Search results for " Synthesis"
showing 10 items of 1625 documents
Industrial Microreactor Process Development up to Production
2008
This chapter is about industrial applications of microprocess technology. Industry is not very active in publishing not only because of confidentiality reasons but also because of the absence of direct need for a corresponding profile. Thus, one cannot expect that the ongoing developments can be shown with a similar degree of completeness, clarity and detailedness, as this is possible for reviewing scientific contributions from academy with a wealth of peer-reviewed papers. Especially, the information of major interest of what has been transferred to production and how do the companies make profit with the new technology is usually kept secret. Thus, it has to be accepted that some informat…
Method for designing PI-type fuzzy controllers for induction motor drives
2001
The paper illustrates a new systematic method for designing PI-type fuzzy controllers for direct field-oriented controlled induction motor drives. First, linear and decoupled models expressing the dynamics of speed, rotor flux, direct and inquadrature stator currents are derived using a nonlinear static compensator and choosing convenient input variables. Then, to guide the dynamics of the above quantities, four conventional PI controllers are designed independently, choosing their bandwidths conveniently. Finally, the input and output scale factors of PI-type fuzzy controllers are derived from the conventional PI controller parameters. The whole drive controller also includes a rotor flux …
Stereo to Wave-Field Synthesis music up-mixing: An objective and subjective evaluation
2008
Sound source separation techniques are known to be very useful in many applications. High fidelity and audio oriented applications are a challenging issue in this topic, however, existing algorithms are far from performing with such a high quality. In this paper, a subjective and objective evaluation are carried out for several algorithms designed for dealing with stereo music mixtures. The performance of these algorithms applied to acoustic scene resynthesis in a Wave Field Synthesis system is discussed.
Hardware implementation of a robust adaptive filter: Two approaches based in High-Level Synthesis design tools
2009
Abstract Adaptive filters are used in a wide range of applications. Impulsive noise affects the proper operation of the filter and the adaptation process. This noise is one of the most damaging types of signal distortion, not always considered when implementing algorithms. Field Programmable Gate Array (FPGA) are widely used for applications where timing requirements are strict. Nowadays, two main design processes can be followed, namely, Hardware Description Language (HDL) and a High Level Synthesis (HLS) design tool for embedded system design. This paper describes the FPGA implementation of an adaptive filter robust to impulsive noise using two approaches based in HLS and the implementati…
Optimum design of two-level MCML gates
2008
In this paper, we address the problem of the optimum design of two-level MOS Current Mode Logic (MCML) gates. In particular, we describe a design methodology based on the concept of crossing-point current already introduced for the optimum design of single-level MCML gates. This methodology is suited both for automated implementation and graphic estimate of the optimum design. Moreover, it clearly shows how some important design parameters affect the optimum values of delay and power consumption. Several gates were designed in an IBM 130 nm CMOS technology. The results of SPICE simulations, reported here, demonstrate the effectiveness of the proposed design methodology.
Preparation of photocatalysts by chemical methodologies
2021
Abstract The synthesis of photocatalytic materials is an important task for obtaining better results in terms of activity and/or selectivity in photocatalysis. This chapter reports an overview of the main methodologies using physical techniques to obtain bulky, supported powders or films and coatings to be used as heterogeneous photocatalysts. The classical chemical methodologies for the preparation of photocatalytic materials are presented in the previous chapter, so the information presented here complements the aforementioned one. Materials scientists and engineers have made significant progresses in the improvement of methods of synthesis of nanomaterial solids by developing different a…
Electro-organic synthesis – a 21st century technique
2020
The severe limitations of fossil fuels and finite resources influence the scientific community to reconsider chemical synthesis and establish sustainable techniques. Several promising methods have emerged, and electro-organic conversion has attracted particular attention from international academia and industry as an environmentally benign and cost-effective technique. The easy application, precise control, and safe conversion of substrates with intermediates only accessible by this method reveal novel pathways in synthetic organic chemistry. The popularity of electricity as a reagent is accompanied by the feasible conversion of bio-based feedstocks to limit the carbon footprint. Several mi…
Trimeprazine is enantioselectively degraded by an activated sludge in ready biodegradability test conditions
2018
[EN] A great number of available pharmaceuticals are chiral compounds. Although they are usually manufactured as racemic mixtures, they can be enantioselectively biodegraded as a result of microbial processes. In this paper, a biodegradability assay in similar conditions to those recommended in OECD tests of enantiomers of trimeprazine (a phenothiazine employed as a racemate) is carried out. Experiments were performed in batch mode using a minimal salts medium inoculated with an activated sludge (collected from a Valencian Waste Water Treatment Plant, WWTP) and supplemented with the racemate. The concentration of the enantiomers of trimeprazine were monitored by means of a chiral HPLC metho…
Microwave-assisted synthesis of PHEA-oligoamine copolymers as potential gene delivery systems
2009
Aims - Copolymers bearing oligoamines and having buffering capacity in the endosomal pH range seems very promising as non viral vectors in gene delivery, due to the great importance of endosomal escaping for an efficient endocellular DNA release. Aim of this paper was to prepare new copolymers based on α,β-poly-(N-2-hydroxyethyl)-D,L-aspartamide (PHEA) as polymeric backbone and bearing an oligoamine, such as diethylentriamine (DETA) in the side chain and useful for gene delivery. Moreover in order to reduce solvent volume and to make faster the reaction, microwave-assisted has been used. Materials and methods - PHEA copolymers bearing different amount of DETA were prepared by using bis(4-ni…
ChemInform Abstract: Organocatalytic Enantioselective Friedel-Crafts Alkylation of 1-Naphthol Derivatives and Activated Phenols with Ethyl Trifluorop…
2016
Financial support from the MINECO [Gobierno de Espana and FEDER (EU)] (CTQ2013-47949-P) and from Generalitat Valenciana (ISIC2012/001) is gratefully acknowledged. M.M.-M. thanks the Universitat de Valencia for a predoctoral grant. C. V. thanks MINECO for JdC contract. Access to NMR and MS facilities from the Servei central de support a la investigacio experimental (SCSIE)-UV is also acknowledged.