Search results for " Synthesis"

showing 10 items of 1625 documents

Synthesis and evaluation of microtubule assembly inhibition and cytotoxicity of prenylated derivatives of cyclo-l-Trp-l-Pro

2000

The synthesis of three isoprenylated derivatives of cyclo-L-Trp-L-Pro is described. These substances have been evaluated for cytotoxic activity in rat normal fibroblast 3Y1 cells and have also been evaluated in vitro for the inhibition of microtubule assembly.

IndolesStereochemistryClinical BiochemistryProtein PrenylationMitosisPharmaceutical ScienceMicrotubulesPeptides CyclicBiochemistryChemical synthesisPiperazinesIndole AlkaloidsMicrotubuleDrug DiscoverymedicineAnimalsFibroblastCytotoxicityMolecular BiologyCells Culturedchemistry.chemical_classificationMolecular StructureChemistryOrganic ChemistryBiological activityFibroblastsIn vitroCyclic peptideRatsmedicine.anatomical_structureBiochemistryCell cultureMolecular MedicineCattleMicrotubule-Associated ProteinsBioorganic & Medicinal Chemistry
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THIOPYRANO[2,3-E]INDOL-2-ONES: ANGELICIN HETEROANALOGUES WITH POTENT PHOTOANTIPROLIFERATIVE ACTIVITY

2008

A new class of compounds, the thiopyrano[2,3-e]indol-2-ones, bioisosters of the angular furocoumarin angelicin, was synthesized with the aim of obtaining new photochemotherapeutic agents. In particular 7,8-dimethyl-thiopyranoindolone 6c s showed a remarkable phototoxicity and a great dose UVA dependence reaching IC(50) values at submicromolar level. This latter photoinduced a massive apoptosis and a remarkable photodamage to lipids and proteins. Although it did not intercalate DNA, it was able to cause photooxidation of DNA bases.

IndolesStereochemistryDNA damageUltraviolet RaysAngelicinThiopyrano[23-e ]indol-2-oneClinical BiochemistryPharmaceutical ScienceHL-60 CellsApoptosisThiopyrano[2Antiproliferative activityBiochemistryChemical synthesischemistry.chemical_compoundInhibitory Concentration 50Jurkat CellsAngelicinPhotochemotherapeutic agentsFurocoumarinsDrug DiscoveryThiolactoneTumor Cells CulturedHumansPhotosensitizer3-e ]indol-2-onesMolecular BiologyPhotosensitizing AgentsFurocoumarinOrganic ChemistryProteinsBiological activityThiopyrano[2; 3-e ]indol-2-ones; Angelicin; Antiproliferative activity; Photochemotherapeutic agents; ApoptosisDNASettore CHIM/08 - Chimica FarmaceuticaMitochondriachemistryPhotochemotherapeutic agentMolecular MedicineLipid PeroxidationPhototoxicityDNA Damage
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Stereoselective Synthesis of Enantiomerically Pure Nupharamine Alkaloids from Castoreum

2009

An animalic note: The first total synthesis of the all-cis nupharamine 2, an alkaloid from beaver castoreum, is based on the stereoselective domino Mannich-Michael reaction of N-galactosylfurylaldimine to give 1 (Piv = pivaloyl), subsequent conjugate cuprate addition, and stereoselective protonation of the enolate. These reactions are all controlled by the carbohydrate. Protonation of the enolate after cleavage of the auxiliary leads to epimer 3.

IndolizidinesIndolizidinesTerpenesChemistryStereochemistryEnantioselective synthesisTotal synthesisRodentiaStereoisomerismProtonationStereoisomerismNupharamineGeneral ChemistryCatalysischemistry.chemical_compoundAlkaloidsPiperidinesAnimalsStereoselectivityEpimerScent GlandsFuransAngewandte Chemie International Edition
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ChemInform Abstract: Inhibitors of Inducible NO Synthase Expression: Total Synthesis of (S)-Curvularin (Ia) and Its Ring Homologues.

2008

Inducible no synthaseBiochemistryChemistryTotal synthesisGeneral MedicineCurvularinRing (chemistry)ChemInform
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Towards efficient inductive synthesis from input/output examples

1994

Inductive synthesisInput/outputComputer scienceFormal languageBrute-force searchArithmeticAlgebraic expression
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ADT implementation and completion by induction from examples

1991

There exists a fast algorithm [2] for inductive synthesis of terminating and ground confluent term rewriting systems from samples. The principles of this algorithm and the methodology of its use for implementation and completion of abstract data types are described.

Inductive synthesisNormalization propertyTheoryofComputation_MATHEMATICALLOGICANDFORMALLANGUAGESComputer scienceExistential quantificationRewritingAbstract data typeAlgorithmFast algorithmTerm (time)
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Inductive synthesis of term rewriting systems

2005

Fast algorithm for inductive synthesis of term rewriting systems is described and proved to be correct. It is implemented and successfully applied for inductive synthesis of different algorithms, including the binary multiplication. The algorithm proposed supports automatic learning process and can be used for designing and implementation of ADT.

Inductive synthesisTheoryofComputation_MATHEMATICALLOGICANDFORMALLANGUAGESComputer scienceBinary multiplicationProcess (computing)RewritingAutomatic learningAbstract data typeAlgorithmFast algorithmTerm (time)
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Machine Learning-Based View Synthesis in Fourier Lightfield Microscopy

2022

Current interest in Fourier lightfield microscopy is increasing, due to its ability to acquire 3D images of thick dynamic samples. This technique is based on simultaneously capturing, in a single shot, and with a monocular setup, a number of orthographic perspective views of 3D microscopic samples. An essential feature of Fourier lightfield microscopy is that the number of acquired views is low, due to the trade-off relationship existing between the number of views and their corresponding lateral resolution. Therefore, it is important to have a tool for the generation of a high number of synthesized view images, without compromising their lateral resolution. In this context we investigate h…

InformáticaMicroscopyFourier lightfield microscopy; view synthesis; neural radiance fields; 3D microscopyComputingMethodologies_IMAGEPROCESSINGANDCOMPUTERVISIONBiochemistryComputer scienceAtomic and Molecular Physics and OpticsAnalytical ChemistryMachine LearningMicroscòpiaInstrumento ópticoImaging Three-DimensionalTecnología avanzadaAlgoritmoNeural radiance fields3D microscopyFourier lightfield microscopyElectrical and Electronic EngineeringView synthesisFourier Anàlisi deInstrumentation
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Rational design of a fluopyram hapten and preparation of bioconjugates and antibodies for immunoanalysis

2015

A fluopyram hapten was designed in which insignificant electronic and structural modifications were foreseen and all potentially interacting chemical moieties were maintained. This hapten was prepared by total synthesis and three immunologically active bioconjugates were obtained and characterized. High-affinity and specific antibodies to fluopyram were raised.

InmunoanalysisbiologySDHI fungicidesGeneral Chemical EngineeringRational designTotal synthesischemical and pharmacologic phenomenaGeneral Chemistrychemistry.chemical_compoundSpecific antibodychemistryBiochemistrybiology.proteinFluopyramAntibodyHaptenHaptens
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One‐pot synthesis of [2+2]‐helicate‐like macrocycle and 2+4‐μ 4 ‐oxo tetranuclear open frame complexes: Chiroptical properties and asymmetric oxidati…

2020

Inorganic Chemistry010405 organic chemistryChemistryPolymer chemistryFrame (networking)One-pot synthesisOxidative coupling of methaneGeneral ChemistrySelf-assembly010402 general chemistry01 natural sciences0104 chemical sciencesApplied Organometallic Chemistry
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