Search results for " NEUTRON"
showing 10 items of 618 documents
A possible solution of the puzzling variation of the orbital period of MXB 1659-298
2017
MXB 1659-298 is a transient neutron star Low-Mass X-ray binary system that shows eclipses with a periodicity of 7.1 hr. The source went to outburst in August 2015 after 14 years of quiescence. We investigate the orbital properties of this source with a baseline of 40 years obtained combining the eight eclipse arrival times present in literature with 51 eclipse arrival times collected during the last two outbursts. A quadratic ephemeris does not fit the delays associated with the eclipse arrival times and the addition of a sinusoidal term with a period of $2.31 \pm 0.02$ yr is required. We infer a binary orbital period of $P=7.1161099(3)$ hr and an orbital period derivative of $\dot{P}=-8.5(…
Combined SANS and SAXS experiments in polyolefins-hydrogenated oligocyclopentadiene (HOCP) blends
1998
Abstract Lamellar morphology in semicrystyalline polymer blends (iPP/HOCP and HDPE/HOCP) is investigated by means of Small Angle X-ray Scattering (SAXS) and Small Angle Neutron Scattering (SANS). The investigated blends present a complex phase diagram, as they show a miscibility gap. SAXS scattering curves of blends lying outside the miscibility gap can be analysed in the frame of the psuedo two phase model. In order to describe the complex morphology of blends lying inside the miscibility gap, the SANS technique revealed necessary. In this paper a novel method to describe the morphology of these complex systems by means of SANS is presented.
Scattering studies of large scale structures at the ultra small angle neutron scattering instrument S18
2002
Abstract In recent years ultra small angle neutron scattering (USANS) has developed into a powerful standard method for large scale structure investigations. The upgraded instrument S18 at the ILL's 58 MW high flux reactor is operated routinely with increasing beam time demand. The performance of the instrument and its abilities will be discussed in this paper. A peak to background ratio better than 10 5 is reached using Agamalian's tail reduction method. A q -range from 2.10 −5 up to 5.10 −2 A −1 can be covered. This allows a clear overlap with standard pinhole SANS instruments. The new way collecting scattering data logarithmically equidistant in q -space saves measuring time. This allows…
Structural and dynamical characterization of melt PEO–salt mixtures
2002
Abstract Salt doped poly ethylene oxide (PEO) mixtures were investigated by means of both small angle neutron scattering and QENS techniques aiming to characterize morphological and dynamical features in the melt state. These experimental evidences provide support to the proposed heterogeneous scenario for polymer electrolytes. In particular, the existence of PEO–cation complexes is proposed to play a major role in intramolecular cooperation and intermolecular transient crosslinks, which affects the mixture properties.
Mixed micelles composed of Peptides and Gadolinium complexes as tumor-specific contrast agents in MRI: a SANS study
2004
A detailed structural investigation on mixed micelle aggregates as target-specific contrast agents for magnetic resonance imaging technique has been carried out by way of small angle neutron scattering measurements. These mixed micelles are formed by two new amphiphilic molecules formed by a bioactive peptide and a claw moiety. The first molecule, C18H37CONH(AdOO)(x)-G-CCK8 (C18LxCCK8, x = 2, 5), contains an 18-carbon-atom alkylic chain bound to the C-terminal of the cholecystokinin octapeptide amide (CCK 26-33 or CCK8) and is able to bind to the overexpressed CCK receptor of some tumor cells. The second molecule, C(18)H(37)CONHLys(DTPAGlu)CONH25- (C18DTPAGlu) or its gadolinium complex [C(1…
Micelles formed from photochemically active amphiphiles: structural characterization by small-angle neutron scattering
1996
Abstract A novel class of photochemically active amphiphiles has been synthesized containing a ketone moiety as a biradical or radical pair precursor on the hydrophobic tail of sodium sulfate surfactants. Alteration of the molecular structure of each ketone-containing surfactant allows for the systematic and predictable manipulation of the micellar size and shape, both of which are important in determining the coupling between the unpaired electrons confined within the micelle and the intraradical dynamics. The structure of the resulting aggregates has been analyzed by small-angle neutron scattering (SANS). The results show that the amphiphiles form ellipsoidal micelles with aggregation num…
Antiferromagnetism and the node structure of the superconducting order parameter of UPd Al
2000
The node structure of the superconducting order parameter of the heavy-fermion system is analyzed within the weak-coupling theory. A pairing interaction induced by the exchange of antiferromagnetic spin excitations is assumed as suggested by recent inelastic neutron scattering experiments and tunneling spectroscopy. The multi-sheeted Fermi surface is taken into account. Based on a model susceptibility for the simple antiferromagnetic structure of , line nodes result at the rim of the magnetic Brillouin zone.
Superconductivity mediated by spin fluctuations in the heavy-fermion compound UPd2 Al3
1999
It is well known that any weak attractive electron–electron interaction in metals can in principle cause the formation of Cooper pairs, which then condense into a superconducting ground state1. In conventional superconductors, this attractive interaction is mediated by lattice vibrations (phonons). But for the heavy-fermion and high-temperature superconductors, alternative pairing interactions are considered to be possible2. For example, the low-temperature properties of heavy-fermion systems are dominated by antiferromagnetic spin fluctuations, which have been considered theoretically3 as a possible cause for Cooper-pair formation. This picture recently received some experimental support: …
A combined small-angle neutron and X-ray scattering study of block copolymers micellisation in supercritical carbon dioxide
2003
Small angle neutron and X-ray scattering (SANS and SAXS) are used to investigate the monomer–aggregate transition of fluorocarbon–hydrocarbon diblock copolymers in supercritical carbon dioxide. SANS data are analyzed using a polydisperse sphere core–shell model. Synchrotron SAXS data have been collected by profiling the pressure at different temperatures, and critical micellization densities have been obtained for a series of diblock solutions. Finally pressure jump experiments, combined with synchrotron SAXS, have revealed two steps in the dynamics of the formation of the aggregates.
Measuring Multiple Residual-Stress Components using the Contour Method and Multiple Cuts
2009
The conventional contour method determines one component of residual stress over the cross section of a part. The part is cut into two, the contour (topographic shape) of the exposed surface is measured, and Bueckner’s superposition principle is analytically applied to calculate stresses. In this paper, the contour method is extended to the measurement of multiple residual-stress components by making multiple cuts with subsequent applications of superposition. The theory and limitations are described. The theory is experimentally tested on a 316L stainless steel disk with residual stresses induced by plastically indenting the central portion of the disk. The multiple-cut contour method resu…