Search results for "Diffraction"
showing 10 items of 1584 documents
Preparation of superconducting thin films of UNiAl
2005
Abstract Epitaxial thin films of the unconventional heavy fermion superconductor UNi 2 Al 3 we prepared by coevaporation of the elementary components in a molecular beam epitaxy system (MBE). The phase purity and structural quality of the films deposited on (0 1 0)- or (1 1 2)-oriented YAlO 3 substrates were studied by X-ray diffraction and RHEED. The observed R ( T ) behavior is consistent with data obtained from bulk samples and proves the purity of the films. Superconductivity was found with transition temperature T c =0.97 K.
Enhanced Surface Ligands Reactivity of Metal Clusters by Bulky Ligands for Controlling Optical and Chiral Properties.
2021
Surface ligands play critical roles in determining the surface properties of metal clusters. However, modulating the properties and controlling the surface structure of clusters through surface‐capping agent displacement remain a challenge. In this work, a silver cluster, [Ag 14 (SPh(CF 3 ) 2 ) 12 (PPh 3 ) 4 (DMF) 4 ] ( Ag 14 ‐DMF , where HSPh(CF 3 ) 2 is 3,5‐bis(trifluoromethyl)benzenethiol, PPh 3 is triphenylphosphine and DMF is N,N‐Dimethylformamide), with weakly coordinated DMF ligands on the surface silver sites, was synthesized by using a mixed ligands strategy (bulky thiolates, phosphines and small solvents). The as‐prepared Ag 14 ‐DMF is a racemic mixture of chiral molecules. Owing …
A study of a differential method for a field diffracted by a rough surface
2006
Since more than one decade, a new generation of microscopes was developed. It is about near field microscopes. Among these devices, we are interested in the PSTM (Photon Scanning Tunnelling Microscopy). Images obtained by this instrument do not reflect, with a better resolution, the topography of the studied samples. In order to improve the performance of this apparatus, several models have been developed. In our case, we propose to retake, by using a differential method, the study of a rough surface. The surface is modelled as two pavements of different sizes and refractive indices. Theoretically, the obtained results agree well with results obtained for a surface having submicronic asperi…
Superresolved Holographic Microscopy
2008
Superresolution methods in digital holographic microscopy provide a useful tool to overcome the Abbe's diffraction limit when using modest microscope lenses. The process improves the cutoff frequency of the microscope lens by means of the generation of a synthetic aperture based on time multiplexing and using 3 main stages: optical coding, optical decoding, and digital postprocessing. After the whole process, a superresolved image is obtained by Fourier transformation of the synthetic aperture.
Superesolution in digital holographic microscopy
2011
In this contribution, we address with the possibility to overcome the limited resolving power of imaging systems beyond the limit imposed by Abbe's diffraction theory. We first review the mathematical foundations underlying superresolution (SR) from an information theory point of view and then we focus on two multiplexing approaches in digital holographic microscopy (DHM) for achieving SR by synthetic aperture (SA) generation.
Synthetic Aperture Lensless Digital Holographic Microscopy (SALDHM) for Superresolved Biological Imaging
2013
Lensless digital holographic microscopy (LDHM) relates with the capability to achieve microscopic imaging working without lenses in the regime of holography. LDHM uses an extremely simplified setup and provides micron-range lateral and depth resolutions in three-dimensional (3D) imaging. Typically, LDHM uses a pinhole to provide spherical divergent illumination over the sample. Then, two different basic schemes are usually adopted for providing holographic recording. The first one assumes the interference between two in-line waves since diffraction by the sample can be considered as a perturbation of the reference wave. The second scheme uses an external reference beam in an off-line config…
Wideband THz time domain spectroscopy based on optical rectification and electro-optic sampling
2013
We present an analytical model describing the full electromagnetic propagation in a THz time-domain spectroscopy (THz-TDS) system, from the THz pulses via Optical Rectification to the detection via Electro Optic-Sampling. While several investigations deal singularly with the many elements that constitute a THz-TDS, in our work we pay particular attention to the modelling of the time-frequency behaviour of all the stages which compose the experimental set-up. Therefore, our model considers the following main aspects: (i) pump beam focusing into the generation crystal; (ii) phase-matching inside both the generation and detection crystals; (iii) chromatic dispersion and absorption inside the c…
Investigation of AC Electrical Properties of MXene-PCL Nanocomposites for Application in Small and Medium Power Generation
2021
The paper examined Ti3C2Tx MXene (T—OH, Cl or F), which is prepared by etching a layered ternary carbide Ti3AlC2 (312 MAX-phase) precursor and deposited on a polycaprolactone (PCL) electrospun membrane (MXene-PCL nanocomposite). X-ray Diffraction analysis (XRD) and Scanning Electron Microscopy (SEM) indicates that the obtained material is pure Ti3C2 MXene. SEM of the PCL-MXene composite demonstrate random Ti3C2 distribution over the nanoporous membrane. Results of capacitance, inductance, and phase shift angle studies of the MXene-PCL nanocomposite are presented. It was found that the frequency dependence of the capacitance exhibited a clear sharp minima in the frequency range of 50 Hz to o…
Multiplexing THz Vortex Beams With a Single Diffractive 3-D Printed Lens
2019
[EN] We present a novel method for experimentally generating multiplexed THz vortex beams by using a single three-dimensional printed element that combines a set of radially distributed spiral phase plates, and a binary focusing Fresnel lens. With this element, we have experimentally demonstrated that THz multiplexing can be tailored to fit within a small space on an optical bench. Results are presented beside numerical simulations, demonstrating the robust nature of the experimental method.
High-pressure X-ray diffraction study of EuWO4 to 12 GPa
2005
In-situ high-pressure X-ray diffraction studies were performed on EuWO4 to 12 GPa. We found that EuWO4 transforms from the tetragonal I41/a structure to the monoclinic I2/a structure at 8.5(5) GPa, being this phase transition re- versible. No other structural change is detected up to 12 GPa. The EOS of EuWO4 is determined from the pressure–volume data. (© 2005 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim)