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showing 10 items of 91 documents
Absolute crystallinity and photocatalytic activity of brookite TiO2 samples
2017
Abstract This study reports a method to determine the absolute crystallinity of partly crystalline brookite TiO2 photocatalysts. A natural, a commercial and various home-prepared brookite powders were characterized by X-ray diffraction analysis, Raman spectroscopy, scanning electron microscopy, UV–vis diffuse reflectance spectroscopy and nitrogen adsorption measurements. The absolute crystallinity was calculated from the ratio between the full width at half maximum intensity of the (121) X-ray diffraction peaks of the brookite samples and the (111) peak of CaF2 as internal standard. The photocatalytic activity of the powders was tested employing the photodegradation of 4-nitrophenol as well…
Fabrication of long period fiber gratings of subnanometric bandwidth.
2017
This paper reports on the fabrication of long period fiber gratings having subnanometric bandwidth in the 1500 nm spectral region. Large gratings have been photo-inscribed in a high NA fiber, the grating pitch and the order of the HE cladding mode are optimized to produce gratings with a large number of periods and preventing the coupling to TE, TM or EH modes. Resonances with a FWHM of 0.83 nm and 0.68 nm have been achieved for gratings 15 and 20 cm long respectively, the free spectral range between transmission notches is 125 nm. The polarization effects and the sensitivity of the gratings to temperature and to strain variations are presented as well. © 2015 Optical Society of America Thi…
Optical absorption and electron paramagnetic resonance of theEα′center in amorphous silicon dioxide
2008
We report a combined study by optical absorption (OA) and electron paramagnetic resonance (EPR) spectroscopy on the E{sub {alpha}}{sup '} point defect in amorphous silicon dioxide (a-SiO{sub 2}). This defect has been studied in {beta}-ray irradiated and thermally treated oxygen-deficient a-SiO{sub 2} materials. Our results have pointed out that the E{sub {alpha}}{sup '} center is responsible for an OA Gaussian band peaked at {approx}5.8 eV and having a full width at half maximum of {approx}0.6 eV. The estimated oscillator strength of the related electronic transition is {approx}0.14. Furthermore, we have found that this OA band is quite similar to that of the E{sub {gamma}}{sup '} center in…
The controlled growth of GaN microrods on Si(111) substrates by MOCVD
2015
Abstract In this paper, a selective area growth (SAG) approach for growing GaN microrods on patterned SiN x /Si(111) substrates by metal-organic chemical vapor deposition (MOCVD) is studied. The surface morphology, optical and structural properties of vertical GaN microrods terminated by pyramidal shaped facets (six { 10 1 ¯ 1 } planes) were characterized using scanning electron microscopy (SEM), room temperature photoluminescence (PL) and Raman spectroscopy, respectively. Measurements revealed high-quality GaN microcolumns grown with silane support. Characterized structures were grown nearly strain-free (central frequency of Raman peak of 567±1 cm −1 ) with crystal quality comparable to bu…
Optical, structural, and morphological characterisation of epitaxial ZnO films grown by pulsed-laser deposition
2013
We report on ZnO epitaxial growth by pulsed-laser deposition (PLD) on different substrates, such as quartz, sapphire, and GaN template. Approximately 1 mu m-thick films were grown under different substrate temperatures and background oxygen conditions. X-ray diffraction analysis indicated preferential growth along the c-axis direction with a full-width at half maximum(FWHM) of the rocking curve as narrow as 230 arcs in the case of the GaN template. Low-temperature photoluminescence showed A-excitonic emission near 3.36 eV and a FWHM of (DXA)-X-0 emission as small as 2.89 meV at 9 K. Atomic force microscope measurements showed that roughness as low as 18 nm could be obtained. These results p…
Vacuum ultraviolet excitation of the 1.9-eV emission band related to nonbridging oxygen hole centers in silica
2004
Physical review / B 69, 153201 (2004). doi:10.1103/PhysRevB.69.153201
Focusing of surface-acoustic-wave fields on (100) GaAs surfaces
2003
Focused surface-acoustic waves (SAWs) provide a way to reach intense acoustic fields for electro- and optoacoustic applications on semiconductors. We have investigated the focusing of SAWs by interdigital transducers (IDTs) deposited on (100)-oriented GaAs substrates. The focusing IDTs have curved fingers designed to account for the acoustic anisotropy of the substrate. Different factors that affect focusing, such as the aperture angle and the configuration of the IDT fingers, were systematically addressed. We show that the focusing performance can be considerably improved by appropriate choice of the IDT metal pads, which, under appropriate conditions, create an acoustic waveguide within t…
Optimization of dual-core and microstructure fiber geometries for dispersion compensation and large mode area
2009
We investigate dual concentric core and microstructure fiber geometries for dispersion compensation. Dispersion values as large as -59 000 ps/(nm km) are achieved, over a broad wavelength range with full width at half maximum exceeding 100 nm. The trade-off between large dispersion and mode area is studied. Geometries with an effective mode area of 30 microm2 and dispersion -19 000 ps/(nm km) and 80 microm2 with -1600 ps/(nm km) are proposed.
Observation of orbitally excited B mesons
1995
Experimental evidence for the existence of orbitally excited B meson states is presented in an analysis of the BÏ and B*Ï distribution of Q = m(B**) - m(B(*)) - m(Ï) using Z0decay data taken with the DELPHI detector at LEP. The mean Q-value of the decays B**â B(*)Ï is measured to be 284 ± 5 (stat.) ± 15 (syst.) MeV/c2, and the Gaussian width of the signal is 79 ± 5 (stat.) ± 8 (syst.) MeV/c2. This signal can be described as a single resonance of mass m = 5732 ± 5 (stat.) ± 20 (syst.) MeV/c2and full width Î = 145 ± 28 MeV/c2. The observed shape is also consistent with the production of several broad and narrow states as predicted by the quark model and partly observed in the D-…
Nuclear physics with ion traps at ISOLDE: present and future
1993
Nuclear physics experiments with ion traps started at the on-line separator ISOLDE/CERN, Geneva, with the installation of the tandem Penning trap mass spectrometer ISOLTRAP. With this device the massM of a stored ion is determined by measuring its cyclotron frequency θc=(q/M)B in a magnetic fieldB. Mass measurements with a resolving powerR=θc/Δθc(FWHM)≈1×106 and accuracies of δM/M≈10−7 were performed on more than sixty unstable isotopes of the elements Rb, Sr, Cs, Ba, Fr, and Ra.