Search results for "Isolation"
showing 10 items of 582 documents
Neo-clerodane diterpenoids from Conyza pyrrhopappa Sch.Bip. ex A.Rich
2019
Two hitherto unknown neo-clerodane-type diterpenoids along with twelve known compounds have been isolated from Conyza pyrrhopappa Sch.Bip. ex A.Rich, a medicinal plant traditionally used across tropical Africa to relieve fever. The structures of isolates have been elucidated by a combination of spectroscopic techniques. The crude extract and the isolated compounds were evaluated in the Hela-S3 cell line and in a panel of microorganisms (bacteria and fungi) at concentrations up to 50 µg/mL. The new compounds were inactive while the pentamethylated flavonoids showed low to significant activity against the cancer cell line used. However, none of the samples showed any activity against the test…
Artificial Intelligence in Monitoring and Diagnostics of Electrical Energy Conversion Systems
2020
Diagnostics and prognostics of electrical energy conversion systems are moving forward with the rapid development of IT and artificial intelligence possibilities. This also broadens the horizons for classical and advanced condition and operation monitoring techniques, resulting in more accurate fault detection, degradation prognosis and calculation of remaining life of energy conversion systems, utilized in every aspect and field of industry today. This paper gives an overview of the necessity for condition monitoring and diagnostics of the mentioned systems, explaining the classical and advanced techniques for diagnostics. Methodology to diagnose and prognose the energy conversion units, w…
Multi-functional Protein Clustering in PPI Networks
2008
Protein-Protein Interaction (PPI) networks contain valuable information for the isolation of groups of proteins that participate in the same biological function. Many proteins play different roles in the cell by taking part in several processes, but isolating the different processes in which a protein is involved is often a difficult task. In this paper we present a method based on a greedy local search technique to detect functional modules in PPI graphs. The approach is conceived as a generalization of the algorithm PINCoC to generate overlapping clusters of the interaction graph in input. Due to this peculiarity, multi-facets proteins are allowed to belong to different groups correspondi…
INNOVATIVE MASS-DAMPING-BASED APPROACHES FOR SEISMIC DESIGN OF TALL BUILDINGS
2021
Mass damping is a well known principle for the reduction of structural vibrations and applied in tall building design in a variety of configurations. With mass usually small (around 1% of building mass), the properly “tuned” mass damper (TMD) shows great effectiveness in reduc-ing wind vibrations, but minor advantages under earthquake excitations. The above limitation can be surpassed by utilizing relatively large mass TMD. For this pur-pose, two different solutions are here proposed. In both cases, the idea is to separate the building into two or more parts, thus allowing for a relative motion between them, and acti-vating the mass damping mechanism. In the first solution, the building is …
Isolation of Adult Rat Cardiomyocytes Using Recombinant Collagenases
2018
Direct isolation of primary cells from tissues and organs allows for the maintenance of important cell characteristics and properties for in vitro studies and a plethora of biomedical applications. Dissociation of cells from the organ of interest is possible due to the enzymatic activity of collagenases. The choice and the dose of these enzymes is the critical step to obtain the maximum number of cells with intact structure and function. In this contest, Abiel collagenases class I (Col G) and class II (Col H) were synthesised using recombinant DNA technologies and their ability to degrade collagen in cell isolation from different tissues was tested. Examples of cells isolated with these enz…
2019
Molecular complexes between glycolic acid and nitrogen were studied in a low-temperature argon matrix with FTIR spectroscopy, and supported by MP2 and BLYPD3 calculations. The calculations indicate 11 and 10 stable complex structures at the MP2 and BLYPD3 levels of theories, respectively. However, only one hydrogen-bonded complex structure involving the most stable SSC conformer of glycolic acid was found experimentally, where the nitrogen molecule is bound with the carboxylic OH group of the SSC conformer. The complex shows a rich site structure variation upon deposition of the matrix in different temperatures and upon annealing experiments, which provide interesting prospects for site-sel…
On the Occurrence of Caffeoyltartronic Acid and Other Phenolics in Chondrilla juncea
1993
Abstract Caffeoyltartronic acid and other eleven phenolic com pounds were identified in the MeOH extract of Chondrilla juncea: the flavonoids luteolin, luteolin-7-glucoside, luteolin-7-galactosylglucuronide and quercetin-3-galactoside; the phenolic acids protocatechuic, caffeic, chlorogenic, isochlorogenic and isoferulic and the coumarins cichoriin and aesculetin. The taxonomic im plications of these com pounds have been discussed.
Isolation of Trimethyltitanium Iodide
1963
Current Bioactive Azole-Containing Natural Products
2010
Pencil Lead as a Matrix for MALDI-ToF Mass Spectrometry of Sensitive Functional Polymers
2007
With the increase in complexity of functional polymers in recent years, MALDI-ToF has become an important tool for gaining precise information on polymer functionality, end groups, and, in special cases, molecular weights. Here we describe how pencil lead, deposited by simply drawing with a regular pencil onto conventional MALDI-ToF targets, can be used as a very attractive matrix for MALDI-ToF mass spectrometry of synthetic polymers. Highly sensitive polymers such as silyl hydride functional poly(styrene), poly(butadiene), and poly(isoprene) have been investigated using conventional MALDI-ToF matrices as well as pencil lead. In all cases, the use of pencil lead prevented oxidation of the h…