Determination of biogenic amines in meat by combined ion-exchange capillary gas chromatography

6533b7dbfe1ef96bd1270190

RESEARCH PRODUCT

Determination of biogenic amines in meat by combined ion-exchange capillary gas chromatography

Jana Slemr Klaus Beyermann

subject

Biogenic Amines Chromatography Gas Meat Swine Tetraphenylborate Biochemistry Gas Chromatography-Mass Spectrometry Analytical Chemistry chemistry.chemical_compound Cadaverine Putrescine Animals Chemical Precipitation Trifluoroacetic Acid Perchloric acid Cadaverine Chromatography Ion exchange Precipitation (chemistry)Organic Chemistry General Medicine Chromatography Ion Exchange Capillary gas chromatography chemistry Putrescine Histamine Histamine

description

Abstract A procedure is described for the determination of putrescine, cadaverine and histamine in meat. Crude perchloric acid extracts were pre-separated on a weakly acidic cation exchanger and the amines quantified by capillary gas chromatography. The diamines were analysed as trifluoroacetyl derivatives and histamine was converted into N α -trifluoroacetyl-N τ -ethoxycarbonylhistamine. The accuracy of the determination of diamines was examined by a precipitation pre-separation method and by mass fragmentometric quantification. The proposed procedure allows the sensitive, sufficiently precise and highly specific determination of putrescine and cadaverine in meat.

year	journal	country	edition	language
1984-01-20	Journal of Chromatography A

https://doi.org/10.1016/s0021-9673(00)96259-9

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