Search results for "Specimen Handling"

showing 6 items of 46 documents

Infrared based saliva screening test for COVID‐19

2021

Severe acute respiratory syndrome coronavirus 2 (SARS-CoV-2) has resulted in an unprecedented need for diagnostic testing that is critical in controlling the spread of COVID-19. We propose a portable infrared spectrometer with purpose-built transflection accessory for rapid point-of-care detection of COVID-19 markers in saliva. Initially, purified virion particles were characterized with Raman spectroscopy, synchrotron infrared (IR) and AFM-IR. A data set comprising 171 transflection infrared spectra from 29 subjects testing positive for SARS-CoV-2 by RT-qPCR and 28 testing negative, was modeled using Monte Carlo Double Cross Validation with 50 randomized test and model sets. The testing se…

SalivaMaterials scienceCoronavirus disease 2019 (COVID-19)Spectrophotometry InfraredInfraredPoint-of-care testingInfrared spectroscopy010402 general chemistry01 natural sciencesProof of Concept StudySensitivity and SpecificityCatalysisSpecimen HandlingCohort Studies03 medical and health sciences0302 clinical medicineCOVID-19 TestingSpectrophotometryChlorocebus aethiopsmedicineCOVID-19 diagnostic infrared spectroscopy Raman spectroscopy saliva SARS-CoV-2 virionsAnimalsHumansQDLeast-Squares AnalysisSalivaVero CellsMass screening030304 developmental biologyDetection limit0303 health sciencessalivaChromatographymedicine.diagnostic_test010405 organic chemistrySARS-CoV-2COVID-19Discriminant AnalysisGeneral Chemistry030206 dentistryGeneral Medicine0104 chemical sciences3. Good healthPoint-of-Care TestingMonte Carlo MethodATR-FTIRResearch ArticleAngewandte Chemie (International Ed. in English)
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Sample preparation strategies for the determination of psychoactive substances in biological fluids

2020

This review focuses on the existing analytical procedures for the determination of new psychoactive substances (NPS) in biological fluids by chromatographic methods. Direct analysis of samples is scarcely employed and most proposed methodologies include a sample pre-treatment in order to remove matrix interferents and, in some cases, pre-concentrate extracts. Current extraction methods for NPS determination in plasma/serum, urine, and oral fluids have been widely discussed, such as liquid-liquid, solid-phase, and micro extraction approaches, highlighting the advantages and drawbacks of the proposed extraction methodologies. Regarding microextraction approaches, techniques like microextracti…

SorbentLiquid Phase MicroextractionLiquid-Liquid ExtractionClinical Chemistry Tests010402 general chemistry01 natural sciencesBiochemistrySpecimen HandlingAnalytical ChemistryMatrix (chemical analysis)Liquid chromatography–mass spectrometryBiological fluidsHumansSample preparationSolid phase extractionSalivaSolid Phase MicroextractionChromatographyPsychotropic DrugsChromatographyChemistrySolid Phase Extraction010401 analytical chemistryOrganic ChemistryExtraction (chemistry)General MedicineBody Fluids0104 chemical sciencesAnalytical proceduresJournal of Chromatography A
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Electron Microscopic Contrast of the Cytoskeleton and Junctional Complexes of Intestinal Epithelial Cells by Ethanolic Phosphotungstic Acid

2000

After glutaraldehyde fixation and treatment with ethanolic phosphotungstic acid (E-PTA) before plastic embedding, sections of rat large intestine showed a characteristic electron contrasting pattern in epithelial cells. The axis of microvilli, terminal web, a thin band below the luminal plasma membrane, centrioles and junctional complexes (tight junctions, adherens junctions, and desmosomes) appeared highly contrasted. In addition to protein components of microfilaments and intermediate filaments, proteins from the junctional complexes could also be implicated in the contrasting reaction with E-PTA. Mitochondrial membranes, chromatin masses, and nucleoli of enterocytes showed considerable e…

Tissue FixationBiologyMicrofilamentSpecimen HandlingAdherens junctionTerminal webGlycocalyxchemistry.chemical_compoundAnimalsIntestine LargePhosphotungstic acidIntestinal MucosaRats WistarCytoskeletonIntermediate filamentCytoskeletonEthanolMicrovilliStaining and LabelingTissue EmbeddingTight junctionEpithelial CellsPhosphotungstic AcidAgricultural and Biological Sciences (miscellaneous)ChromatinMitochondriaRatsCell biologySolutionsMicroscopy ElectronIntercellular JunctionschemistrySolventsAnatomyCell NucleolusEuropean Journal of Morphology
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Dimensional stability of contemporary irreversible hydrocolloids: humidor versus wet tissue storage.

2012

Statement of problem The storage time and conditions of irreversible hydrocolloid impressions affect their accuracy and in turn the precision of the definitive cast. Recommendations for proper storage are, however, based on theoretical assumptions rather than facts. Purpose The purpose of this study was to assess the influence of the 2 most common storage conditions on the dimensional stability of 7 contemporary irreversible hydrocolloids (IH) for a period of up to 7 days. Material and methods Twelve specimens per material (Blueprint, Cavex CA37, Cavex ColorChange, Jeltrate, Orthoprint, Cavex Orthotrace, and Tetrachrom) were fabricated according to ISO/CD 21563. The specimens were either st…

medicine.medical_specialtyMaterials scienceDental Impression TechniqueTime FactorsPost hocAlginatesDental Impression MaterialsReproducibility of ResultsHumidityModels DentalSurgerySpecimen HandlingmedicineTukey's range testHumansDental Impression TechniqueColloidsOral SurgeryBiomedical engineeringThe Journal of prosthetic dentistry
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Handling and pathology reporting of specimens with carcinoma of the urinary bladder, ureter, and renal pelvis.

2003

Abstract Objective: Pathologists play a pivotal role in the diagnosis and in the report of the pathological features related to prognosis. Methods: To meet these endpoints, the following issues must be accomplished: adequate information about the patient history, proper handling of the specimens, identification of the reliable histopathological techniques necessary to reach the more detailed diagnostic information and evaluate the prognostic variables, and a standardized pathological report. Results: Recent efforts to standardize the histopathological evaluation have generated significant confusion among the urological and pathological communities as well. No consensus has been achieved abo…

medicine.medical_specialtyUrologyBiopsySpecimen HandlingmedicineHumansMedical historyKidney PelvisPhysician's RoleGrading (tumors)Neoplasm StagingBladder cancerPathology Clinicalbusiness.industryUreteral NeoplasmsAnatomical pathologyProfessional PracticePathology Reportmedicine.diseasePrognosisKidney NeoplasmsSurgerySquamous carcinomamedicine.anatomical_structureEpidermoid carcinomaUrinary Bladder NeoplasmsRadiologybusinessRenal pelvisEuropean urology
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Stability of Cannabinoids in Hair Samples Exposed to Sunlight

2000

It has been well recognized that hashish and marihuana lose potency during storage because of a decrease in the content of tetrahydrocannabinol (THC), which is the major psychoactive constituent of cannabis (1). The effect of oxygen on stored plant and resin materials or solutions of pure cannabinoids seems much less significant than that of higher temperatures (≥37 °C) or light (2)(3)(4)(5)(6)(7). A few data are available on the stability of THC and major metabolites in blood (8)(9)(10)(11). However, the stability of cannabinoids in the hair shaft has not been addressed, although scalp hair represents one of the most exposed parts of the body. Therefore, a study was performed to elucidate …

medicine.medical_treatmentClinical BiochemistryCannabinolAnalytical chemistryHashishSpecimen HandlingMatrix (chemical analysis)chemistry.chemical_compoundmedicineCannabidiolHumansDronabinolTetrahydrocannabinolDichloromethaneChromatographybiologyCannabinoidsBiochemistry (medical)biology.organism_classificationSubstance Abuse DetectionchemistrySunlightCannabinolCannabinoidCannabisCannabidiolHairmedicine.drugClinical Chemistry
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