Search results for "ALLOYS"
showing 10 items of 1689 documents
Defect characterization in Al welded joints by non-contact Lamb wave technique
2006
Abstract The use of air-coupled sensors to detect flaws in Al welded joints and the advantage of Lamb wave for their characterization has been proved. Ultrasonic waves were generated by a pulsed laser and by contact angle-beam transducer, and received by an air-coupled capacitive transducer. Laser-based configuration was used to quickly locate the defect, whereas the angle-beam contact probe configuration to characterize it thanks to the dispersive behavior of Lamb waves. Guided waves allow inspection of the complete thickness with only one scan, permitting to detect and to size both internal and surface defects; their high flexibility in the measurement is due to the various parameters cha…
Study of magnesium and aluminum alloys absorption coefficient during Nd:YAG laser interaction
2007
International audience; In laser processes, the absorption factor of laser Nd:YAG by metals plays a very important role. In order to model laser welding, we need to know its evolution during the process. The theoretical calculation does not enable the prediction of the absorption factor in the case of a keyhole mode. It is difficult to predict the effect of plasma and recoil pressure on the shape of the keyhole. In this paper, an integrating sphere is used to determine the absorption factor during the laser process, which is carried out on two types of magnesium alloys (WE43 and RZ5) and an aluminum alloy. We obtain the evolution in time of the absorption factor according to different steps…
Effect of alloy type and casting technique on the fracture strength of implant-cemented structures.
2010
Objectives: To evaluate the influence of alloy type and casting procedure on the fracture strength (FS) of metallic frameworks for implant-supported fixed prostheses. Study design: Thirty three-unit structures for lower posterior bridges were waxed-up and randomly assigned to two groups (n=15) according to alloy type and casting technique: Group 1 (C): cobalt-chromium cast in a centrifugal machine (TS1, Degussa-Hüls); Group 2 (T): titanium cast in a pressure-differential device (Cyclarc II, Morita). Each structure was cemented onto two prefabricated abutments under a constant seating pressure. After 6 months of water aging, samples were loaded in a static universal testing machine (EFH/5/FR…
Non-destructive technique to detect local buried defects in metal sample by scanning microwave microscopy
2012
International audience; Based on the skin effect, our recent developments using scanning microwave microscopy lead to propose a non-destructive method to detect located buried defect in metal samples like stainless steel. A 3D tomography is possible by taking advantage of microwave measurement, using a vector network analyzer in bandwidth frequencies, and the nanometer resolution positioning capabilities with atomic force microscopy. At each used frequency, an incident electromagnetic wave is sent to the sample and the reflected wave gives information on a specific depth layer in the material. With diagnostic tools of nanotechnologies (SEM. AFM, etc.), different stainless steel samples (fro…
Hybrid electrochemical/electrochromic Cu(II) ion sensor prototype based on PANI/ITO-electrode
2017
Abstract Conducting polymer polyaniline (PANI) based electrochromic films were electrochemically synthesized on indium tin oxide (ITO) covered glass electrodes and their electrochromic performances were investigated by spectroscopic methods before and after the incubation in Cu(II) ion containing aqueous solution. Chemical structure of synthesized PANI layer was evaluated by FTIR. The electrochromic performance of PANI film was determined by measuring of spectroscopic signals before and after the incubation of PANI film coated electrode in Cu(II) ion containing solution. During the change of potential, which was applied to PANI-modified electrode, the colour of PANI thin film turned from gr…
Benzene monitoring by micro-machined sensors with SnO2 layer obtained by using micro-droplet deposition technique
2011
International audience; SnO2 thin layers were deposited by the way of the micro-droplet technique. The sensor substrate consisted of a thin membrane developed on oxidised silicon wafer. The sensing layers were deposited by means of the micro-droplet technique into thin layers of about 100 nm. Such devices were tested for benzene detection. The obtained results showed a very high sensitivity for this chemical compound since 500 ppb were detected. The results presented in this paper were not focused on the reactional mechanism of benzene detection but rather on the development of a cheap and sensitive sensor using sol-gel and micro-droplet processes. Since these layers were elaborated using s…
Silica nanoparticle core structure examined by the E?Si? center 29Si strong hyperfine interaction
2015
Abstract β-Ray irradiation up to 1.2 GGy was employed to induce E′Si γ defects and to study the structure of silica nanoparticles with diameters from 7 up to 20 nm. Defect concentration and their 29 Si strong hyperfine doublet were investigated through electron paramagnetic resonance measurements. Our data indicate that stable defects are located in the nanoparticle core. Furthermore, the E′Si γ hyperfine interaction evidences that the core structure is denser than bulk silica and independent from the particle size. Finally, we put in evidence that the core structure is stable and unaffected by the irradiation in the investigated dose range maintaining the specific features of nanoparticles.
A nanostructured sensor of hydrogen peroxide
2017
Abstract A nanostructured electrochemical sensor of hydrogen peroxide was fabricated growing self-standing Pd nanowires (Pd NWs) into polycarbonate (PC) membranes through a simple metal galvanic deposition. Conditions of deposition were adjusted in order to attain 2–5 μm long Pd wires. Characterization of Pd-NWs was performed by scanning electrode microscopy, energy-dispersive X-ray spectroscopy and X-ray diffraction. Properties of the nanostructured sensor were studied by cyclic voltammetry and chronoamperometry in phosphate buffer—ethanol solution. Addition of pure ethanol to the test solution was essential in order to increase wettability of the nanostructures. Sensing features were comp…
Mesenchymal stem cell proliferation and differentiation on load-bearing trabecular Nitinol scaffolds.
2013
Bone tissue regeneration in load-bearing regions of the body requires high-strength porous scaffolds capable of supporting angiogenesis and osteogenesis. 70% porous Nitinol (NiTi) scaffolds with a regular 3-D architecture resembling trabecular bone were produced from Ni foams using an original reactive vapor infiltration technique. The "trabecular Nitinol" scaffolds possessed a high compressive strength of 79 MPa and high permeability of 6.9×10(-6) cm2. The scaffolds were further modified to produce a near Ni-free surface layer and evaluated in terms of Ni ion release and human mesenchymal stem cell (hMSC) proliferation (AlamarBlue), differentiation (alkaline phosphatase activity, ALP) and …
Ordering and dewetting in spin-coated films of a liquid crystalline main chain polymer
2006
Abstract The ordering of spin-coated films of a main-chain smectic liquid crystalline polymer with an azobenzene group connected by flexible spacers to a phenyl malonate unit has been studied as a function of film thickness using scanning force microscopy and UV/Vis spectroscopy. Already the as-prepared films are characterized by a significant out-of-plane orientation of the azobenzene groups. Annealing of films thicker than 7 nm results in aggregation and homeotropical alignment of azobenzene groups forming smectic layers parallel to the substrate. An optically isotropic mesophase was found upon annealing in the temperature range of smectic mesophase. Films thinner than the bilayer thickne…