0000000000338586

AUTHOR

W. Seiler

showing 2 related works from this author

Commissioning of the vacuum system of the KATRIN Main Spectrometer

2016

The KATRIN experiment will probe the neutrino mass by measuring the β-electron energy spectrum near the endpoint of tritium β-decay. An integral energy analysis will be performed by an electro-static spectrometer (``Main Spectrometer''), an ultra-high vacuum vessel with a length of 23.2 m, a volume of 1240 m[superscript 3], and a complex inner electrode system with about 120 000 individual parts. The strong magnetic field that guides the β-electrons is provided by super-conducting solenoids at both ends of the spectrometer. Its influence on turbo-molecular pumps and vacuum gauges had to be considered. A system consisting of 6 turbo-molecular pumps and 3 km of non-evaporable getter strips ha…

010302 applied physicsPhysicsLight nucleusPhysics - Instrumentation and DetectorsSpectrometerSpectrometersPhysics::Instrumentation and DetectorsVacuum-basedFOS: Physical sciencesInstrumentation and Detectors (physics.ins-det)01 natural sciencesEnergy analysisNuclear physics0103 physical sciencesEnergy spectrumGas systems and purificationNeutrino detectorsddc:620010306 general physicsInstrumentationMathematical PhysicsEngineering & allied operationsKATRINdetectors
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Method for determination of formaldehyde in air in the pptv-range by HPLC after extraction as 2,4-dinitrophenyl-hydrazone

1982

The derivatization of formaldehyde with 2,4-dinitrophenylhydrazine and the extraction of the product formalhydrazone is studied. The determination is carried out by HPLC. Applying a cryogenic sampling technique and a sampling volume of 300l of air the detection limit of formaldehyde in air is 30 pptv and this is suitable for measurements of formaldehyde in the atmosphere. (IFU)

chemistry.chemical_classificationDetection limitChromatographyChemistryClinical BiochemistryExtraction (chemistry)FormaldehydeHydrazoneGeneral MedicineHigh-performance liquid chromatographyAnalytical Chemistrychemistry.chemical_compoundGeneral Materials ScienceDinitrophenylDerivatizationFresenius' Zeitschrift für analytische Chemie
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