6533b827fe1ef96bd1285dea
RESEARCH PRODUCT
High-pressure flow-injection assembly. Indirect determination of glycine by atomic absorption spectrometry.
J. Martínez CalatayudJ. V. García Mateosubject
AnalyteAnalytical chemistryGlycinechemistry.chemical_elementBiochemistryAnalytical Chemistrylaw.inventionchemistry.chemical_compoundlawElectrochemistryCalibrationEnvironmental ChemistrySpectroscopychemistry.chemical_classificationChromatographyChemistrySpectrophotometry AtomicTemperatureHydrogen-Ion ConcentrationCopperAmino acidLinear rangeGlycineCarbonic AcidCarbonateIndicators and ReagentsAtomic absorption spectroscopydescription
A procedure for the determination of glycine is described. The method is based on the reaction of the analyte with finely powdered, solid copper(II) carbonate in a continuous-flow assembly. The optimum experimental conditions of pH, temperature, sample volume, flow-rate, column length and internal diameter, and the linear range of calibration, were studied. Interference from foreign substances that accompany this amino acid in pharmaceutical formulations was studied, and the method was applied to the determination of glycine.
year | journal | country | edition | language |
---|---|---|---|---|
1991-03-01 | The Analyst |