Search results for " Total"

KOSMOS 2018 Gran Canaria mesocosm study: particle flux data from sediment trap

2021

The data set compiles sinking flux data collected during a KOSMOS mesocosm experiment carried out in the frame work of the Ocean Artificial Upwelling project. The experiment was performed in the North-East Atlantic Ocean off the coast of Gran Canaria in autumn 2018 and lasted for 39 days. In this study we investigated the effect of different intensities of artificial upwelling combined with two upwelling modes (recurring additions versus one singular addition) on POC export and its potential transfer efficiency to depth. The data set includes the amounts of surface water that were exchanged with nutrient-rich deep water (from ~300 m depth). It also contains particle flux data, i.e. POC flux…

Detection, characterization and sizing of hydrogen induced cracking in pressure vessels using phased array ultrasonic data processing

2016

Abstract Pressure vessels operating in sour service conditions in refinery environments can be subject to the risk of H₂S cracking resulting from the hydrogen entering into the material. This risk, which is related to the specific working conditions and to the quality of the steel used, shall be properly managed in order to maintain the highest safety at a cost-effective level. Nowadays the typical management strategy is based on a risk based inspection (RBI) evaluation to define the inspection plan used in conjunction with a fitness for service (FFS) approach in defining if the vessel, although presenting dangerous defects such as cracks, can still be considered “fit for purpose” for a giv…

Determination of quality parameters of beers by the use of attenuated total reflectance-Fourier transform infrared spectroscopy

2005

Abstract The estimation of important quality parameters of beers, such as original and real extracts and alcohol content, has been evaluated by attenuated total reflectance-Fourier transform infrared spectroscopy (ATR-FTIR) using a partial least square (PLS) calibration approach. Two sample populations, one consisting of 24 samples and other of 21 samples, obtained from the Spanish market and covering different types of beer were used. The first set was used for building and validating the model, whereas the second, measured 6 months after, was used for evaluating its robustness. The spectral range and the size of the calibration set and its suitability for building the PLS model have been …

Comparison between topographic and photogrammetric techniques for deformation monitoring of the dome of the Massimo Theatre in Palermo

2012

This paper shows the first results of a study aimed at monitoring the deformations of the dome of the Massimo Theatre in Palermo caused by thermal dilatations, with the use of topographic and photogrammetric integrated techniques. Particularly, two robotic total stations and high precision digital photogrammetric systems were employed. In order to correlate the displacements of the rollers on which the steel structure of the dome rest with the thermal gradients, different thermal images were acquired by a thermal imaging camera. The main goal of the work was to compare the two techniques with reference to very small (submillimeter) deformation measurements. The obtained results show that th…

Monitoraggio delle deformazioni della cupola del Teatro Massimo di Palermo con l’impiego di tecniche topografiche e fotogrammetriche integrate.

2012

L’articolo riporta i primi risultati di uno studio finalizzato al monitoraggio delle deformazioni della cupola del Teatro Massimo di Palermo provocate dalle dilatazioni termiche, con l’impiego di tecniche topografiche e fotogrammetriche integrate. In particolare, sono state utilizzate due stazioni totali robotizzate e sistemi di fotogrammetria digitale di elevata precisione. Per correlare gli spostamenti dei carrelli sui quali poggia la struttura in acciaio della cupola con i gradienti termici, sono state acquisite immagini termiche diversificate. L’obiettivo principale del lavoro consisteva nel confronto delle due tecniche di rilievo in relazione a misure di deformazione di entità molto ri…

Monitoraggio topografico e fotogrammetrico della cupola del teatro Massimo

2012

L’articolo riporta i primi risultati di uno studio finalizzato al monitoraggio delle deformazioni della cupola del Teatro Massimo di Palermo provocate dalle dilatazioni termiche, con l’impiego di tecniche topografiche e fotogrammetriche integrate. In particolare, sono state utilizzate due stazioni totali robotizzate e sistemi di fotogrammetria digitale di elevata precisione. Per correlare gli spostamenti dei carrelli sui quali poggia la struttura in acciaio della cupola con i gradienti termici, sono state acquisite immagini termiche diversificate. L’obiettivo principale del lavoro consisteva nel confronto delle due tecniche di rilievo in relazione a misure di deformazione di entità molto ri…

Preliminary studies about thermal degradation of edible oils through attenuated total reflectance mid-infrared spectrometry

2009

Abstract Degradation of edible oils during their heating process has been evaluated through the determination of cis -unsaturation and trans -fatty acids together with free fatty acids as a function of time and temperature heating. Two types of cooking oils, sunflower and seed (mixture of different seeds non-detailed), were heated at three different temperatures (147, 171 and 189 °C) during a total time of 1920 min (32 h) shared out in four sessions of 8 h each one, and samples were studied from their spectra obtained by Fourier transform infrared spectrometry using attenuated total reflectance measurements. A critical comparison between different multivariate calibration models built based…

Implosión democrática / 1

2008

Comparative study of reflectance cells for PLS-FTIR determination of sugars in soft drinks

1998

A comparative study has been carried out between a horizontal Attenuated Total Reflectance (h-ATR) cell and a Cylindrical Internal Reflection (CIR) cell (CIRCLE cell). Both cells were employed for the determination of glucose, fructose, sucrose and total sugar in soft drinks and fruit juices using absorbance measurements at two resolution values (4 and 8 cm–1). Data were processed by Partial Least Squares regression (PLS). Using a resolution of 4 cm–1, mean relative errors of prediction from 0.6% to 1.3% were obtained using the horizontal-ATR and from 0.6% to 2.8% using the CIRCLE cell resulting in a limit of detection from 0.03% in the case of sucrose to 0.21% for total sugar for the h-ATR…

Direct ATR-FTIR determination of sucrose in beet root.

2000

A simple and fast procedure has been developed for the direct determination of sucrose in beet root samples through attenuated total reflectance Fourier transform infrared absorbance measurements (ATR-FTIR) at 1056 cm(-1) with a baseline established between 1187 and 887 cm(-1). The method only requires a previous crushing or liquefaction of samples and it is free from matrix effects and from the interference of minoritary sugars and fermentation molecules. Aqueous solutions of sucrose can be used as standards and recovery values from 101 to 103% were found for spiked concentration levels from 3.5 to 10.5% (w/w). The limit of detection provided by this method corresponds to 0.15% (w/w) of su…