Search results for "Styrenes"

showing 10 items of 63 documents

Polymeric nanoparticles of different sizes overcome the cell membrane barrier.

2012

Abstract Polymeric nanoparticles have tremendous potential either as carriers or markers in treatment for diseases or as diagnostics in biomedical applications. Finding the optimal conditions for effective intracellular delivery of the payload to the location of interest is still a big challenge. The particles have to overcome the barrier of the cell membrane. Here, we investigated the uptake in HeLa cells of fluorescent polystyrene particles with different size and surface charge. Particles stabilized with the nonionic surfactant Lutensol AT50® (132 nm, 180 nm, 242 nm, 816 nm, 846 nm diameter) were synthesized via dispersion polymerization. Cationic particles (120 nm, 208 nm, 267 nm, 603 n…

PolymersAnalytical chemistryPharmaceutical ScienceNanoparticleSurface areaSurface-Active AgentsDrug Delivery SystemsPulmonary surfactantMicroscopy Electron TransmissionCationsHumansSurface chargeParticle SizeFluorescent DyesDispersion polymerizationMicroscopy ConfocalChemistryCell MembraneCationic polymerizationGeneral MedicineFlow CytometryEndocytosisMiniemulsionAlcoholsBiophysicsParticleNanoparticlesPolystyrenesBiotechnologyHeLa CellsEuropean journal of pharmaceutics and biopharmaceutics : official journal of Arbeitsgemeinschaft fur Pharmazeutische Verfahrenstechnik e.V
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Uptake of polymeric nanoparticles in a human induced pluripotent stem cell-based blood-brain barrier model: Impact of size, material, and protein cor…

2021

The blood–brain barrier (BBB) maintains the homeostasis of the central nervous system, which is one of the reasons for the treatments of brain disorders being challenging in nature. Nanoparticles (NPs) have been seen as potential drug delivery systems to the brain overcoming the tight barrier of endothelial cells. Using a BBB model system based on human induced pluripotent stem cells (iPSCs), the impact of polymeric nanoparticles has been studied in relation to nanoparticle size, material, and protein corona. PLGA [poly(lactic-co-glycolic acid)] and PLLA [poly(d,l-lactide)] nanoparticles stabilized with Tween® 80 were synthesized (50 and 100 nm). iPSCs were differentiated into human brain m…

PolymersInduced Pluripotent Stem CellsStatic ElectricityGeneral Physics and AstronomyNanoparticleProtein Corona02 engineering and technology010402 general chemistryBlood–brain barrier01 natural sciencesModels BiologicalGeneral Biochemistry Genetics and Molecular BiologyBiomaterialschemistry.chemical_compoundPolylactic Acid-Polyglycolic Acid CopolymermedicineElectric ImpedanceHumansGeneral Materials ScienceParticle SizeInduced pluripotent stem cellEndothelial CellsCell DifferentiationGeneral ChemistryHuman brain021001 nanoscience & nanotechnologyDynamic Light ScatteringFractionation Field Flow0104 chemical sciencesPLGAmedicine.anatomical_structurechemistryBlood-Brain BarrierSelective adsorptionDrug deliveryCalibrationBiophysicsNanoparticlesPolystyrenesProtein Corona0210 nano-technologyBiointerphases
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α-Chymotrypsin-Catalyzed Reaction Confined in Block-Copolymer Vesicles

2010

Herein the reactivity of the enzyme α-chymotrypsin in the confinement of polystyrene-block-poly(acrylic acid) (PS-b-PAA) vesicles was investigated. Enzyme and substrate molecules were encapsulated in PS-b-PAA vesicles with internal diameters ranging from 26 nm to 165 nm during the formation of the vesicles. While the loading efficiencies of enzyme and substrate molecules were practically identical for vesicles of identical size, they were found to increase with decreasing vesicle size. The kinetics of the α-chymotrypsin catalyzed hydrolysis of N-succinyl-Ala-Ala-Phe-7-amido-4-methylcoumarin (AMC) was evaluated following the increase of the absorption of the product 7-amino-4-methylcoumarin …

PolymersKineticsAcrylic ResinsPhotochemistryMETIS-269964Ultraviolet visible spectroscopyCoumarinsChymotrypsinNanotechnologyOrganic chemistryReactivity (chemistry)Physical and Theoretical ChemistryChymotrypsinbiologyChemistryHydrolysisVesicleSubstrate (chemistry)Atomic and Molecular Physics and OpticsTurnover numberKineticsBiocatalysisbiology.proteinPolystyrenesSpectrophotometry UltravioletAbsorption (chemistry)ChemPhysChem
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An immunoassay for terbutryn using direct hapten linkage to a glutaraldehyde network on the polystyrene surface of standard microtiter plates.

2001

2-Aminobutylamino-4-ethylamino-6-isopropylamino-1,3,5-triazine (ABA-atrazine) has been synthesized and used as a coating hapten in an immunoassay with a monoclonal antibody against terbutryn. Coating was achieved by covalently linking ABA-atrazine to a glutaraldehyde polymer network directly bound to the polystyrene surface of a standard 96-well microtiter plate. The assay was carefully optimized. In particular, the coating hapten concentration had a strong effect on the ELISA sensitivity. By including a pre-incubation step a low test midpoint (IC50-value) of 0.130 microg L(-1) was achieved. As far as we are aware this is the most sensitive ELISA for terbutryn yet reported. The coating-hapt…

PolymersSurface PropertiesEnzyme-Linked Immunosorbent Assayengineering.materialBiochemistrySensitivity and Specificitychemistry.chemical_compoundMicrotiter plateCoatingmedicineChromatographymedicine.diagnostic_testHerbicidesTriazinesNetwork onAntibodies MonoclonalchemistryCovalent bondGlutaralImmunoassayCalibrationengineeringPolystyrenesGlutaraldehydePolystyreneHaptenHaptensFresenius' journal of analytical chemistry
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Straightforward Approach for Preparing Durable Antibacterial ZnO Nanoparticle Coatings on Flexible Substrates

2022

Flexible antibacterial materials have gained utmost importance in protection from the distribution of bacteria and viruses due to the exceptional variety of applications. Herein, we demonstrate a readily scalable and rapid single-step approach for producing durable ZnO nanoparticle antibacterial coating on flexible polymer substrates at room temperature. Substrates used are polystyrene, poly(ethylene-co-vinyl acetate) copolymer, poly(methyl methacrylate), polypropylene, high density polyethylene and a commercial acrylate type adhesive tape. The deposition was achieved by a spin-coating process using a slurry of ZnO nanoparticles in toluene. A stable modification layer was obtained when tolu…

PolymersnanoparticleOrganic ChemistryE. coliPharmaceutical Sciencecoating:NATURAL SCIENCES::Physics [Research Subject Categories]S. aureus540ZnO; nanoparticle; coating; flexible substrate; antibacterial; <i>E. coli</i>; <i>S. aureus</i>Anti-Bacterial AgentsAnalytical Chemistryantibacterialflexible substrateChemistry (miscellaneous)Drug DiscoveryEscherichia coliSolventsZnOPolystyrenesMolecular MedicineZinc OxidePhysical and Theoretical ChemistryToluene
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Attachment of Marine Sponge Cells of Hymeniacidon perleve on Microcarriers

2003

Toward the development of an in vitro cultivation of marine sponge cells for sustainable production of bioactive metabolites, the attachment characteristics of marine sponge cells of Hymeniacidon perleve on three types of microcarriers, Hillex, Cytodex 3, and glass beads, were studied. Mixed cell population and enriched cell fractions of specific cell types by Ficoll gradient centrifugation (6%/8%/15%/20%) were also assessed. Cell attachment ratio (defined as the ratio of cells attached on microcarrier to the total number of cells in the culture) on glass beads is much higher than that on Cytodex 3 and Hillex for both mixed cell population and cell fraction at Ficoll 15-20% interface. The h…

PopulationCell Culture TechniquesFicollMarine BiologyBeadMicrobiologyMaterials TestingCell AdhesionAnimalsCentrifugationBovine serum albumineducationCells Culturededucation.field_of_studyChromatographybiologyMicrocarrierDextransMembranes Artificialbiology.organism_classificationMicrospheresPoriferaSpongeCell culturevisual_artvisual_art.visual_art_mediumbiology.proteinPolystyrenesGlassBiotechnologyBiotechnology Progress
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Polystyrene Sulfonate–Porphyrin Assemblies: Influence of Polyelectrolyte and Porphyrin Structure

2011

In this study, electrostatic self-assembly of different polystyrene sulfonates and a set of tetravalent cationic porphyrins is investigated. It is shown that association of linear polystyrene sulfonates of different molar masses yields finite size nanoscale assemblies that are stable in aqueous solution. Aggregates are compared to the ones of cylindrical brushes, revealing that both form assemblies in the 100 nm range with the charge ratio (molar ratio of porphyrin charges to polyelectrolyte charges) being determining, while the morphology of the resulting network-like assemblies is different for both polyelectrolyte architectures. For the smallest 8k polystyrene sulfonate, in addition, sto…

PorphyrinsLightStatic ElectricityMicroscopy Atomic ForcePorphyrin structurePolystyrene sulfonatechemistry.chemical_compoundScattering Small AnglePolymer chemistryMaterials ChemistryScattering RadiationPhysical and Theoretical ChemistryCationic polymerizationPorphyrinPolyelectrolyteNanostructuresSurfaces Coatings and FilmsQuaternary Ammonium CompoundsNeutron DiffractionZincchemistryPolystyrenesSpectrophotometry UltravioletSelf-assemblyPolystyreneCopperThe Journal of Physical Chemistry B
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Simple, Fast, Bright, and Stable Light Sources

2012

In this work we show that solution-processed light-emitting electrochemical cells (LECs) based on only an ionic iridium complex and a small amount of ionic liquid exhibit exceptionally good performances when applying a pulsed current: sub-second turn-on times and almost constant high luminances (>600 cd m(-2) ) and power efficiencies over the first 600 h. This demonstrates the potential of LECs for applications in solid-state signage and lighting.

SIMPLE (dark matter experiment)Materials scienceLightbusiness.industryMechanical EngineeringAnalytical chemistryTin Compoundschemistry.chemical_elementIonic bondingElectrochemical TechniquesEquipment DesignThiophenesIridiumElectrochemical cellchemistry.chemical_compoundchemistryCoordination ComplexesMechanics of MaterialsIonic liquidPolystyrenesOptoelectronicsGeneral Materials ScienceGlassIridiumbusinessAdvanced Materials
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Some substrates and inhibitors of cytosolic epoxide hydrolase induce sister-chromatid exchanges in mammalian cells, but do not induce gene mutations …

1993

Abstract Trans -stilbene oxide, trans -β-methylstyrene, 7,8-oxide, trans -β-ethylstyrene, 7,8-oxide, trans -β-propylstyrene 7,8-oxide and 4-fluorochalcone oxide were investigated for genotoxic activity in bacterial and mammalian cells, in the absence of external xenobiotic-metabolising systems. All compounds strongly enhanced the frequency of sister-chromatid exchanges (SCE) in cultured human lymphocytes. None of them was mutagenic in Salmonella typhimurium (reversion of the his − strains TA98, TA100 and TA104). The limit of detection was 1 20,000 to 1 10 6 of the activity of the positive control, benzo[ a ]pyrene 4,5-oxide, depending on the compound and the bacterial strain. Trans -β-methy…

Salmonella typhimuriumHealth Toxicology and MutagenesisHamsterSister chromatid exchangeGene mutationChinese hamsterAmes testStyreneschemistry.chemical_compoundChalconeChalconesCricetulusStyrene oxideCricetinaeStilbenesGeneticsAnimalsHumansLymphocytesEpoxide hydrolaseMolecular Biologychemistry.chemical_classificationEpoxide HydrolasesbiologyMutagenicity Testsbiology.organism_classificationEnzymeBiochemistrychemistryEpoxy CompoundsSister Chromatid ExchangeCell DivisionMutagensMutation research
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Potent Aroma Compounds of Two Red Wine Vinegars

2000

Gas chromatography olfactometry (GCO) was used to determine key aroma compounds of two red wine vinegars. Sensory analysis was performed to choose the best neutralization agent of acetic acid (NaOH or MgO) and to test representativeness of four extracts obtained by different methods (dichloromethane extraction, XAD-2, mixture of XAD-2 and XAD-7, and Extrelut resins extraction). Neutralization with NaOH followed by dichloromethane extraction was selected to extract volatile compounds of vinegars. Key odorant compounds were determined by GCO based on detection frequency with 13 people. In the two red wine vinegars, 13 odors were perceived by at least 70% of the panelists, and 8 compounds amon…

Spectrophotometry InfraredAcrylic ResinsWine01 natural sciencesGas Chromatography-Mass SpectrometryButyric acidAcetic acidchemistry.chemical_compound0404 agricultural biotechnology[SDV.IDA]Life Sciences [q-bio]/Food engineeringComputingMilieux_MISCELLANEOUSAromaAcetic AcidDichloromethaneWineChromatographybiology010401 analytical chemistryExtraction (chemistry)04 agricultural and veterinary sciencesGeneral Chemistry[SDV.IDA] Life Sciences [q-bio]/Food engineeringbiology.organism_classification040401 food science0104 chemical scienceschemistryOdorPolystyrenesIon Exchange ResinsGas chromatographyGeneral Agricultural and Biological SciencesJournal of Agricultural and Food Chemistry
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