Author: Wolfgang Schmitt-sody

0000000000862959

AUTHOR

Wolfgang Schmitt-sody

showing 2 related works from this author

Umsetzung von amino-aziminen mit basen

1980

Abstract Amino-azimines of type (1) react at room temperature with bases (ammonia, aliphatic amines, hydrazine and methyl-hydrazine, aqueous/ethanolic sodium hydroxide) by cleavage of the to the and the NNN moieties (azide).

chemistry.chemical_compoundAmmoniaAqueous solutionchemistrySodium hydroxideOrganic ChemistryDrug DiscoveryHydrazinePolymer chemistryOrganic chemistryAzideCleavage (embryo)BiochemistryTetrahedron Letters

researchProduct

Mechanismus der Umsetzung von 1,1-Diphenylhydrazin mit Azodicarbonsäure-diethylester

1979

Bei der Umsetzung von 1,1-Diphenylhydrazin (1a) mit Azodicarbonsaure-diethylester (2a) uber-lagern sich funf Reaktionsmechanismen: A und B) Oxidation des Diphenylhydrazins 1a durch den Azodicarbonsaureester 2a zum Aminonitren 8; Bildung des Tetrazens 10 entweder durch Dimerisierung von 8 oder uber das Tetrazan 11; Zerfall von 11 in N2 und Diphenylamin. — C) Addition des Aminonitrens 8 an den Azodicarbonsaureester 2a zum Aminoazimin 3a; Zerfall von 3a in das Urethan 4a und den Azidoameisensaureester 5a. — D) Isomerisierung des Aminoazimins 3a zu 13 und Reduktion von 13 durch 1a zum Tetrazen 14; Spaltung von 14 in Diphenylamin und das Azid 15; Zerfall von 15 in Ethylcyanat (17) und den Kohlen…

Diethyl azodicarboxylatechemistry.chemical_compoundEthanolchemistryTetrazeneOrganic ChemistryDiphenylamineAzidePhysical and Theoretical ChemistryCyanateMedicinal chemistryEthyl formateDiimineLiebigs Annalen der Chemie

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