0000000001303529

AUTHOR

Anne Lüpke

showing 7 related works from this author

Front Cover: Filling the Gap in the Metallacrown Family: The 9‐MC‐3 Chromium Metallacrown (Chem. Eur. J. 13/2021)

2021

CrystallographyChromiumFront coverchemistryOrganic ChemistryStructural integritychemistry.chemical_elementGeneral ChemistryMetallacrownCatalysisChemistry – A European Journal
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Unsymmetrical Iron P-NH-P' Catalysts for the Asymmetric Pressure Hydrogenation of Aryl Ketones.

2017

R.H.M. thanks NSERC Canada for a Discovery grant and the Canada Council for the Arts for a Killam Fellowship. This work was also made possible by the SCICOMP NMR facilities provided by the Canada Foundation for Innovation, project number 19119, and the Ontario Ministry of Research, Innovation and Science. The Deutscher Akademischer Austauschdienst (DAAD) is thanked for support for A.P. Calculations were performed using the facilities of SHARCNET and Scinet of Compute/Calcul Canada

010405 organic chemistryArylOrganic ChemistryNoyori asymmetric hydrogenationGeneral Chemistry010402 general chemistry01 natural sciencesCatalysis0104 chemical sciencesCatalysischemistry.chemical_compoundchemistryOrganic chemistryChristian ministryChemistry (Weinheim an der Bergstrasse, Germany)
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Filling the Gap in the Metallacrown Family: The 9‐MC‐3 Chromium Metallacrown

2021

Abstract In this work, we report on a long‐sought missing complex in the metallacrown family. We synthesized and characterized the novel chromium metallacrown (MC) complex {CrIII(μ 2‐piv)3[9‐MCCr(III)N(shi)‐3](morph)3}⋅MeOH (in which shi3−=salicyl hydroxamate, piv=pivalate, and morph=morpholine). The MC with a 9‐MC‐3 cavity of kinetically inert chromium(III) ions was synthesized by a solvothermal reaction. Magnetization measurements reveal a high spin ground state.

9-MC-3540 Chemistry and allied sciencesCluster Compounds | Hot PaperCommunicationOrganic Chemistrykinetic stabilityStructural integritychemistry.chemical_elementGeneral ChemistrySolvothermal reactionCatalysisCommunicationsIonmetallacrownMagnetizationCrystallographyChromiumchemistry.chemical_compoundstructural integritychemistry540 ChemieMorpholinechromiumGround stateMetallacrownChemistry (Weinheim an Der Bergstrasse, Germany)
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CCDC 1525652: Experimental Crystal Structure Determination

2017

Related Article: Samantha A. M. Smith, Paraskevi O. Lagaditis, Anne Lüpke, Alan J. Lough, Robert H. Morris|2017|Chem.-Eur.J.|23|7212|doi:10.1002/chem.201701254

carbonyl-(chloro)-[2-(diphenylphosphanyl)-N-{2-[bis(propan-2-yl)phosphanyl]ethyl}-1-phenylethan-1-amine]-(hydrido)-ironSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1525651: Experimental Crystal Structure Determination

2017

Related Article: Samantha A. M. Smith, Paraskevi O. Lagaditis, Anne Lüpke, Alan J. Lough, Robert H. Morris|2017|Chem.-Eur.J.|23|7212|doi:10.1002/chem.201701254

carbonyl-dichloro-[2-(diphenylphosphanyl)-N-{2-[bis(propan-2-yl)phosphanyl]ethyl}-1-phenylethan-1-amine]-ironSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1538240: Experimental Crystal Structure Determination

2017

Related Article: Samantha A. M. Smith, Paraskevi O. Lagaditis, Anne Lüpke, Alan J. Lough, Robert H. Morris|2017|Chem.-Eur.J.|23|7212|doi:10.1002/chem.201701254

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterscarbonyl-(dichloro)-[1-(diphenylphosphanyl)-N-{2-[bis(propan-2-yl)phosphanyl]ethyl}-3-methylbutan-2-amine]-ironExperimental 3D Coordinates
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CCDC 2047296: Experimental Crystal Structure Determination

2021

Related Article: Anne Lüpke, Luca M. Carrella, Eva Rentschler|2021|Chem.-Eur.J.|27|4283|doi:10.1002/chem.202004947

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinatestris(mu-N2-dioxidobenzene-1-carboximidato)-tris(mu-pivalato)-tris(morpholine)-tetra-chromium(iii) methanol solvate
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