Search results for "PERFORMANCE"
showing 10 items of 4457 documents
Determination of aminoglycoside and macrolide antibiotics in meat by pressurized liquid extraction and LC-ESI-MS
2010
A simple method for the simultaneous determination of dihydrostreptomycin, spectinomycin, spiramycin, streptomycin, tilmicosin, and tylosin in meat has been developed using pressurized liquid extraction and LC-triple quadrupole MS (LC-ESI-MS/MS). The pressurized liquid extraction operational parameters were optimized and no protein precipitating and fat removing steps were required. A gradient HPLC separation was developed with ion-pair mobile phases consisting of aqueous 1 mM heptafluorobutyric acid water and methanol. Protonated molecules were used as precursor ions for CID. Data acquisition under MS/MS was achieved by applying multiple reaction monitoring of three fragment ion transition…
Identification of drying oils used in pictorial works of art by liquid chromatography of the 2-nitrophenylhydrazides derivatives of fatty acids.
2004
A new HPLC-UV-Vis method for identification of drying oils from binding media or protective film used in pictorial works of art prior to conservation or restoration is proposed. Chromophore derivatization of fatty acids released by hydrolysis of structural drying oils is studied. The derivatization reagent selected was 2-nitrophenylhydrazine with 1-ethyl-3-(3-dimethyl animopropyl)carbodiimide hydrochloride/pyridine as catalyst. This reaction was carried out using microwave heating. Mobile phase was methanol/water/n-propanol/acetic acid (80:14:5:1) running in isocratic mode. Absorbance was measured at 400nm. In these conditions, hydrazides of myristic, palmitic, oleic, and stearic acids were…
Methacrylate ester-based monolithic columns for nano-LC separation of tocopherols in vegetable oils
2010
The separation and determination of tocopherols (Ts) in vegetable oils by nano-LC chromatography with UV-vis detection using lauryl methacrylate ester-based monolithic columns has been developed. The separation of Ts was optimized in terms of mobile phase composition on the basis of the best compromise among efficiency, resolution and analysis time. Using a mobile phase composed of ACN/methanol/water, an excellent resolution between Ts was achieved within 18 min. The LODs were lower than 0.26 μg/mL, being repeatability values of retention time and peak area below 0.15 and 3.1%, respectively. The method was applied to the quantification of Ts and tocotrienols present in several vegetable oil…
HPLC Method for Cyst(e)ine and Methionine in Infant Formulas
1996
Cyst(e)ine and methionine were converted into cysteic acid and methionine sulfone by oxidizing with performic acid. The oxidized samples were then subjected to acid hydrolysis (6N HCl, 105-110°C/24 hr). After derivatization with phenylisothiocyanate, reverse phase HPLC separation was carried out at 48°C and with UV detection. Different gradients and pH values in the eluent were assayed to determine the best resolution. Analytical parameters, detection and quantification limits, linearity, precision and accuracy, were determined. The method was reliable and accurate for measuring cyst(e)ine and methionine in infant formulae.
Vanhempien kausaaliattribuutioiden yhteys lapsen koulumenestykseen
2000
Cimdu adītāja, stāstniece Jette Užāne un viņas performance
2020
Darbā “Cimdu adītāja, stāstniece Jette Užāne un viņas performance”, izmantojot naratatīva pētījuma metodes, biogrāfisko, autobiogrāfisko un performances pieeju, tiek atklāta cimdu adītājas J.Užānes naratīva veidošanas un darbības dažādie aspekti. J.Užānes devums - lietišķā māksla (cimdu adīšanas) un performance (cimdu stāsti, pasaules uzskats dienasgrāmatās, cimdu izrādes) tiek ievietots plašākā folkloras tradīcijas izpētes kontekstā. J.Užāne atjauno un paplašina cimdu adīšanas tradīciju – pētot etnogrāfisko rakstu un krāsu salikumu nozīmi, viņa atklāj jaunu telpu radīšanai, saglabājot tradīcijas kodolu. J.Užāne cimdam piešķir jaunu jēgu un rada mākslas darbus. Tiek secināts, ka sabiedrība,…
Smart Micro-Grid Performance using Renewable Energy
2020
The aim of this research is to determine the performance of PV panels, wind turbines, battery storage and power imported from the grid to the system which will ensure a reliable energy supply, as well as the technical feasibility of a smart microgrid system. Indonesia’s renewable energy potential for electricity reaches 443 GW, where solar energy is the largest potential, namely 4.8 KWh m–2 or equivalent to 112 000 GWp, but only 10 MWp has been utilized. The most basic problem in this system, namely, the uncertainty of wind energy and solar energy, one of the most vital factors in the optimal size of a renewable energy-based smart microgrid system is the reliability of the system being buil…
Co-produzione di valore nei servizi museali e performance multidimensionali: un approccio dinamico a supporto del management culturale
2021
Contesto della ricerca: nei piccoli centri urbani la co-produzione di servizi museali può essere una leva per la generazione di valore pubblico. Obiettivi del paper: lo scritto mira ad illustrare come un approccio multidimensionale di performance governance sia in grado di offrire una prospettiva sistemica per l’identificazione degli outcome gestionali, organizzativi e di comunità nonché di evidenziare leve per il miglioramento dei processi di generazione di valore nei musei e a beneficio della comunità. Metodologia: dapprima si è proceduto alla revisione della letteratura sul tema della co-produzione di servizi pubblici. Per analizzare le performance di tali contesti collaborativi si è cos…
Polygenic association between attention-deficit/hyperactivity disorder liability and cognitive impairments.
2022
AbstractBackgroundA recent genome-wide association study (GWAS) identified 12 independent loci significantly associated with attention-deficit/hyperactivity disorder (ADHD). Polygenic risk scores (PRS), derived from the GWAS, can be used to assess genetic overlap between ADHD and other traits. Using ADHD samples from several international sites, we derived PRS for ADHD from the recent GWAS to test whether genetic variants that contribute to ADHD also influence two cognitive functions that show strong association with ADHD: attention regulation and response inhibition, captured by reaction time variability (RTV) and commission errors (CE).MethodsThe discovery GWAS included 19 099 ADHD cases …