PHOSPHORORGANISCHE VERBINDUNGEN 115 WEGE ZUM ANALYTISCHEN NACHWEIS VON VERBINDUNGEN MIT DER P(O)F- UND P(O)SR-GRUPPE

6533b7dcfe1ef96bd1271cb9

RESEARCH PRODUCT

PHOSPHORORGANISCHE VERBINDUNGEN 115 WEGE ZUM ANALYTISCHEN NACHWEIS VON VERBINDUNGEN MIT DER P(O)F- UND P(O)SR-GRUPPE

Leopold Horner Werner Hallenbach

subject

Reaction conditions Chemistry Stereochemistry Medicinal chemistry Fluorescence

description

Abstract Acridine-9-hydroxamicacid 5 is suitable for the analytical detection of the model phosphorylfluorides 7 by fluorescence. The model compounds are rearranged according to Lossen and degradated to the fluorescent 9-aminoacridine 6 using defined reaction conditions. Thiophospho-S-esters (with diethyl-thiophosphinicacid-S-butylester 8 as a model compound) are cleaved to the corresponding phosphoryl-fluorides (a) and mercaptanes (b) by fluorolysis. (a) is identified qualitatively with acridine-9-hydroxamicacid 5, (b) by the Ellman-reaction. Zum Fluoreszenznachweis der Modellphosphorylfluoride 7 ist Acridin-9-hydroxamsaure 5 geeignet. Die Modellverbindungen 7 werden unter Einhaltung definierter Bedingungen nach Lossen umgelagert und zum fluoreszierenden 9-Aminoacridin 6 abgebaut. Thiophospho-S-ester (Modell: Diethylthiophosphinsaure-S-butylester 8) werden durch Fluorolyse in die entsprechenden Phosphorylfluoride (a) und Mercaptane (b) uberfuhrt. (a) wird mit Acridin-9-hydroxamsaure 5 und (b) nach Ellman...

year	journal	country	edition	language
1984-08-01	Phosphorus and Sulfur and the Related Elements

https://doi.org/10.1080/03086648408077639

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