of a new subs…

chemistry.chemical_classification010405 organic chemistryLigandCarboxylic acidEnllaços químicsQuímica organometàl·licaKetones010402 general chemistryIsonicotinic acidLigands01 natural sciencesMedicinal chemistry0104 chemical sciencesInorganic Chemistrychemistry.chemical_compoundLligandschemistrySpin crossoverCetonesPyridineCompostos de coordinacióPhysical and Theoretical ChemistryInorganic Chemistry
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Tunable Spin-Crossover Behavior of the Hofmann-like Network {Fe(bpac)[Pt(CN) 4 ]} through Host-Guest Chemistry

2013

A study of the spin-crossover (SCO) behavior of the tridimensional porous coordination polymer {Fe(bpac)[Pt(CN)4]} (bpac=bis(4-pyridyl) acetylene) on adsorption of different mono- and polyhalobenzene guest molecules is presented. The resolution of the crystal structure of {Fe(bpac)[Pt(CN) 4]}A?G (G=1,2,4-trichlorobenzene) shows preferential guest sites establishing I?A?A?A?I? stacking interactions with the host framework. These host-guest interactions may explain the relationship between the modification of the SCO behavior and both the chemical nature of the guest molecule (electronic factors) and the number of adsorbed molecules (steric factors). Copyright © 2013 WILEY-VCH Verlag GmbH & …

Steric effectsclathrates010405 organic chemistryCoordination polymerStereochemistryOrganic Chemistryhost–guest systemsStackingGeneral ChemistryCrystal structure010402 general chemistrystacking interactions01 natural sciencesCatalysis0104 chemical scienceschemistry.chemical_compoundCrystallographymetal–organic frameworkschemistryspin crossoverSpin crossoverMoleculeMetal-organic framework[CHIM.COOR]Chemical Sciences/Coordination chemistryHost–guest chemistry
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Effect of nanostructuration on the spin crossover transition in crystalline ultrathin films† †Electronic supplementary information (ESI) available: M…

2019

Film thickness and microstructure critically affect the spin crossover transition of a 2D coordination polymer.

FabricationMaterials scienceChemistry MultidisciplinarySpin transitionNanotechnology010402 general chemistry01 natural sciencesCondensed Matter::Materials ScienceTHIN-FILMSSpin crossoverMETAL-ORGANIC FRAMEWORKCondensed Matter::SuperconductivityNANOPARTICLESThin film[PHYS.COND]Physics [physics]/Condensed Matter [cond-mat]Nanoscopic scaleTEMPERATUREComputingMilieux_MISCELLANEOUSchemistry.chemical_classificationQuantitative Biology::BiomoleculesScience & Technology010405 organic chemistryGeneral ChemistryPolymerQuímicaMicrostructureTHERMAL HYSTERESIS0104 chemical sciencesCondensed Matter::Soft Condensed MatterChemistrySIZENanocrystalchemistryLAYERVACUUMPhysical SciencesPHASE-TRANSITIONSCondensed Matter::Strongly Correlated ElectronsCOORDINATION POLYMERSChemical Science
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Epitaxial Thin-Film vs Single Crystal Growth of 2D Hofmann-Type Iron(II) Materials: A Comparative Assessment of their Bi-Stable Spin Crossover Proper…

2020

Integration of the ON-OFF cooperative spin crossover (SCO) properties of FeII coordination polymers as components of electronic and/or spintronic devices is currently an area of great interest for potential applications. This requires the selection and growth of thin films of the appropriate material onto selected substrates. In this context, two new series of cooperative SCO two-dimensional FeII coordination polymers of the Hofmann-type formulated {FeII(Pym)2[MII(CN)4]·xH2O}n and {FeII(Isoq)2[MII(CN)4]}n (Pym = pyrimidine, Isoq = isoquinoline; MII = Ni, Pd, Pt) have been synthesized, characterized, and the corresponding Pt derivatives selected for fabrication of thin films by liquid-phase …

Materials scienceQuímica organometàl·lica010402 general chemistryEpitaxy01 natural sciencesHofmann-type clathratesspin crossoverSpin crossoverGeneral Materials ScienceHardware_ARITHMETICANDLOGICSTRUCTURESThin filmMaterialschemistry.chemical_classificationSpintronicsSingle crystal growth010405 organic chemistrybusiness.industryepitaxial growthEpitaxial thin filmPolymer0104 chemical sciencescoordination polymersBi stablesize-reduction effectchemistrythin filmsOptoelectronicsbusiness
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Ultrathin Films of 2D Hofmann-Type Coordination Polymers: Influence of Pillaring Linkers on Structural Flexibility and Vertical Charge Transport

2019

Searching for novel materials and controlling their nanostructuration into electronic devices is a challenging task ahead of chemists and chemical engineers. Even more so when this new application requires an exquisite control over the morphology, crystallinity, roughness and orientation of the films produced. In this context, it is of critical importance to analyze the influence of the chemical composition of perspective materials on their properties at the nanoscale. We report the fabrication of ultrathin films (thickness < 30 nm) of a family of FeII Hofmann-like coordination polymers by using an optimized liquid phase epitaxy (LPE) set-up. The series [Fe(L)2{Pt(CN)4}] (L = pyridine, pyri…

TechnologyMaterials scienceGeneral Chemical EngineeringMaterials ScienceQuímica organometàl·licaMaterials Science MultidisciplinaryNanotechnology02 engineering and technology010402 general chemistry01 natural sciencesTask (project management)METAL-ORGANIC FRAMEWORKSTHIN-FILMSNANOPARTICLESMaterials ChemistryElectronicsMOLECULAR WIRESLIQUID-METALchemistry.chemical_classificationFlexibility (engineering)Science & TechnologyCONDUCTANCEChemistry PhysicalSPIN-CROSSOVERCharge (physics)General ChemistryPolymerNANOSHEETS021001 nanoscience & nanotechnology0104 chemical sciencesChemistrychemistryLAYERPhysical SciencesMaterials nanoestructurats0210 nano-technologyTRANSITIONChemistry of Materials
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Switchable Spin-Crossover Hofmann-Type 3D Coordination Polymers Based on Tri- and Tetratopic Ligands

2018

[EN] Fe-II spin-crossover (SCO) coordination polymers of the Hofmann type have become an archetypal class of responsive materials. Almost invariably, the construction of their architectures has been based on the use of monotopic and linear ditopic pyridine like ligands. In the search for new Hofmann-type architectures with SCO properties, here we analyze the possibilities of bridging ligands with higher connectivity degree. More precisely, the synthesis and structure of {Fe-II(L-N3)[M-I(CN)(2)](2)}center dot(Guest) (Guest = nitro-benzene, benzonitrile, o-dichlorobenzene; M-I = Ag, Au) and {Fe-II(L-N4)[Ag-2(CN)(3)][Ag(CN)(2)]}center dot H2O are described, where L-N3 and L-N4 are the tritopic…

chemistry.chemical_classification010405 organic chemistryPolymerType (model theory)010402 general chemistry01 natural sciences0104 chemical sciencesInorganic ChemistryNitrobenzenechemistry.chemical_compoundBenzonitrileCrystallographychemistrySpin crossoverFISICA APLICADAPhysical and Theoretical ChemistryBenzene
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Synergetic effect of host-guest chemistry and spin crossover in 3D Hofmann-like metal-organic frameworks [Fe(bpac)M(CN)4] (M=Pt, Pd, Ni).

2012

The synthesis and characterization of a series of three-dimensional (3D) Hofmann-like clathrate porous metal-organic framework (MOF) materials [Fe(bpac)M(CN) 4] (M=Pt, Pd, and Ni; bpac=bis(4-pyridyl)acetylene) that exhibit spin-crossover behavior is reported. The rigid bpac ligand is longer than the previously used azopyridine and pyrazine and has been selected with the aim to improve both the spin-crossover properties and the porosity of the corresponding porous coordination polymers (PCPs). The 3D network is composed of successive {Fe[M(CN) 4]} n planar layers bridged by the bis-monodentate bpac ligand linked in the apical positions of the iron center. The large void between the layers, w…

Pyrazine010405 organic chemistryChemistryStereochemistrymicroporous materialsTransition temperatureOrganic Chemistryhost–guest systemsStackingSpin transitionGeneral Chemistry010402 general chemistry01 natural sciencesCatalysis0104 chemical scienceschemistry.chemical_compoundCrystallographymetal–organic frameworksspin crossoverSpin crossoveradsorptionMoleculeMetal-organic framework[CHIM.COOR]Chemical Sciences/Coordination chemistryHost–guest chemistryChemistry (Weinheim an der Bergstrasse, Germany)
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Cover Feature: Cyanido‐Bridged Fe II –M I Dimetallic Hofmann‐Like Spin‐Crossover Coordination Polymers Based on 2,6‐Naphthyridine (Eur. J. Inorg. Che…

2018

Inorganic Chemistrychemistry.chemical_classificationCrystallographyFeature (computer vision)ChemistrySpin crossoverCover (algebra)PolymerEuropean Journal of Inorganic Chemistry
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Thermal and pressure-induced spin crossover in a novel three-dimensional Hoffman-like clathrate complex

2011

The synthesis and crystal structure of the interpenetrated metal–organic framework material Fe(bpac)2[Ag(CN)2]2 (bpac = 4,4′-bis(pyridyl)acetylene) are reported along with the characterization of its spin crossover properties by variable temperature magnetometry and Mossbauer spectroscopy. The complex presents an incomplete stepped spin transition as a function of temperature that is modified upon successive thermal cycling. The pressure-induced transition has also been investigated by means of high pressure Raman spectroscopy using a diamond anvil cell. The results show that it is possible to reach the thermally-inaccessible fully low spin state at room temperature by applying hydrostatic …

Spin statesCondensed matter physicsChemistryHydrostatic pressureSpin transitionGeneral ChemistryTemperature cyclingCrystal structureCatalysissymbols.namesakeSpin crossoverMössbauer spectroscopyMaterials ChemistrysymbolsPhysical chemistryRaman spectroscopyNew Journal of Chemistry
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Cyanido-Bridged FeII-MI Dimetallic Hofmann-Like Spin-Crossover Coordination Polymers Based on 2,6-Naphthyridine

2017

[EN] Two new 3D spin-crossover (SCO) Hofmann-type coordination polymers {Fe(2,6-naphthy)[Ag(CN)2][Ag2(CN)3]} (1; 2,6-naphthy = 2,6-naphthyridine) and {Fe(2,6-naphthy)- [Au(CN)2]2}·0.5PhNO2 (2) were synthesized and characterized. Both derivatives are made up of infinite stacks of {Fe[Ag(CN)2]2- [Ag2(CN)3]}n and {Fe[Au(CN)2]2}n layered grids connected by pillars of 2,6-naphthy ligands coordinated to the axial positions of the FeII centers of alternate layers.

Void (astronomy)SilverStereochemistryIron02 engineering and technology010402 general chemistry01 natural sciencesInorganic ChemistryNitrobenzenechemistry.chemical_compoundN ligandsSpin crossoverMoleculechemistry.chemical_classificationPolymerMetal-organic frameworks021001 nanoscience & nanotechnologySpin crossover0104 chemical sciencesCrystallographychemistryFISICA APLICADAMetal-organic frameworkGold0210 nano-technology
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{[Hg(SCN)3]2(n-L)}2-: An Efficient Secondary Building Unit for the Synthesis of 2D Iron(II) Spin-Crossover Coordination Polymers

2018

[EN] We report an unprecedented series of two-dimensional (2D) spin-crossover (SCO) heterobimetallic coordination polymers generically formulated as {Fe-II[(He(SCN)(3))(2)](L)(x))}center dot Solv, where x = 2 for L = tvp (trans-(4,4'-vinylenedipyridine)) (1tvp), bpmh ((1E,2E)-1,2-bis(pyridin-4-ylmethylene)hydrazine) (1bpmh center dot nCH(3)OH; n = 0, 1), by eh ( (1E,2E)-1,2-bis (1-(pyridin-4-yl) ethyliden e) hydrazine) (Ibpeh center dot nH(2)O; n = 0, 1) and x = 2.33 for L = 0 0 bpbz (1,4-bis(pyridin-4-yl)benzene) (1bpbz center dot nH(2)O; n = 0, 2/ 3). The results confirm that self-assembly of Fell, [Hg-II(SCN)(4)](2-), and ditopic rodlike bridging ligands L containing 4-pyridyl moieties f…

ChemistryLigandEnthalpySolvation02 engineering and technology010402 general chemistry021001 nanoscience & nanotechnology01 natural sciencesLIESST0104 chemical sciencesInorganic ChemistrySolventchemistry.chemical_compoundCrystallographySpin crossoverFISICA APLICADAMoleculePhysical and Theoretical Chemistry0210 nano-technologyBenzene
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CCDC 2018380: Experimental Crystal Structure Determination

2020

Related Article: Rubén Turo-Cortés, Carlos Bartual-Murgui, Javier Castells-Gil, M. Carmen Muñoz, Carlos Martí-Gastaldo, José Antonio Real|2020|Chemical Science|11|11224|doi:10.1039/D0SC04246C

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterscatena-[octakis(mu-cyano)-tetrakis(5-aminopyrimidine)-di-iron(ii)-di-palladium(ii) dihydrate]Experimental 3D Coordinates
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CCDC 1965274: Experimental Crystal Structure Determination

2020

Related Article: Manuel Meneses-Sánchez, Lucía Piñeiro-López, Teresa Delgado, Carlos Bartual-Murgui, M. Carmen Muñoz, Pradip Chakraborty, José Antonio Real|2020|J.Mater.Chem.C|8|1623|doi:10.1039/C9TC06422B

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterscatena-((mu-44'-(buta-13-diyne-14-diyl)dipyridine)-tetrakis(mu-cyano)-di-gold-iron pyrene)Experimental 3D Coordinates
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CCDC 2018391: Experimental Crystal Structure Determination

2020

Related Article: Rubén Turo-Cortés, Carlos Bartual-Murgui, Javier Castells-Gil, M. Carmen Muñoz, Carlos Martí-Gastaldo, José Antonio Real|2020|Chemical Science|11|11224|doi:10.1039/D0SC04246C

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterscatena-[octakis(mu-cyano)-tetrakis(5-aminopyrimidine)-di-iron(ii)-di-platinum(ii) hydrate]Experimental 3D Coordinates
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CCDC 1852557: Experimental Crystal Structure Determination

2018

Related Article: Francisco Javier Valverde-Muñoz, M. Carmen Muñoz, Sacramento Ferrer, Carlos Bartual-Murgui, José A. Real|2018|Inorg.Chem.|57|12195|doi:10.1021/acs.inorgchem.8b01842

catena-[tetrakis(mu-cyano)-(mu-44'4''-(benzene-135-triyltri(ethyne-21-diyl))tripyridine)-iron(ii)-di-silver(i) nitrobenzene solvate]Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1572177: Experimental Crystal Structure Determination

2017

Related Article: Carlos Bartual-Murgui, Lucía Piñeiro-López, F. Javier Valverde-Muñoz, M. Carmen Muñoz, Maksym Seredyuk, José Antonio Real|2017|Inorg.Chem.|56|13535|doi:10.1021/acs.inorgchem.7b02272

Space GroupCrystallography(N1N2-bis(quinolin-8-yl)ethane-12-diamine)-bis(isothiocyanato)-iron(ii)Crystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1572180: Experimental Crystal Structure Determination

2017

Related Article: Carlos Bartual-Murgui, Lucía Piñeiro-López, F. Javier Valverde-Muñoz, M. Carmen Muñoz, Maksym Seredyuk, José Antonio Real|2017|Inorg.Chem.|56|13535|doi:10.1021/acs.inorgchem.7b02272

Space GroupCrystallographyCrystal System(N1N2-bis(quinolin-8-yl)ethane-12-diamine)-bis(selenocyanato)-ironCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1879899: Experimental Crystal Structure Determination

2019

Related Article: Francisco Javier Valverde-Muñoz, Maksym Seredyuk, Manuel Meneses-Sánchez, M. Carmen Muñoz, Carlos Bartual-Murgui, José A. Real|2019|Chemical Science|10|3807|doi:10.1039/C8SC05256E

Space GroupCrystallographyCrystal System(NNN-tris(2-(((1-n-butyl-1H-imidazol-2-yl)methylidene)amino)ethyl)amine)-iron bis(hexafluoroarsenate hexafluorophosphate)Crystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1879896: Experimental Crystal Structure Determination

2019

Related Article: Francisco Javier Valverde-Muñoz, Maksym Seredyuk, Manuel Meneses-Sánchez, M. Carmen Muñoz, Carlos Bartual-Murgui, José A. Real|2019|Chemical Science|10|3807|doi:10.1039/C8SC05256E

Space GroupCrystallography(NNN-tris(2-(((1-n-butyl-1H-imidazol-2-yl)methylidene)amino)ethyl)amine)-iron bis(hexafluoroarsenate)Crystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1572183: Experimental Crystal Structure Determination

2017

Related Article: Carlos Bartual-Murgui, Lucía Piñeiro-López, F. Javier Valverde-Muñoz, M. Carmen Muñoz, Maksym Seredyuk, José Antonio Real|2017|Inorg.Chem.|56|13535|doi:10.1021/acs.inorgchem.7b02272

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters(N1N2-bis(quinolin-8-yl)ethane-12-diamine)-bis(isothiocyanato)-nickel(ii)Experimental 3D Coordinates
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CCDC 2072901: Experimental Crystal Structure Determination

2021

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2017

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CCDC 1965275: Experimental Crystal Structure Determination

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researchProduct

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2020

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researchProduct

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2020

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CCDC 1965272: Experimental Crystal Structure Determination

2020

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researchProduct

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researchProduct

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2018

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researchProduct

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2020

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researchProduct

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2019

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researchProduct

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2017

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researchProduct

CCDC 2072904: Experimental Crystal Structure Determination

2021

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researchProduct

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2020

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researchProduct

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2021

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researchProduct

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2021

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researchProduct

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2020

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researchProduct

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2018

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researchProduct

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2019

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CCDC 2018388: Experimental Crystal Structure Determination

2020

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CCDC 1585094: Experimental Crystal Structure Determination

2018

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Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinatescatena-(bis(mu-44'-(ethene-12-diyl)dipyridine)-tetrakis(mu-thiocyanato)-bis(thiocyanato)-iron-di-mercury)
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CCDC 1910591: Experimental Crystal Structure Determination

2019

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CCDC 1585095: Experimental Crystal Structure Determination

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Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterscatena-(bis(mu-44'-(hydrazine-12-diylidenedimethylylidene)dipyridine)-tetrakis(mu-thiocyanato)-bis(thiocyanato)-iron-di-mercury methanol solvate)Experimental 3D Coordinates
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CCDC 1965271: Experimental Crystal Structure Determination

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Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterscatena-((mu-44'-(anthracene-910-diyl)dipyridine)-tetrakis(mu-cyano)-di-gold-iron)Experimental 3D Coordinates
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CCDC 1852562: Experimental Crystal Structure Determination

2018

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catena-[pentakis(mu-cyano)-(mu-44'4''4'''-(benzene-1245-tetrayltetra(ethyne-21-diyl))tetrapyridine)-iron(ii)-tri-silver(i) monohydrate]Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1989162: Experimental Crystal Structure Determination

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CCDC 1965270: Experimental Crystal Structure Determination

2020

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Space GroupCrystallographyCrystal Systemcatena-(bis(mu-44'-(anthracene-910-diyl)dipyridine)-octakis(mu-cyano)-di-iron-tetra-gold)Crystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1862017: Experimental Crystal Structure Determination

2018

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CCDC 1572179: Experimental Crystal Structure Determination

2017

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CCDC 2090596: Experimental Crystal Structure Determination

2021

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CCDC 1572178: Experimental Crystal Structure Determination

2017

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CCDC 2090597: Experimental Crystal Structure Determination

2021

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CCDC 1989158: Experimental Crystal Structure Determination

2020

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CCDC 2090599: Experimental Crystal Structure Determination

2021

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CCDC 2018383: Experimental Crystal Structure Determination

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CCDC 1917750: Experimental Crystal Structure Determination

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