6533b873fe1ef96bd12d5637
RESEARCH PRODUCT
Automated Photo-Induced Fluorescence Determination of Flumetsulam
D. López MaloJ. Martínez CalatayudR. Garrido Medinasubject
AnalyteChromatographyAqueous solutionChemistryBiochemistry (medical)Clinical BiochemistryExtraction (chemistry)Fluorescence spectrometryAnalytical chemistryBiochemistryFluorescenceAnalytical ChemistryCartridgeFluorometerElectrochemistrySample preparationSpectroscopydescription
The present article deals with a new procedure for determination of the herbicide flumetsulam. The fluorimetric procedure is performed on the basis of photo-increased fluorimetric emission of the pesticide solution and by means of a multicommutation continuous-flow assembly. The alkaline solution containing the analyte is irradiated online and then directly forced through the fluorimeter flow cell. The analysis of different samples is completely automated, as the analyte separation was performed online by including a separation cartridge in the manifold. When dealing with solid samples (such as soil samples), the automation was completed by adding to the manifold the corresponding device for the aqueous extraction of the analyte from the sample suspension.
year | journal | country | edition | language |
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2009-06-05 | Analytical Letters |