Search results for "COLUMN"

HIGH-RESOLUTION PALAEONVIRONMENTAL RECONSTRUCTION OF ODP HOLE 963D (SICILY CHANNEL) DURING THE LAST DEGLACIATION BASED ON CALCAREOUS NANNOFOSSILS

2004

Abstract A palaeoenvironmental reconstruction of Ocean Drilling Program (ODP) Hole 963D (Sicily Channel) has been obtained on the basis of quantitative abundance fluctuations in the calcareous nannofossil assemblages. The studied hole is characterized by a very high sedimentary resolution and covers the last ca. 20 kyr. A new palaeoclimatic curve, based on the Gephyrocapsa muellerae/Upper Photic Zone (UPZ) group ratio, permitted the detection of the rapid climatic fluctuations that characterized the last deglaciation. Cold water masses occupied the Sicily Channel during the glacial period and the Younger Dryas, whereas they were generally warm during the Bolling–Allerod and the Holocene. An…

Spatial distribution of phytoplankton and picocyanobacteria in Lake Tanganyika in March and April 1998

2003

The spatial distribution of phytoplankton and picocyanobacteria was studied in Lake Tanganyika in relation to environmental factors. Sampling was conducted within three weeks during the wet season of 1998 when the water column stratification was most stable. The secchi depth varied between 11 and 16 m, except off the river Malagarasi (3 m). The depth of the euphotic zone was 33 to 56 m. Altogether, 218 phytoplankton taxa were identified. Their total biomass varied between 13 and 88 mg m−3 fresh weight. Picocyanobacteria were present at very high densities (104 to 6 × 10 5 cells ml−1). The influence of the river Malagarasi appeared to spread along the water surface because of the lower densi…

2019

We report a complete genome sequence of a Finnish isolate of the fish pathogen Flavobacterium columnare . Using PacBio RS II sequencing technology, the complete circular genome of F. columnare strain B185 with 3,261,404 bp was obtained.

Determination of 5-nitrofurylacrylic acid in wines by high-performance liquid chromatography

1988

The use of core-shell high-performance liquid chromatography column technology to improve biogenic amine quantification in wine

2015

BACKGROUND HPLC column technology has been improved, providing better resolution of closely eluting compounds, better analyte sensitivity, and shorter analysis times. The core-shell technology columns offer a faster analysis through the use of shorter columns without compromising resolution. The aim of this work was to improve the methods for determination of biogenic amines (BAs) in wine using the new HPLC PFP core-shell column technology. RESULTS Two different elution programs were designed to quantify BAs with the core-shell PFP column. Program I flow rate was 2 mL min−1. The total elution time was 10 min. In elution program II, the flow rate was 0.8 mL min−1 and the total elution time w…

Comparison of two serially coupled column systems and optimization software in isocratic liquid chromatography for resolving complex mixtures.

2012

Although there is a great deal of stationary phases having different selectivities (even practically orthogonal selectivities), these very rarely are taken as a factor to be optimized during method development. The chromatographer selects the stationary phase usually in a trial-and-error fashion (or based on the solute nature and expected interactions), and then optimizes continuous factors as the mobile phase composition, pH, temperature and flow-rate. However, the optimization of the stationary phase nature and column length (which are discrete factors) may be interesting. In this regard, the optimization of the coupling of individual columns may yield separations that are not possible wi…

Modelling and simulation of gas-liquid hydrodynamics in mechnically stirred tanks

2007

Abstract Computational fuid dynamics (CFD) is an increasingly important tool for carrying out realistic simulations of process equipment. In the case of multiphase systems the development of CFD models is less advanced than for single-phase systems. In the present work CFD simulations of gas–liquid stirred tanks are reported. An Eulerian–Eulerian multi-fluid approach is used in conjunction with the simplest two-phase extension of the k–ɛ turbulence model. All bubbles are assumed to share the same size. The effect of inter-phase forces on simulation results is separately considered. As concerns drag, it is shown that the sole parameter needed to characterize the dispersed phase behaviour is …

Efficient and Mild Ytterbium(III)-Catalyzed Tosylation of Alcohols.

2004

Ytterbium(III) trifluoromethanesulfonate efficiently catalyzes the reaction of primary and secondary alcohols with toluenesulfonic acid anhydride to yield the alkyl tosylates in high yields. The reactions were carried outunder neutral and mild conditions and product purification was easily achieved by means of short column chromatography.

Mercosur en marcha

2004

Leaching of glyphosate and AMPA under two soil management practices in Burgundy vineyards (Vosne-Romanée, 21-France)

2005

Some drinking water reservoirs under the vineyards of Burgundy are contaminated with herbicides. Thus the effectiveness of alternative soil management practices, such as grass cover, for reducing the leaching of glyphosate and its metabolite, AMPA, through soils was studied. The leaching of both molecules was studied in structured soil columns under outdoor conditions for 1 year. The soil was managed under two vineyard soil practices: a chemically treated bare calcosol, and a vegetated calcosol. After 680 mm of rainfall, the vegetated calcosol leachates contained lower amounts of glyphosate and AMPA (0.02% and 0.03%, respectively) than the bare calcosol leachates (0.06% and 0.15%, respectiv…