6533b82dfe1ef96bd1290bb5

RESEARCH PRODUCT

Manganese iron oxide superparamagnetic powder by mechanochemical processing. Nanoparticles functionalization and dispersion in a nanofluid

A. La BarberaMariangela BellusciChiara AliottaChiara AliottaDino FioraniDavide PeddisFranco PadellaDaniela SecciMartina PilloniMartina Pilloni

subject

Materials scienceNanoparticlechemistry.chemical_elementBioengineeringNanotechnologyFerrite; Ferrofluid; Magnetic nanoparticles; Mechanochemical synthesis; Nanomedicine; Synthesis of nanofluidsManganeseNanofluidSynthesis of nanofluidsGeneral Materials ScienceFerriteGeneral ChemistryMagnetic nanoparticlesFerrite Mechanochemical synthesisFerrofluid NanomedicineSynthesis of nanofluidsCondensed Matter PhysicsAtomic and Molecular Physics and OpticsNanomedicinechemistryChemical engineeringFerrofluidModeling and SimulationMagnetic nanoparticlesSurface modificationNanomedicineFerrite (magnet)Magnetic nanoparticlesMechanochemical synthesisSuperparamagnetism

description

Manganese ferrite nanoparticles were synthesized using a High-Energy Ball-Milling mechanochemical method. After 1 h of milling, the process produces a material consisting of single crystalline domain nanoparticles having a diameter of about 8 nm. Chemical properties of the synthesized powders allow an easy functionalization with citric acid. Both as-obtained and functionalized samples show superparamagnetic behaviour at room temperature, and the functionalized powder is stably dispersible in aqueous media at physiological pH. The average hydrodynamic diameter is equal to similar to 60 nm. Nanoparticles obtained by the reported High-Energy Ball-Milling method can be synthesized with high yield and low costs and can be successfully utilized in ferrofluids development for biomedical applications.

10.1007/s11051-012-0904-7https://dx.doi.org/10.1007/s11051-012-0904-7