Search results for "Biological activity"

showing 10 items of 465 documents

Novel bioactive bromopyrrole alkaloids from the Mediterranean sponge Axinella verrucosa

2005

The Mediterranean sponge Axinella verrucosa has been investigated for its alkaloid composition and has been found to produce a complex mixture of bromopyrrole alkaloids. Along with the previously isolated compounds 5-18, four novel alkaloids of this class, compounds 1-4, have been isolated, and their structures established through spectroscopic methods. Compounds 1-4 were found to display neuroprotective activity against the agonists serotonin and glutamate in vitro.

SerotoninSpectrometry Mass Electrospray Ionizationendocrine systemAxinella verrucosaMagnetic Resonance SpectroscopyStereochemistryClinical BiochemistryThin layerGlutamic AcidPharmaceutical ScienceSpectrometry Mass Fast Atom BombardmentPharmacognosycomplex mixturesBiochemistryAnimal originPyrrole derivativesNatural productCell LineAlkaloidsBromopyrrole alkaloidDrug DiscoveryAnimalsPyrrolesheterocyclic compoundsMolecular BiologyNeuronsMarine spongeMolecular StructurebiologyChemistryorganic chemicalsAlkaloidOrganic ChemistryQuisqualic AcidBiological activitybiology.organism_classificationPoriferaSpongeNeuroprotective activity.Axinella verrucosaMolecular MedicineCalciumChromatography Thin LayerSerotonin AntagonistsExcitatory Amino Acid Antagonists
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Anti-inflammatory glycoterpenoids from Scrophularia auriculata.

2000

The activity of the four glycoterpenoids: two saponins, verbascosaponin A and verbascosaponin, and two iridoids, scropolioside A and scrovalentinoside, isolated from Scrophularia auriculata ssp. pseudoauriculata, were studied in different models of acute and chronic inflammation. Both saponins significantly inhibited the mouse paw edema induced by carrageenan and ear edema induced by single and multiple doses of 12-O-tetradecanoylphorbol 13-acetate (TPA). Verbascosaponin A showed a potency twice as high as that of indomethacin in the acute TPA model. Verbascosaponin A and scropolioside A were active after a long latency period against ethyl phenylpropiolate edema, as are glucocorticoids. Wh…

Serotoninmedicine.drug_classAnti-Inflammatory AgentsInflammationPharmacognosyPharmacologyAnti-inflammatoryCapillary Permeabilitychemistry.chemical_compoundMiceGlucosidesEdemaMedicineAnimalsEdemaHypersensitivity DelayedIridoidsGlycosidesPyransPharmacologyPlants Medicinalbiologybusiness.industryTerpenesBiological activityEarScrophularia auriculataSaponinsbiology.organism_classificationTriterpenesCarrageenanMechanism of actionchemistryImmunologyIridoid GlycosidesTetradecanoylphorbol AcetateFemalemedicine.symptombusinessEuropean journal of pharmacology
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Silyl modification of biologically active compounds. 13. Synthesis, cytotoxicity and antibacterial action ofN-methyl-N-(2-triorganylsiloxyethyl)-1,2,…

2012

A series of N-methyl-N-(2-triorganylsiloxyethyl)-1,2,3,4-tetrahydro(iso)quinolinium iodides has been synthesized via dehydrocondensation reaction of N-(2-hydroxyethyl)-1,2,3,4-tetrahydroisoquinoline, N-(2-hydroxyethyl)-1,2,3,4-tetrahydroquinoline and 4,4-dimethyl-N-(2-hydroxyethyl)-4-sila-1,2,3,4-tetrahydroisoquinoline with trialkyl(aryl)hydrosilanes and subsequent alkylation, and characterized by 1H, 13C and 29Si NMR and mass spectroscopy. The biological activity data exhibited a marked enhancement of inhibitory activity against tumour cell lines and almost all the test bacterial/fungal strains in comparison with their 2-hydroxyethyl precursors. Cytotoxicity in the microgram range against …

SilylationStereochemistryArylBiological activityGeneral ChemistryAlkylationmedicine.diseaseInorganic Chemistrychemistry.chemical_compoundchemistryCell culturemedicineCholineCytotoxicityFibrosarcomaApplied Organometallic Chemistry
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Guanaconetins, new antitumoral acetogenins, mitochondrial complex I and tumor cell growth inhibitors

2005

The antitumoral activity of a series of acetylated bis-tetrahydrofuranic acetogenins with a threo/trans/threo/trans/erythro relative configuration was characterized by four new natural and two semisynthetic, 15,24,30-trioxygenated acetogenins that were found to inhibit mitochondrial complex I enzyme as well as growth of several tumor cell lines. Placement of acetyl groups along the alkyl chain modulated the potency of the bis-tetrahydrofuranic acetogenins and could be important for future utilization of these compounds as chemotherapeutic agents.

Spectrometry Mass Electrospray IonizationMagnetic Resonance SpectroscopyAcetogeninsStereochemistryClinical BiochemistryPharmaceutical ScienceAntineoplastic AgentsBiochemistryChemical synthesisLactonesStructure-Activity Relationshipchemistry.chemical_compoundCell Line TumorNeoplasmsDrug DiscoveryHumansStructure–activity relationshipMolecular BiologyCell Proliferationchemistry.chemical_classificationElectron Transport Complex IMolecular StructureChemistryCell growthOrganic ChemistryBiological activityGrowth InhibitorsEnzymeBiochemistryAcetylationCell cultureAcetogeninMolecular MedicineFatty AlcoholsBioorganic & Medicinal Chemistry
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Structural analysis of the lipid A isolated from Hafnia alvei 32 and PCM 1192 lipopolysaccharides[S]

2010

Hafnia alvei, a Gram-negative bacterium, is an opportunistic pathogen associated with mixed hospital infections, bacteremia, septicemia, and respiratory diseases. The majority of clinical symptoms of diseases caused by this bacterium have a lipopolysaccharide (LPS, endotoxin)-related origin. The lipid A structure affects the biological activity of endotoxins predominantly. Thus, the structure of H. alvei lipid A was analyzed for the first time. The major form, asymmetrically hexa-acylated lipid A built of beta-D-GlcpN4P-(1-->6)-alpha-D-GlcpN1P substituted with (R)-14:0(3-OH) at N-2 and O-3, 14:0(3-(R)-O-12:0) at N-2', and 14:0(3-(R)-O-14:0) at O-3', was identified by ESI-MS(n) and MALDI-tim…

Spectrometry Mass Electrospray IonizationendotoxinLipopolysaccharideAcylationOligosaccharidesQD415-436BiochemistryMicrobiologyLipid Achemistry.chemical_compoundOpportunistic pathogenEndocrinologyPalmitoylationEscherichiapalmitoylationmass spectrometryPolish Collection of MicroorganismsbiologyHafnia alveiBiological activityCell Biologybiology.organism_classificationOxygenHafnia alveiLipid AchemistrySpectrometry Mass Matrix-Assisted Laser Desorption-Ionizationlipids (amino acids peptides and proteins)BacteriaResearch ArticleJournal of Lipid Research
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Sarcophytolide: a new neuroprotective compound from the soft coral Sarcophyton glaucum

1998

Abstract Bioactivity-guided fractionation of an alcohol extract of the soft coral Sarcophyton glaucum collected from the intertidal areas and the fringing coral reefs near Hurghada, Red Sea, Egypt resulted in the isolation of a new lactone cembrane diterpene, sarcophytolide. The structure of this compound was deduced from its spectroscopic data and by comparison of the spectral data with those of known closely related cembrane-type compounds. In antimicrobial assays, the isolated compound exhibited a good activity towards Staphylococcus aureus, Pseudomonas aeruginosa , and Saccharomyces cerevisiae. Sarcophytolide was found to display a strong cytoprotective effect against glutamate-induced …

Staphylococcus aureusProgrammed cell deathSecondary metaboliteToxicologyNeuroprotectionCnidariaMicechemistry.chemical_compoundmedicineAnimalsRats WistarGlutamate receptorNeurotoxicityBiological activitymedicine.diseaseMolecular biologyRatsNeuroprotective AgentsProto-Oncogene Proteins c-bcl-2chemistryBiochemistryNMDA receptorCalciumDiterpenesDiterpenemedicine.drugToxicology
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Novel pathogenic mechanism of microbial metalloproteinases: liberation of membrane-anchored molecules in biologically active form exemplified by stud…

1996

Certain membrane-anchored proteins, including several cytokines and cytokine receptors, can be released into cell supernatants through the action of endogenous membrane-bound metalloproteinases. The shed molecules are then able to fulfill various biological functions; for example, soluble interleukin-6 receptor (sIL-6R) can bind to bystander cells, rendering these cells sensitive to the action of IL-6. Using IL-6R as a model substrate, we report that the metalloproteinase from Serratia marcescens mimics the action of the endogenous shedding proteinase. Treatment of human monocytes with the bacterial protease led to a rapid release of sIL-6R into the supernatant. This effect was inhibitable …

Staphylococcus aureusProteasesmedicine.medical_treatmentImmunologyBiologyMatrix metalloproteinaseMicrobiologyMonocytesSubstrate SpecificityAntigens CDChlorocebus aethiopsmedicineAnimalsHumansReceptorSerratia marcescensMetalloproteinaseProteaseMembrane ProteinsMetalloendopeptidasesBiological activityBacterial InfectionsReceptors InterleukinListeria monocytogenesReceptors Interleukin-6Recombinant ProteinsBlotInfectious DiseasesSolubilityBiochemistryPseudomonas aeruginosaParasitologySignal transductionResearch ArticleSignal TransductionInfection and Immunity
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4-Diazopyrazole Derivatives as Potential New Antibiofilm Agents

2008

<i>Background:</i> The recognition that chronic infections and infections associated with medical devices are biofilm related has been the impulse for investigating the antibiofilm properties of some diazopyrazoles biologically active as antimicrobials. <i>Methods:</i> The susceptibility of staphylococcal biofilms was determined at concentrations ranging from 25 to 1.5 µg/ml using crystal violet and methylthiazotetrazolium (MTT) staining. In the case of <i>Candida albicans,</i> we first assessed the anti-germ tube formation effect of 4-NO<sub>2</sub> (compound 1c) and then we evaluated its antibiofilm activity at concentrations ranging from 10…

StaphylococcusGerm tubeMicrobiologychemistry.chemical_compoundCandida albicansDrug DiscoveryPharmacology (medical)Crystal violetCandida albicansPharmacologyTube formationAza CompoundsMolecular StructurebiologyStaphylococcus biofilms Candida Albicans biofilms Antibiofilms activity DiazopyrazolesBiofilmBiological activityGeneral Medicinebiology.organism_classificationAntimicrobialSettore CHIM/08 - Chimica FarmaceuticaCorpus albicansInfectious DiseasesOncologychemistryBiofilmsPyrazoles
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Novel Acylated Triterpene Glycosides from Muraltia heisteria

2002

Four new acylated triterpene glycosides (1-4) have been isolated as two inseparable mixtures of the trans- and cis-3,4,5-trimethoxycinnamoyl derivatives (1,2 and 3,4) from the roots of Muraltia heisteria. The structures of these compounds were elucidated by various 1D and 2D NMR techniques, including (1)H and (13)C, COSY, NOESY, HSQC, TOCSY, and HMBC experiments and FABMS. Compounds 3 and 4 were shown to be cytotoxic in a human colon cancer cell line but did not show any ability to potentiate in vitro cisplatin cytotoxicity.

StereochemistryAcylationSaponinPharmaceutical ScienceStereoisomerismPharmacognosyPlant RootsAnalytical ChemistrySouth AfricaTriterpeneDrug DiscoveryTumor Cells CulturedHumansOrganic chemistryNuclear Magnetic Resonance BiomolecularChromatography High Pressure LiquidPharmacologychemistry.chemical_classificationMolecular StructureChemistryHydrolysisOrganic ChemistryGlycosideStereoisomerismBiological activitySaponinsAntineoplastic Agents PhytogenicTriterpenesTerpenoidPolygalaceaeComplementary and alternative medicineMolecular MedicineCisplatinDrug Screening Assays AntitumorHT29 CellsTwo-dimensional nuclear magnetic resonance spectroscopyJournal of Natural Products
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N-Heterocyclic choline analogues based on 1,2,3,4-tetrahydro(iso)quinoline scaffold with anticancer and anti-infective dual action

2016

Pharmacological effects of biologically active “small molecules” can be improved by their targeted modification, which affects drug delivery and interaction with tumor cells and microorganisms. We aimed to evaluate anticancer and antimicrobial activity of lipid-like choline derivatives modified via simultaneous introduction of tetrahydro(iso)quinoline based pharmacophore system at nitrogen atom and long chain alkyl substituent at oxygen atom. Target compounds were synthesized under phase-transfer catalysis conditions followed by quaternization, and evaluated for cytotoxicity and NO-generation ability on HT-1080 and MG-22A tumor cell lines and NIH 3T3 normal mouse fibroblasts, and screened f…

StereochemistryAntineoplastic AgentsMicrobial Sensitivity TestsGram-Positive Bacteriamedicine.disease_cause01 natural sciencesDNA gyraseCholineInhibitory Concentration 50Mice03 medical and health scienceschemistry.chemical_compoundDrug Delivery Systems0302 clinical medicineAnti-Infective AgentsCell Line TumorNeoplasmsGram-Negative BacteriamedicineAnimalsHumansCytotoxicityEscherichia coliPharmacologybiology010405 organic chemistryQuinolineFungiBiological activityGeneral MedicineAntimicrobialbiology.organism_classificationProteus mirabilis0104 chemical scienceschemistry030220 oncology & carcinogenesisNIH 3T3 CellsQuinolinesAntibacterial activityPharmacological Reports
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